CN100345505C - Extrusion processing method and device for extracting soybean isoflavone, saponin and oligosaccharide - Google Patents
Extrusion processing method and device for extracting soybean isoflavone, saponin and oligosaccharide Download PDFInfo
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- CN100345505C CN100345505C CNB2004100755525A CN200410075552A CN100345505C CN 100345505 C CN100345505 C CN 100345505C CN B2004100755525 A CNB2004100755525 A CN B2004100755525A CN 200410075552 A CN200410075552 A CN 200410075552A CN 100345505 C CN100345505 C CN 100345505C
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Abstract
The present invention relates to a method and a device for extracting soybean isoflavone, saponin and oligosaccharide. The present invention is characterized in that the present invention provides an extrusion puffing processing device and an extrusion puffing processing method for extracting soybean isoflavone, soybean saponin and soybean oligosaccharide by extrusion puffing soybeans, soybean gemmule and soybean hypocotyls and defatting. When defatted soybean meal obtained from extrusion puffing products of soybeans of the present invention, and soybean meal obtained from a traditional oil preparation method by leaching soybean squeezing blanks and the existing oil preparation methods by puffing and leaching soybeans at home and abroad are respectively put in extracting devices for extracting the substances with a solvent, the yield of soybean isoflavone is increased by 15% to 100% by the method of the present invention, and the yields of soybean saponin and soybean oligosaccharide are increased by 10% to 70%; when the defatted soybean meal obtained from the present invention, and soybean meal prepared from soybean gemmule soybean hypocotyls and soybean meal, which are treated by microwaves or ultrasonic waves and defatted, or are directly defatted, are respectively put in extracting devices for extracting the substances with a solvent, the yields of soybean isoflavone, soybean saponin and soybean oligosaccharide are increased by 10% to 80% by the method of the present invention.
Description
Technical field
The present invention relates to the processing of farm products method and apparatus, more particularly, relate to the processing method and the processing unit (plant) of soybean in the process of extracting isoflavones, soyasaponins, soyabean oligosaccharides, soybean germ, soybean plumular axis, dregs of beans.
Technical background
Studies show that isoflavones, soyasaponins, soyabean oligosaccharides have the physiological action of multiple beneficial in health, as: 1, can treat and suppress cancers such as prostate cancer, colon cancer, breast cancer; 2, reduce the synthetic of body inner cholesterol, reduce body's cholesterol concentration, treatment and angiocardiopathy preventing; 3, the treatment women's climacteric syndrome, as vexed urgency make an uproar, osteoporosis, blood fat rising etc.; 4, improve immune function of human body, anti-inflammatory effect etc. is arranged.Therefore extremely people's concern of the extraction of isoflavones, soyasaponins, soyabean oligosaccharides.
The raw material that extracts mainly comprises soybean, soybean germ, soybean plumular axis, dregs of beans etc.In recent years, relate to patented technology more (Jiang Haokui etc., the technology of continuously extracting glycitin, compound sugar, saponin, the application number: 00109111 that extracts isoflavones, soyasaponins, soyabean oligosaccharides; Nie Zejun, the method for extraction isoflavones, application number: 02109628; Wang Zhe etc., the extracting method of isoflavones, soyasaponins, soyabean oligosaccharides, application number: 02109533.7 etc.), above-mentioned raw materials is entering extraction equipment, before solvent (as ethanol) extraction, through cleaning, microwave or ultrasonic wave processing, degreasing, enter extraction equipment then, use solvent (as ethanol) to extract process such as isoflavones, soyasaponins, soyabean oligosaccharides; Perhaps above-mentioned raw materials passes through cleaning, degreasing earlier, enters extraction equipment again, uses process such as solvent (as ethanol) extraction, at last until obtaining isoflavones, soyasaponins, soyabean oligosaccharides.Practice shows: soybean, soybean germ, soybean plumular axis, dregs of beans etc. are through above-mentioned preliminary treatment process, enter extraction equipment again, use the process of solvent extraction isoflavones, soyasaponins, soyabean oligosaccharides, the yield of the isoflavones that obtains, soyasaponins, soyabean oligosaccharides is lower.
