CH519475A - Organic sulphonate prodn - Google Patents
Organic sulphonate prodnInfo
- Publication number
- CH519475A CH519475A CH1234567A CH1234567A CH519475A CH 519475 A CH519475 A CH 519475A CH 1234567 A CH1234567 A CH 1234567A CH 1234567 A CH1234567 A CH 1234567A CH 519475 A CH519475 A CH 519475A
- Authority
- CH
- Switzerland
- Prior art keywords
- olefins
- olefin
- degrees
- water
- organic
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
- C07C303/20—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by addition of sulfurous acid or salts thereof to compounds having carbon-to-carbon multiple bonds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The olefin is pre-treated by bodying until viscosity is increased by 5 to 30 fold by finely dispersing (e.g. blowing or churning into the olefins) at 90 degrees to 200 degrees C a molecular O2-containing gas through the olefin. Sulphitation then gives high yields, quickly and without solvents excess reactants or initiators. Aqueous sulphurous acid or one of its salts is used optionally formed in situ unless the organic sulphonate is required in the form of its salt of an organic base, when the organic base, such as alkanolamine, is mixed with the bodied olefins and 1/2 to 1/4 of the wt. of the olefins of water is added, and finely dispersed SO2 is passed through until the pH of a 5% solution is below 7.0 and the degree of solubility of a test sample in water does not increase any further.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH1234567A CH519475A (en) | 1967-09-01 | 1967-09-01 | Organic sulphonate prodn |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH1234567A CH519475A (en) | 1967-09-01 | 1967-09-01 | Organic sulphonate prodn |
Publications (1)
Publication Number | Publication Date |
---|---|
CH519475A true CH519475A (en) | 1972-02-29 |
Family
ID=4382154
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH1234567A CH519475A (en) | 1967-09-01 | 1967-09-01 | Organic sulphonate prodn |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH519475A (en) |
-
1967
- 1967-09-01 CH CH1234567A patent/CH519475A/en not_active IP Right Cessation
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PL | Patent ceased |