CH204128A - Process for the production of a vat dye. - Google Patents

Process for the production of a vat dye.

Info

Publication number
CH204128A
CH204128A CH204128DA CH204128A CH 204128 A CH204128 A CH 204128A CH 204128D A CH204128D A CH 204128DA CH 204128 A CH204128 A CH 204128A
Authority
CH
Switzerland
Prior art keywords
production
vat dye
dye
azobenzene
condensed
Prior art date
Application number
Other languages
German (de)
Inventor
Aktiengesellsc Farbenindustrie
Original Assignee
Ig Farbenindustrie Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ig Farbenindustrie Ag filed Critical Ig Farbenindustrie Ag
Publication of CH204128A publication Critical patent/CH204128A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09BORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B43/00Preparation of azo dyes from other azo compounds
    • C09B43/32Preparation of azo dyes from other azo compounds by reacting carboxylic or sulfonic groups, or derivatives thereof, with amines; by reacting keto-groups with amines
    • C09B43/36Preparation of azo dyes from other azo compounds by reacting carboxylic or sulfonic groups, or derivatives thereof, with amines; by reacting keto-groups with amines with amino-anthracene or amino-anthraquinone dyes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

      Zusatzpatent    zum Hauptpatent Nr. 200369.    Verfahren zur Herstellung eines     Nüpenfarbstoffes.       Vorliegendes Patent bezieht sich auf ein       Verfahren:    zur     Herstellung        eines        Küpenfarb-          stoffes,    dadurch gekennzeichnet,     dass    man  ein funktionelles Derivat     ,der        Azobenzol-3    .

       5-          diearbonsäure    mit     l@Ami.no-5-benzoylamino-          anthTachinon        im.        Molekularverhältnis    1:2       kondensiert.     



  Der so erhaltene     Farbstoff    färbt Baum  wolle aus     violetter        güpe    in sehr echten gel  ben Tönen.  



  <I>Beispiel:</I>  31 Teile     Azobenzol-3.        5-dicarbonsäure-di-          chlorid,    das beispielsweise durch Kondensa  tion von     Nitrosobenzol    mit     5-Amino-isophthal-          säure    und Behandlung der so erhaltenen       Dicarbonsäure    mit     Thionylchloridhergestellt     werden kann und das     nach    dem     Umkristalli-          sieren        aus        Benzin.    :

  den     Schmelzpunkt    121   C       zeigt,    werden in     o-Dichlorbenzol        durch    mehr-         ständiges    Erhitzen mit 70     Teilen        1-Amino-          Zi-benzoylamiuoanthrachinon    kondensiert. Der       gebildete        Farbstoff        wird    dann abgesaugt,     ,ge-          waschen    und     getrocknet.  



      Additional patent to main patent no. 200369. Process for the production of a pebble dye. The present patent relates to a process: for the production of a vat dye, characterized in that a functional derivative, the azobenzene-3.

       5- diacid with l@Ami.no-5-benzoylamino-anthTachinon im. Molecular ratio 1: 2 condensed.



  The dye obtained in this way dyes cotton from violet güpe in very real yellow tones.



  <I> Example: </I> 31 parts of azobenzene-3. 5-dicarboxylic acid dichloride, which can be produced, for example, by condensation of nitrosobenzene with 5-amino-isophthalic acid and treatment of the dicarboxylic acid thus obtained with thionyl chloride, and that after recrystallization from gasoline. :

  shows the melting point 121 ° C., are condensed in o-dichlorobenzene by heating for several times with 70 parts of 1-amino-Zi-benzoylamiuoanthraquinone. The dye formed is then filtered off with suction, washed and dried.

 

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines Küpen- farbstoffes, dadurch ,gekennzeichnet, dass man ein funktionelles Derivat der Azobenzol-3 . 5- dicarbonsäure mit 1-Amino-5-benzoylamino- authrachinon im MoIekularverhältniss 1: PATENT CLAIM: Process for the production of a vat dye, characterized in that a functional derivative of azobenzene-3. 5- dicarboxylic acid with 1-amino-5-benzoylamino-authraquinone in a molecular ratio of 1: 2 kondensiert. Der so erhaltene Farbstoff färbt Baum wolle aus violetter güpe in. sehr echten :gel ben Tönen. 2 condensed. The dye obtained in this way dyes cotton from a violet güpe in very real: yellow tones.
CH204128D 1936-09-16 1937-09-06 Process for the production of a vat dye. CH204128A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE204128X 1936-09-16
CH200369T 1938-03-21

Publications (1)

Publication Number Publication Date
CH204128A true CH204128A (en) 1939-04-15

Family

ID=25723474

Family Applications (1)

Application Number Title Priority Date Filing Date
CH204128D CH204128A (en) 1936-09-16 1937-09-06 Process for the production of a vat dye.

Country Status (1)

Country Link
CH (1) CH204128A (en)

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