Summary of the invention
The object of the present invention is to provide extrusion processing method and processing unit (plant) in a kind of process of extracting isoflavones, soyasaponins, soyabean oligosaccharides.What it can solve that prior art exists extracts isoflavones, soyasaponins, problem that the soyabean oligosaccharides yield is lower with solvent from materials such as soybean, soybean germ, soybean plumular axis, dregs of beans.
In order to reach the purpose that addresses the above problem, technical measures of the present invention are, a kind of isoflavones that is used to extract is provided, saponin, the extruding machining apparatus of compound sugar, the sleeve of wherein said pressurizing unit is by the first segment sleeve 2 of axial opposite opened, the second joint sleeve 4, the 3rd joint sleeve 5 and the 4th joint sleeve 7 are formed, described sleeve is by back and preceding the installation, sleeve integral body is axial opposite opened, first segment sleeve 2, the second joint sleeve 4, the 3rd joint sleeve 5 and the 4th joint sleeve 7 can be closed, by the above-mentioned top and the bottom of respectively saving sleeve of securing member locking, first segment screw rod 1, the second joint screw rod 6 and the 3rd joint screw rod 10 are sleeved on the main shaft 15, described screw rod is rotated with main shaft 15 by back and preceding the installation; Two opposite opened integral body that first segment sleeve 2, the second joint sleeve 4 the 3rd joint sleeve 5 and the 4th joint sleeve 7 are formed can distinguish around the shaft that A and B outwards rotate, and sleeve integral body is separated vertically; The compression ratio of screw rod integral body is 7～15, the externally threaded helical angle of the second joint screw rod 6, the 3rd joint screw rod 10 and the helical angle of the internal thread of second sleeve 4, the 3rd sleeve 5, quadruplet tube 7 about equally, theory was exported 1～4 times of volume when the small end that the end of the 3rd joint screw rod 10 and the volume between template 8 inner surfaces should be the 3rd joint screw rod 10 was goed around; The aperture of the nib 9 of template 8 is Φ 6mm～Φ 14mm, and is adjustable, and the length of nib 9 is 6mm～20mm, and is adjustable.
The present invention also provides a kind of isoflavones that is used to extract, saponin, the extruding method of compound sugar, wherein said method may further comprise the steps: with soybean, soybean germ, soybean plumular axis, dregs of beans is cleared up earlier, when moisture content surpasses 14%, carry out low temperature drying, bake out temperature is less than 45 ℃, make moisture content be less than or equal to 14%, pulverize then, particle diameter is 0.65mm～0.90mm, push above-mentioned soybean with described pressurizing unit, soybean germ, soybean plumular axis, the crushed material of dregs of beans, wherein the parameter area of pressurizing unit is: first segment sleeve 2 is not heated or cooled, the second joint sleeve 4, the temperature of the 3rd joint sleeve 5 and the 4th joint sleeve 7 is respectively 30 ℃～60 ℃, 45 ℃～80 ℃ and 65 ℃～95 ℃, self controllable adjusting; The rotating speed of the screw rod integral body that first segment screw rod 1, the second joint screw rod 6 and the 3rd joint screw rod 10 are formed is 130r/min～265r/min, and is adjustable.
Soybean of the present invention, soybean germ, soybean plumular axis, extrusion processing methods such as dregs of beans, expanded soybean to be extruded, soybean germ, soybean plumular axis, dregs of beans etc. are through cleaning (impurity elimination, remove stone, de-iron etc.), if moisture content is higher than 14%, should carry out low temperature drying, baking temperature should be less than 45 ℃, make its moisture content be less than or equal to 14%, pulverize above-mentioned material then, particle diameter after the pulverizing is 0.65mm～0.90mm, above-mentioned comminuting matter enters extrusion pressing puffing apparatus from feeding mouth, material behind the extrusion is extruded from nib, cooling back degreasing, puff after the degreasing enters extraction equipment, uses the solvent extraction isoflavones, soyasaponins, soyabean oligosaccharides.
