CH312054A - Process for the preparation of a diammonium compound. - Google Patents

Process for the preparation of a diammonium compound.

Info

Publication number
CH312054A
CH312054A CH312054DA CH312054A CH 312054 A CH312054 A CH 312054A CH 312054D A CH312054D A CH 312054DA CH 312054 A CH312054 A CH 312054A
Authority
CH
Switzerland
Prior art keywords
amyl
ethoxy
bis
decane
preparation
Prior art date
Application number
Other languages
German (de)
Inventor
Ag J R Geigy
Original Assignee
Ag J R Geigy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ag J R Geigy filed Critical Ag J R Geigy
Publication of CH312054A publication Critical patent/CH312054A/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/33—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings
    • C07C211/34—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings of a saturated carbon skeleton
    • C07C211/38—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of rings other than six-membered aromatic rings of a saturated carbon skeleton containing condensed ring systems

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  



  Verfahren zur Herstellung einer   Diammoniumverbindung.   



   Gegenstand vorliegenden Patentes ist ein Verfahren zur Herstellung einer Diammoniumverbindung, welches dadurch gekennzeichnet ist, dass man 1 Mol 1,10-Bis-[ss-(n  amyl-methylamino)-äthoxy]-dekan    mit 2 Mol   Methylbromid umsetzt.   



   Die so erhaltene neue Verbindung, das 1,10 Bis-   [fl- (n-amyl-dimethyl-ammonium)-äthoxy j-    dekan-dibromid, schmilzt bei   182 .    Sie soll als Arzneimittel und als Zwischenprodukt für Arzneimittel Verwendung finden.



      B6ispt61 :   
21,4 Teile   1,      : 10-Bis- [ss- (n-amyl-methyl-      amino')-äthoxy]-dekan werden    mit 80 Teilen troekenem Aceton und 12 Teilen Methylbro  , nid    14 Stunden im   Einsehmelzrohr    in einem W'asserbad von   50-60     erwärmt. Nach Erkalten wird abgesaugt und das erhaltene 1,10 Bis-   [ss-      (n-amyl-dimethyl-ammonium)-äthoxy]-      dekan-dibromid    aus wenig abs,. Methanol unter Zusatz von Butanon umkristallisiert. Es schmilzt bei   182 .     



   PATENTANSPRUCH :
Verfahren zur Herstellung einer Diammoniumverbindung, dadurch gekennzeichnet, dass man   1    Mol   1,      10-Bis-[ss-(n-amyl-methylamino)-    äthoxy]-dekan mit 2 Mol Methylbromid umsetzt.



   Die erhaltene neue Verbindung, das 1,10  Bis-Fss- (n-amyl-dimetlZyl-ammonium)-äthoxy]      dekan-dibromid,    schmilzt bei   182 .    

**WARNUNG** Ende DESC Feld konnte Anfang CLMS uberlappen**.





  



  Process for the preparation of a diammonium compound.



   The present patent relates to a process for the preparation of a diammonium compound, which is characterized in that 1 mole of 1,10-bis [ss- (n amyl-methylamino) ethoxy] decane is reacted with 2 moles of methyl bromide.



   The new compound obtained in this way, 1.10 bis- [fl- (n-amyl-dimethyl-ammonium) -ethoxy j-decane dibromide, melts at 182. It is intended to be used as a medicinal product and as an intermediate for medicinal products.



      B6ispt61:
21.4 parts of 1,: 10-bis- [ss- (n-amyl-methyl-amino ') -ethoxy] decane are mixed with 80 parts of dry acetone and 12 parts of methylbrown in a water bath for 14 hours in a one-piece tube heated from 50-60. After cooling, it is filtered off with suction and the 1.10 bis- [ss- (n-amyl-dimethyl-ammonium) -ethoxy] -decane dibromide obtained from a little abs. Recrystallized methanol with the addition of butanone. It melts at 182.



   PATENT CLAIM:
Process for the preparation of a diammonium compound, characterized in that 1 mol of 1, 10-bis [ss- (n-amyl-methylamino) ethoxy] decane is reacted with 2 mol of methyl bromide.



