CH202440A - Process for the production of a condensation product. - Google Patents

Process for the production of a condensation product.

Info

Publication number
CH202440A
CH202440A CH202440DA CH202440A CH 202440 A CH202440 A CH 202440A CH 202440D A CH202440D A CH 202440DA CH 202440 A CH202440 A CH 202440A
Authority
CH
Switzerland
Prior art keywords
condensation product
production
pyridine
water
toluidoanthraquinone
Prior art date
Application number
Other languages
German (de)
Inventor
Gesellschaft Fuer Chemis Basel
Original Assignee
Chem Ind Basel
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chem Ind Basel filed Critical Chem Ind Basel
Publication of CH202440A publication Critical patent/CH202440A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
    • C09B1/16—Amino-anthraquinones
    • C09B1/20—Preparation from starting materials already containing the anthracene nucleus
    • C09B1/36—Dyes with acylated amino groups
    • C09B1/46—Dyes with acylated amino groups the acyl groups being residues of cyanuric acid or an analogous heterocyclic compound
    • C09B1/467—Dyes with acylated amino groups the acyl groups being residues of cyanuric acid or an analogous heterocyclic compound attached to two or more anthraquinone rings
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
    • C09B1/16—Amino-anthraquinones
    • C09B1/20—Preparation from starting materials already containing the anthracene nucleus
    • C09B1/26—Dyes with amino groups substituted by hydrocarbon radicals
    • C09B1/32—Dyes with amino groups substituted by hydrocarbon radicals substituted by aryl groups
    • C09B1/325—Dyes with no other substituents than the amino groups
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B43/00—Preparation of azo dyes from other azo compounds
    • C09B43/12—Preparation of azo dyes from other azo compounds by acylation of amino groups
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B43/00—Preparation of azo dyes from other azo compounds
    • C09B43/12—Preparation of azo dyes from other azo compounds by acylation of amino groups
    • C09B43/124—Preparation of azo dyes from other azo compounds by acylation of amino groups with monocarboxylic acids, carbamic esters or halides, mono- isocyanates, or haloformic acid esters
    • C09B43/132—Preparation of azo dyes from other azo compounds by acylation of amino groups with monocarboxylic acids, carbamic esters or halides, mono- isocyanates, or haloformic acid esters having the carboxylic group directly attached to an aromatic carbocyclic ring
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B69/00—Dyes not provided for by a single group of this subclass

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Coloring (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

  <B>Zusatzpatent</B> zum     Hauptpatent    Nr. 200372.    Verfahren zur     Herstellung    eines     Kondensationsproduktes.       Es wurde gefunden, dass man ein neues  Kondensationsprodukt erhält, wenn man auf       1-Amino-4-p-toluidoanthrachinon    2     Mol    des       Toluol-2.        4-disulfochlorids    in Gegenwart von       Pyridin    einwirken lässt. Das neue Produkt  bildet ein dunkles Pulver, das sich in Wasser  mit violetter Farbe auflöst und zum Färben  in der Textilindustrie verwendet werden  kann.  



  <I>Beispiel:</I>  Man verrührt 16,4 Teile     1-Amino-4-p-          toluidoanthrachinon    mit 120 Teilen     Pyridin.     Hierauf streut man 36     Teile        Toluoldisulfo-          chlorid    hinzu, steigert die Temperatur bis  zum Siedepunkt und hält bei dieser Tem  peratur, bis eine Probe der     Reaktionsmasse     bei dieser Temperatur in Wasser löslich ist.

    Das     Pyridin    wird durch     Destillation    im Va  kuum     entfernt,    der Rückstand     in    warmem  Wasser aufgelöst, und das Kondensations  produkt mit gussalzenden     Mitteln,    z. B. Na-         triumchlorid    abgeschieden. Nach dem Filtrie  ren, nötigenfalls nach dem Waschen mit Salz  wasser, wird das Produkt getrocknet; es kann  durch     Ausziehen    mit Alkoholen, z. B.     trok-          kenem    Methylalkohol, frei von anorganischen  Salzen erhalten werden. Man erhält ein  dunkles Pulver, dessen     wässrige    Lösung  Wolle aus saurem Bade violett anfärbt.