The present invention compared with prior art has following advantage:
1. the soybean puffing thing of extrusion processing of the present invention, the dregs of beans and the traditional soybean press for extracting juice base leaching system oil that obtain through degreasing leach the oily dregs of beans that obtains of system with present domestic and international soybean puffing, enter extraction equipment respectively, compare with solvent extraction isoflavones, soyasaponins, soyabean oligosaccharides, wherein the isoflavones yield can improve 15%～100%, and the yield of soyasaponins and soyabean oligosaccharides all can improve 10%～70%.
2. the puff of the soybean germ of extrusion processing of the present invention, soybean plumular axis, dregs of beans, the swelling soya dreg and soybean germ, soybean plumular axis, the dregs of beans that obtain through degreasing pass through earlier or handle without microwave or ultrasonic wave, the dregs of beans that obtains of degreasing again, enter extraction equipment respectively, compare with solvent extraction isoflavones, soyasaponins, soyabean oligosaccharides, can improve the yield 10%～80% of isoflavones, soyasaponins, soyabean oligosaccharides.
Description of drawings
Fig. 1 is the front view of extrusion pressing puffing apparatus of the present invention;
Fig. 2 is the half sectional view of the vertical view of extrusion pressing puffing apparatus of the present invention.
The specific embodiment
Referring to accompanying drawing 1 and Fig. 2, to implement the sleeve of extrusion pressing puffing apparatus of the present invention and form by first segment sleeve 2, the second joint sleeve 4, the 3rd joint sleeve 5 and the 4th joint sleeve 7 by back and preceding installation of axial opposite opened, sleeve integral body is axial opposite opened.First segment sleeve 2, the second joint sleeve 4, the 3rd joint sleeve 5 and the 4th joint sleeve 7 closures during work, by securing member 14, securing member 16, securing member 13, securing member 17, securing member 12, securing member 18, securing member 11 and the above-mentioned top and the bottom of respectively saving sleeve of securing member 19 lockings, first segment screw rod 1, the second joint screw rod 6 and the 3rd joint screw rod 10 are sleeved on the main shaft 15, described screw rod is rotated with main shaft 15 by back and preceding the installation.When checking the inner surface of the outer surface of first segment screw rod 1, the second joint screw rod 6 and the 3rd joint screw rod 10 parts and first segment sleeve 2, the second joint sleeve 4, the 3rd joint sleeve 5 and the 4th joint sleeve 7, template of dismantling 8 and securing member 14, securing member 16, securing member 13, securing member 17, securing member 12, securing member 18, securing member 11 and securing member 19, save two opposite opened integral body that sleeve 7 is formed by first segment sleeve 2, the second joint sleeve 4 the 3rd joint sleeve 5 and the 4th, A and B outwards rotate around the shaft respectively, and sleeve integral body is separated vertically.The compression ratio of screw rod integral body is 7～15, the externally threaded helical angle of the second joint screw rod 6, the 3rd joint screw rod 10 and the helical angle of the internal thread of second sleeve 4, the 3rd sleeve 5, quadruplet tube 7 about equally, theory that the end of the 3rd joint screw rod 10 and the volume between template 8 inner surfaces should be the 3rd small end that saves screw rod 10 when going around transfers out 1～4 times of volume.First segment sleeve 2 is not heated or cooled, and the outer surface of the second joint sleeve 4, the 3rd joint sleeve 5 and the 4th joint sleeve 7 is by the vapours or the electrical heating of band pressure, by cooling water or force air cooling, the warm self controllable adjusting of tube.
During duty, the first segment sleeve 2 of above-mentioned extrusion pressing puffing apparatus is not heated or cooled, the temperature of the second joint sleeve 4, the 3rd joint sleeve 5 and the 4th joint sleeve 7 is respectively 30 ℃～60 ℃, 45 ℃～80 ℃ and 65 ℃～95 ℃, self controllable adjusting, the aperture of the nib 9 of template 8 are that Φ 6mm～Φ 14mm is adjustable, and the length of nib 9 is that 6mm～20mm is adjustable, the rotating speed of the screw rod integral body that first segment screw rod 1, the second joint screw rod 6 and the 3rd joint screw rod 10 are formed is 130r/min～265r/min, and is adjustable.
