CH216112A - Process for the preparation of an azo dye. - Google Patents

Process for the preparation of an azo dye.

Info

Publication number
CH216112A
CH216112A CH216112DA CH216112A CH 216112 A CH216112 A CH 216112A CH 216112D A CH216112D A CH 216112DA CH 216112 A CH216112 A CH 216112A
Authority
CH
Switzerland
Prior art keywords
azo dye
preparation
ogynaphthalene
aminobenzoyl
diphenyl
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH216112A publication Critical patent/CH216112A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B29/00Monoazo dyes prepared by diazotising and coupling
    • C09B29/24Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
    • C09B29/28Amino naphthols
    • C09B29/30Amino naphtholsulfonic acid

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)

Description

  

  Verfahren zur Herstellung eines     Azofarbstoi%s.       Vorliegendes Patent bezieht sich auf ein       Verfahren    zur Herstellung eines     Azofarb-          stoffes,    dadurch gekennzeichnet, dass man die       Diazoverhindung    von     N-(3-Aminobenzoyl)-          N-,do        dekahydro    -     diphenyl-2'-methyl    -     phenyl-          amin    mit     1-(2',5'-Dimethyl-4'-chlorbenzol-          sulfoamino)    - 8     -ogynaphthalin-    3,

  6 -     disulfon-          säure    vereinigt.  



  Der so erhaltene Farbstoff ist trocken ein         rotes        Pulver,    dessen     lebhafte    rote Färbungen  auf Wolle sehr gute Echtheitseigenschaften,  insbesondere gegen Wäsche, Walke, Schweiss  und Seewasser, sowie gute Lichtechtheit be  sitzen.  



       Beispiel:     38,6 Teile     N-(3-Aminobenzoyl)-N-dodeka-          hydro    -     diphenyl-2'-methyl    -     phenylamin    der  Formel  
EMI0001.0025     
    werden     diazotiert    und die     Diazoverbindung     wird in     Gegenwart    von überschüssigem Ätz-         kalk    mit 53 Teilen     1-(2',5'-Dimethyl-4'-          chlorbenzol-sufoamino)-    8 -ogynaphthalin-3,6-           disulfonsäure    vereinigt.

   Der Farbstoff wird  dann in das     Natriumsalz    übergeführt und  dieses abgeschieden und getrocknet.



  Process for the production of an azo dye% s. The present patent relates to a process for the production of an azo dye, characterized in that the diazo compound of N- (3-aminobenzoyl) - N-, do decahydro - diphenyl-2'-methyl - phenyl amine with 1- ( 2 ', 5'-dimethyl-4'-chlorobenzenesulfoamino) - 8 -ogynaphthalene- 3,

  6 - disulfonic acid combined.



  The dyestuff thus obtained is a dry red powder, the vivid red colorations of which have very good fastness properties on wool, in particular against laundry, fulling, perspiration and seawater, and also good lightfastness.



       Example: 38.6 parts of N- (3-aminobenzoyl) -N-dodecahydro-diphenyl-2'-methyl-phenylamine of the formula
EMI0001.0025
    are diazotized and the diazo compound is combined with 53 parts of 1- (2 ', 5'-dimethyl-4'-chlorobenzene-sufoamino) -8 -ogynaphthalene-3,6-disulfonic acid in the presence of excess quicklime.

   The dye is then converted into the sodium salt, which is deposited and dried.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines Azofarb- stoffes, dadurch gekennzeichnet, daB man die Diazoverbindung von N-(3-Aminobenzoyl)- N-dodekahydro - diphenyl-2'-methyl - phenyl- mit 1-(2',5"-Dimethyl-4'-chlorbenzol- i amin sulfoamino)- 8 -ogynaphthalin - 3,6 - disulfon- säure vereinigt. Claim: Process for the production of an azo dye, characterized in that the diazo compound of N- (3-aminobenzoyl) -N-dodecahydro-diphenyl-2'-methyl-phenyl- with 1- (2 ', 5 "-dimethyl -4'-chlorobenzene- i amine sulfoamino) - 8 -ogynaphthalene - 3,6 - disulfonic acid combined. Der so erhaltene Farbstoff ist trocken ein rotes Pulver, dessen lebhafte rote Färbungen auf Walle sehr gute Echtheitseigenschaften, insbesondere gegen Wäsche, Walke, Schweiss und Seewasser, sowie gute Lichtechtheit be sitzen. The dyestuff thus obtained is a dry red powder, the vivid red colorations of which have very good fastness properties, especially against laundry, fulling, sweat and seawater, and good lightfastness.
CH216112D 1938-06-02 1939-05-26 Process for the preparation of an azo dye. CH216112A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE216112X 1938-06-02
CH212418T 1939-05-26

Publications (1)

Publication Number Publication Date
CH216112A true CH216112A (en) 1941-07-31

Family

ID=25725235

Family Applications (1)

Application Number Title Priority Date Filing Date
CH216112D CH216112A (en) 1938-06-02 1939-05-26 Process for the preparation of an azo dye.

Country Status (1)

Country Link
CH (1) CH216112A (en)

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