   The new compound obtained, 1.10 bis-Fss- (n-amyl-dimetlZyl-ammonium) ethoxy] decane dibromide, melts at 182.

** WARNING ** End of DESC field could overlap beginning of CLMS **.

Claims (1)

**WARNUNG** Anfang CLMS Feld konnte Ende DESC uberlappen **. ** WARNING ** Beginning of CLMS field could overlap end of DESC **. Verfahren zur Herstellung einer Diammoniumverbindung. Process for the preparation of a diammonium compound. Gegenstand vorliegenden Patentes ist ein Verfahren zur Herstellung einer Diammoniumverbindung, welches dadurch gekennzeichnet ist, dass man 1 Mol 1,10-Bis-[ss-(n amyl-methylamino)-äthoxy]-dekan mit 2 Mol Methylbromid umsetzt. The present patent relates to a process for the preparation of a diammonium compound, which is characterized in that 1 mole of 1,10-bis [ss- (n amyl-methylamino) ethoxy] decane is reacted with 2 moles of methyl bromide. Die so erhaltene neue Verbindung, das 1,10 Bis- [fl- (n-amyl-dimethyl-ammonium)-äthoxy j- dekan-dibromid, schmilzt bei 182 . Sie soll als Arzneimittel und als Zwischenprodukt für Arzneimittel Verwendung finden. The new compound obtained in this way, 1.10 bis- [fl- (n-amyl-dimethyl-ammonium) -ethoxy j-decane dibromide, melts at 182. It is intended to be used as a medicinal product and as an intermediate for medicinal products. B6ispt61 : 21,4 Teile 1, : 10-Bis- [ss- (n-amyl-methyl- amino')-äthoxy]-dekan werden mit 80 Teilen troekenem Aceton und 12 Teilen Methylbro , nid 14 Stunden im Einsehmelzrohr in einem W'asserbad von 50-60 erwärmt. Nach Erkalten wird abgesaugt und das erhaltene 1,10 Bis- [ss- (n-amyl-dimethyl-ammonium)-äthoxy]- dekan-dibromid aus wenig abs,. Methanol unter Zusatz von Butanon umkristallisiert. Es schmilzt bei 182 . B6ispt61: 21.4 parts of 1,: 10-bis- [ss- (n-amyl-methyl-amino ') -ethoxy] decane are mixed with 80 parts of dry acetone and 12 parts of methylbrown in a water bath for 14 hours in a one-piece tube heated from 50-60. After cooling, it is filtered off with suction and the 1.10 bis- [ss- (n-amyl-dimethyl-ammonium) -ethoxy] -decane dibromide obtained from a little abs. Recrystallized methanol with the addition of butanone. It melts at 182. PATENTANSPRUCH : Verfahren zur Herstellung einer Diammoniumverbindung, dadurch gekennzeichnet, dass man 1 Mol 1, 10-Bis-[ss-(n-amyl-methylamino)- äthoxy]-dekan mit 2 Mol Methylbromid umsetzt. PATENT CLAIM: Process for the preparation of a diammonium compound, characterized in that 1 mol of 1, 10-bis [ss- (n-amyl-methylamino) ethoxy] decane is reacted with 2 mol of methyl bromide. Die erhaltene neue Verbindung, das 1,10 Bis-Fss- (n-amyl-dimetlZyl-ammonium)-äthoxy] dekan-dibromid, schmilzt bei 182 . The new compound obtained, 1.10 bis-Fss- (n-amyl-dimetlZyl-ammonium) ethoxy] decane dibromide, melts at 182.
CH312054D 1952-06-13 1952-06-13 Process for the preparation of a diammonium compound. CH312054A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH312054T 1952-06-13
CH308688T 1955-07-31

Publications (1)

Publication Number Publication Date
CH312054A true CH312054A (en) 1955-12-15

Family

ID=25735509

Family Applications (1)

Application Number Title Priority Date Filing Date
CH312054D CH312054A (en) 1952-06-13 1952-06-13 Process for the preparation of a diammonium compound.

Country Status (1)

Country Link
CH (1) CH312054A (en)

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