Soybean, soybean germ, soybean plumular axis, dregs of beans are earlier through cleaning (impurity elimination, remove stone, de-iron etc.), if moisture content surpasses 14%, need through low temperature drying, bake out temperature is less than 45 ℃, make moisture content be less than or equal to 14%, milling soya seeds, soybean germ, soybean plumular axis, dregs of beans then, the particle diameter after the pulverizing is 0.65mm～0.90mm, above-mentioned material is from feeding mouth 3 feeding extrusion pressing puffing apparatus.Material saves in the extrusion chamber of the outer surface of screw rod 6, the 3rd joint screw rod 10 and the inner surface formation that first segment sleeve 2, the second joint sleeve 4, the 3rd joint sleeve the 5, the 4th save sleeve 7 at first segment screw rod 1, second, rotate with main shaft 15, first segment screw rod 1, the second joint screw rod 6 and the 3rd joint screw rod 10, simultaneously, material is extruded to template 8 by feeding mouth 3 and moves.Be extruded material in the cavity and extrude, form the column structure puff of porous from nib 9.Then it is cooled to 50 ℃～55 ℃, carry out degreasing (as entering the fat etc. that infuser extracts soybean, soybean germ, soybean plumular axis, dregs of beans), the residual oil content of the extrusion dregs of rice should be less than 1%, enter extraction equipment then, use the process of solvent extraction isoflavones, soyasaponins, soyabean oligosaccharides, until obtaining isoflavones, soyasaponins, soyabean oligosaccharides.
Claims (5)
1. one kind is used to extract isoflavones, saponin, the extruding machining apparatus of compound sugar, it is characterized in that, the sleeve of described extruding machining apparatus is by the first segment sleeve (2) of axial opposite opened, the second joint sleeve (4), the 3rd joint sleeve (5) and the 4th joint sleeve (7) are formed, described sleeve is by back and preceding the installation, sleeve integral body is axial opposite opened, first segment sleeve (2), the second joint sleeve (4), the 3rd joint sleeve (5) and the 4th joint sleeve (7) can be closed, by the above-mentioned top and the bottom of respectively saving sleeve of securing member locking, first segment screw rod (1), the second joint screw rod (6) and the 3rd joint screw rod (10) are sleeved on the main shaft (15), described screw rod is rotated with main shaft (15) by back and preceding the installation; Two opposite opened integral body that first segment sleeve (2), the second joint sleeve (4), the 3rd joint sleeve (5) and the 4th joint sleeve (7) are formed can distinguish around the shaft (A, B) outwards rotation separates sleeve integral body vertically; The compression ratio of screw rod integral body is 7～15, the helical angle of the internal thread of externally threaded helical angle and second sleeve (4) of the second joint screw rod (6), the 3rd joint screw rod (10), the 3rd sleeve (5), quadruplet tube (7) about equally, theory was exported 1～4 times of volume when the small end that the end of the 3rd joint screw rod (10) and the volume between template (8) inner surface should be the 3rd joint screw rod (10) was goed around; The aperture of the nib (9) of template (8) is Φ 6mm～Φ 14mm, and is adjustable, and the length of nib (9) is 6mm～20mm, and is adjustable.
2. one kind is used to extract isoflavones, saponin, the extruding method of compound sugar, it is characterized in that, said method comprising the steps of: with soybean, soybean germ, soybean plumular axis, dregs of beans is cleared up earlier, when moisture content surpasses 14%, carry out low temperature drying, bake out temperature is less than 45 ℃, make moisture content be less than or equal to 14%, pulverize then, particle diameter is 0.65mm～0.90mm, push above-mentioned soybean with the described extruding machining apparatus of claim 1, soybean germ, soybean plumular axis, the crushed material of dregs of beans, wherein the parameter area of pressurizing unit is: first segment sleeve (2) is not heated or cooled, the second joint sleeve (4), the temperature of the 3rd joint sleeve (5) and the 4th joint sleeve (7) is respectively 30 ℃～60 ℃, and 45 ℃～80 ℃ and 65 ℃～95 ℃, self controllable adjusting; The rotating speed of the screw rod integral body that first segment screw rod (1), the second joint screw rod (6) and the 3rd joint screw rod (10) are formed is 130r/min～265r/min, and is adjustable.
