CH200301A - Process for the preparation of a quaternary ammonium compound. - Google Patents
Process for the preparation of a quaternary ammonium compound.Info
- Publication number
- CH200301A CH200301A CH200301DA CH200301A CH 200301 A CH200301 A CH 200301A CH 200301D A CH200301D A CH 200301DA CH 200301 A CH200301 A CH 200301A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- quaternary ammonium
- ammonium compound
- chlorobenzyl
- chloride
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title claims description 4
- 150000003856 quaternary ammonium compounds Chemical class 0.000 title claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- BASMANVIUSSIIM-UHFFFAOYSA-N 1-chloro-2-(chloromethyl)benzene Chemical compound ClCC1=CC=CC=C1Cl BASMANVIUSSIIM-UHFFFAOYSA-N 0.000 claims description 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 2
- PBLNBZIONSLZBU-UHFFFAOYSA-N 1-bromododecane Chemical compound CCCCCCCCCCCCBr PBLNBZIONSLZBU-UHFFFAOYSA-N 0.000 description 1
- 125000006282 2-chlorobenzyl group Chemical group [H]C1=C([H])C(Cl)=C(C([H])=C1[H])C([H])([H])* 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000000645 desinfectant Substances 0.000 description 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- TWFQJFPTTMIETC-UHFFFAOYSA-N dodecan-1-amine;hydron;chloride Chemical compound [Cl-].CCCCCCCCCCCC[NH3+] TWFQJFPTTMIETC-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- -1 o-chlorobenzyl chloride - Dodecylammoniumchlorid Chemical compound 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung einer quaternären Ammoniumverbindung. Gegenstand vorliegenden Patentes ist ein Verfahren zur Darstellung einer quaternären Ammoniumverbindung, dadurch ,gekennzeich net, dass man N-Dimethyl-dodecylamin durch Einwirken von o-Chlorbenzylchlorid in N-Di- methyl - N - (o - chlorbenzyl)
- dodecylammo - niumchlorid überführt.
Das so erhältliche Produkt bildet eine gelbliche harzige Masse, die sieh in Wasser und Alkohol leicht löst. Es soll als Desinfek- tions- und Konservierungsmittel Anwendung finden.
<I>Beispiel:</I> 213 Gewichtsteile N-Dimethyldodecyl- amin, erhältlich .durch Umsetzung von Dime- thylamin mit Dodecylbromid als farblose Flüssigkeit vom Siedepunkt 120-121' bei 7-8 mm Druck, werden mit 161 Gewichts teilen o-Chlorbenzylchlorid 12 Stunden auf <B>100'</B> erwärmt.
Nach dem Erkalten erhält man das Dimethyl - N - (o_ chlorbenzyl) - ,dodecyl- ammoniumchlorid als sehwach .gelbliche, har zige Masse, die sich in Wasser und in Alko hol leicht löst.
Process for the preparation of a quaternary ammonium compound. The subject of the present patent is a process for the preparation of a quaternary ammonium compound, characterized in that N-dimethyl-dodecylamine is converted into N-dimethyl - N - (o - chlorobenzyl) by the action of o-chlorobenzyl chloride
- Dodecylammoniumchlorid transferred.
The product obtainable in this way forms a yellowish resinous mass which dissolves easily in water and alcohol. It should be used as a disinfectant and preservative.
<I> Example: </I> 213 parts by weight of N-dimethyldodecylamine, obtainable by reacting dimethylamine with dodecyl bromide as a colorless liquid with a boiling point of 120-121 'at 7-8 mm pressure, with 161 parts by weight o- Chlorobenzyl chloride heated to <B> 100 '</B> for 12 hours.
After cooling, the dimethyl - N - (o_chlorbenzyl) -, dodecylammonium chloride is obtained as a very weak, yellowish, resinous mass that dissolves easily in water and alcohol.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH175812T | 1934-04-03 | ||
| DE200301X | 1935-05-25 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH200301A true CH200301A (en) | 1938-09-30 |
Family
ID=25719761
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH200301D CH200301A (en) | 1934-04-03 | 1936-04-15 | Process for the preparation of a quaternary ammonium compound. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH200301A (en) |
-
1936
- 1936-04-15 CH CH200301D patent/CH200301A/en unknown
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