  <B> Additional patent </B> to main patent no. 200372. Process for the production of a condensation product. It has been found that a new condensation product is obtained if 2 moles of 2-toluene are added to 1-amino-4-p-toluidoanthraquinone. 4-disulfochlorids can act in the presence of pyridine. The new product forms a dark powder that dissolves in water with a purple color and can be used for dyeing in the textile industry.



  <I> Example: </I> 16.4 parts of 1-amino-4-p-toluidoanthraquinone are stirred with 120 parts of pyridine. 36 parts of toluene disulfochloride are sprinkled on this, the temperature is raised to the boiling point and maintained at this temperature until a sample of the reaction mass is soluble in water at this temperature.

    The pyridine is removed by distillation in vacuo, the residue dissolved in warm water, and the condensation product with casting salting agents, eg. B. sodium chloride deposited. After Filtrie ren, if necessary after washing with salt water, the product is dried; it can be made by soaking with alcohols, e.g. B. dry methyl alcohol, free of inorganic salts can be obtained. A dark powder is obtained, the aqueous solution of which dyes wool from an acid bath purple.

Claims (1)

PATENTANSPRUCH: Verfahren zur Herstellung eines Konden sationsproduktes, dadurch gekennzeichnet, dass man auf 1-Amino-4-p-toluidoanthrachi- non 2 Mol des Toluol-2.4-disidfochlorids in Gegenwart von Pyridin einwirken lässt. Das neue Produkt bildet ein dunkles Pulver, das sieh in Wasser mit violetter Farbe auflöst und zum Färben in der Textilindustrie ver wendet werden kann. PATENT CLAIM: Process for the production of a condensation product, characterized in that 1-amino-4-p-toluidoanthraquinone is allowed to act on 2 mol of toluene-2,4-disidofochloride in the presence of pyridine. The new product forms a dark powder that dissolves in water with a purple color and can be used for dyeing in the textile industry.
CH202440D 1936-11-11 1936-11-11 Process for the production of a condensation product. CH202440A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CH202440T 1936-11-11
CH200372T 1936-11-11

Publications (1)

Publication Number Publication Date
CH202440A true CH202440A (en) 1939-01-15

Family

ID=4442279

Family Applications (5)

Application Number Title Priority Date Filing Date
CH202440D CH202440A (en) 1936-11-11 1936-11-11 Process for the production of a condensation product.
CH202439D CH202439A (en) 1936-11-11 1936-11-11 Process for the production of a condensation product.
CH202441D CH202441A (en) 1936-11-11 1936-11-11 Process for the production of a condensation product.
CH202442D CH202442A (en) 1936-11-11 1936-11-11 Process for the production of a condensation product.
CH200372D CH200372A (en) 1936-11-11 1936-11-11 Process for the production of a condensation product.

Family Applications After (4)

Application Number Title Priority Date Filing Date
CH202439D CH202439A (en) 1936-11-11 1936-11-11 Process for the production of a condensation product.
CH202441D CH202441A (en) 1936-11-11 1936-11-11 Process for the production of a condensation product.
CH202442D CH202442A (en) 1936-11-11 1936-11-11 Process for the production of a condensation product.
CH200372D CH200372A (en) 1936-11-11 1936-11-11 Process for the production of a condensation product.

Country Status (2)

Country Link
CH (5) CH202440A (en)
FR (1) FR828532A (en)

Also Published As

Publication number Publication date
CH202439A (en) 1939-01-15
CH200372A (en) 1938-10-15
CH202441A (en) 1939-01-15
FR828532A (en) 1938-05-19
CH202442A (en) 1939-01-15

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