3. extruding method as claimed in claim 2, it is characterized in that, the crushed material of soybean, soybean germ, soybean plumular axis, dregs of beans should cool off after extruding, its temperature is 50 ℃～55 ℃, degreasing again, the residual oil content of the extruding dregs of rice after the degreasing should enter extraction equipment then less than 1%, with solvent extraction isoflavones, saponin, compound sugar wherein.
4. extruding method as claimed in claim 2 is characterized in that, described cleaning comprises impurity elimination, removes stone, de-iron.
5. extruding method as claimed in claim 3 is characterized in that, described solvent is an ethanol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100755525A CN100345505C (en) | 2004-12-21 | 2004-12-21 | Extrusion processing method and device for extracting soybean isoflavone, saponin and oligosaccharide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100755525A CN100345505C (en) | 2004-12-21 | 2004-12-21 | Extrusion processing method and device for extracting soybean isoflavone, saponin and oligosaccharide |
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| Publication Number | Publication Date |
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| CN1631274A CN1631274A (en) | 2005-06-29 |
| CN100345505C true CN100345505C (en) | 2007-10-31 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB2004100755525A Expired - Fee Related CN100345505C (en) | 2004-12-21 | 2004-12-21 | Extrusion processing method and device for extracting soybean isoflavone, saponin and oligosaccharide |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100432238C (en) * | 2005-12-09 | 2008-11-12 | 山东理工大学 | Method and apparatus for extruding and cooking starch syrup raw muterial and saccharification method |
| CN101054605B (en) * | 2007-05-11 | 2011-06-15 | 山东理工大学 | Processing method, device and saccharification method for starch syrup raw material by extruding and adding enzyme |
| CN102838575B (en) * | 2012-08-30 | 2014-08-20 | 东北农业大学 | Method for extracting isoflavone in soybean germ with aid of extrusion and expansion pretreatments |
| CN111204071A (en) * | 2018-11-22 | 2020-05-29 | 海崴生物科技股份有限公司 | Continuous plant extraction machine |
| CN110183409B (en) * | 2019-06-17 | 2021-02-23 | 山东师范大学 | Method for efficiently extracting soybean isoflavone from umbilicus |
| CN111748047B (en) * | 2020-07-29 | 2022-03-29 | 河南科技大学 | Preparation method of dioscorea opposita oligosaccharide |
| CN115286603A (en) * | 2022-08-30 | 2022-11-04 | 三原利华生物技术有限公司 | Method for preparing soybean isoflavone and soyasaponin based on defatted soybean germ |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4248141A (en) * | 1978-08-18 | 1981-02-03 | Miller Jr Harry W | Method and apparatus for debittering soybeans |
| CN1254811A (en) * | 1998-11-25 | 2000-05-31 | 孙逸龙 | Luminous artistical lampshade |
| CN1265037A (en) * | 1997-07-30 | 2000-08-30 | 因迪纳有限公司 | Soya extract, process for its prepn. and pharmaceutical compsn. |
| CN1456558A (en) * | 2002-05-10 | 2003-11-19 | 九台市东山粮库贸易部 | Method for extracting soybean isoflavone |
-
2004
- 2004-12-21 CN CNB2004100755525A patent/CN100345505C/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4248141A (en) * | 1978-08-18 | 1981-02-03 | Miller Jr Harry W | Method and apparatus for debittering soybeans |
| CN1265037A (en) * | 1997-07-30 | 2000-08-30 | 因迪纳有限公司 | Soya extract, process for its prepn. and pharmaceutical compsn. |
| CN1254811A (en) * | 1998-11-25 | 2000-05-31 | 孙逸龙 | Luminous artistical lampshade |
| CN1456558A (en) * | 2002-05-10 | 2003-11-19 | 九台市东山粮库贸易部 | Method for extracting soybean isoflavone |
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| CN1631274A (en) | 2005-06-29 |
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Application publication date: 20050629 Assignee: Zibo JINDA Technology Co., Ltd. Assignor: Shandong University of Technology Contract record no.: 2010370000062 Denomination of invention: Extrusion processing method and device for extracting soybean isoflavone, saponin and oligosaccharide Granted publication date: 20071031 License type: Exclusive License Record date: 20100224 |
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Granted publication date: 20071031 Termination date: 20121221 |