CH202171A - Process for the preparation of a nitro dye. - Google Patents
Process for the preparation of a nitro dye.Info
- Publication number
- CH202171A CH202171A CH202171DA CH202171A CH 202171 A CH202171 A CH 202171A CH 202171D A CH202171D A CH 202171DA CH 202171 A CH202171 A CH 202171A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- nitro dye
- brown
- dye
- nitro
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B51/00—Nitro or nitroso dyes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. 199466. Verfahren zur Herstellung eines Nitrofarbstoffes. Gegenstand des vorliegenden Zusatz patentes ist ein Verfahren zur .Herstellung eines Nitrofarbstoffes, welches dadurch ge kennzeichnet ist, dass man 4-Aminophenyl-l- methyltaurin mit 2-Chlor-3,5-dinitro-l-benzoe- säure kondensiert.
Beispiel: 230 Gewichtsteile 4-Aminophenyl-l-methyl- taurin von der Formel:
EMI0001.0010
werden in wenig Wasser mit Natriumkarbonat neutralisiert und in Gegenwart von 136 Ge wichtsteilen kristallisiertem Natriumacetat mit 268,5 Gewichtsteilen 2-chlor-3,5-dinitro- 1-benzoesaurem Natrium einige Stunden zum Sieden erhitzt. Nach beendeter Kondensation wird der Farbstoff durch Aussalzen isoliert.
Das so erhaltene Produkt stellt ein braunes Pulver dar, das in Wasser mit brauner Farbe leicht löslich ist und Leder in gelbbraunen Tönen gleichmässig durchfärbt.
Additional patent to main patent no. 199466. Process for the production of a nitro dye. The subject of the present additional patent is a process for the production of a nitro dye, which is characterized in that 4-aminophenyl-1-methyltaurine is condensed with 2-chloro-3,5-dinitro-1-benzoic acid.
Example: 230 parts by weight of 4-aminophenyl-l-methyl-taurine of the formula:
EMI0001.0010
are neutralized in a little water with sodium carbonate and heated to boiling for a few hours in the presence of 136 parts by weight of crystallized sodium acetate with 268.5 parts by weight of 2-chloro-3,5-dinitro-1-benzoic acid sodium. When the condensation has ended, the dye is isolated by salting out.
The product obtained in this way is a brown powder which is easily soluble in water with a brown color and uniformly dyes leather in yellow-brown shades.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE202171X | 1936-05-02 | ||
CH199466T | 1939-11-09 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH202171A true CH202171A (en) | 1938-12-31 |
Family
ID=25723315
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH202171D CH202171A (en) | 1936-05-02 | 1937-04-22 | Process for the preparation of a nitro dye. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH202171A (en) |
-
1937
- 1937-04-22 CH CH202171D patent/CH202171A/en unknown
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