CH180296A - Process for the production of a new dye. - Google Patents
Process for the production of a new dye.Info
- Publication number
- CH180296A CH180296A CH180296DA CH180296A CH 180296 A CH180296 A CH 180296A CH 180296D A CH180296D A CH 180296DA CH 180296 A CH180296 A CH 180296A
- Authority
- CH
- Switzerland
- Prior art keywords
- new dye
- production
- amino
- blue
- acid
- Prior art date
Links
- 239000002253 acid Substances 0.000 claims description 4
- 235000005811 Viola adunca Nutrition 0.000 claims description 2
- 235000013487 Viola odorata Nutrition 0.000 claims description 2
- 235000002254 Viola papilionacea Nutrition 0.000 claims description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 210000002268 wool Anatomy 0.000 claims description 2
- 244000154870 Viola adunca Species 0.000 claims 1
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 2
- FYXJXUMICYGRKV-UHFFFAOYSA-N 2-[(2-amino-5-nitrophenyl)methylsulfonylmethyl]-4-nitroaniline Chemical compound NC1=CC=C([N+]([O-])=O)C=C1CS(=O)(=O)CC1=CC([N+]([O-])=O)=CC=C1N FYXJXUMICYGRKV-UHFFFAOYSA-N 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 240000009038 Viola odorata Species 0.000 description 1
- 244000172533 Viola sororia Species 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 125000000664 diazo group Chemical class [N-]=[N+]=[*] 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 235000010288 sodium nitrite Nutrition 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B29/00—Monoazo dyes prepared by diazotising and coupling
- C09B29/24—Monoazo dyes prepared by diazotising and coupling from coupling components containing both hydroxyl and amino directing groups
- C09B29/28—Amino naphthols
- C09B29/30—Amino naphtholsulfonic acid
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Zusatzpatent zum Hauptpatent Nr. <B>178224.</B> Verfahren zur Herstellung eines neuen Farbstoffes. Es wurde gefunden, dass man einen neuen Farbstoff erhält, wenn man diazotiertes 2- Amino-5-nitrophenylmethylsulfon in saurem Medium mit der 9--Amino-8-oxynaphthalin- 6-sulfonsäure vereinigt. Der neue Farbstoff bildet ein blaues Pulver, das sich in Wasser init blativioletter Farbe löst.
Es färbt Wolle # ai -is saurem Bade in echten blaustichig vio- letten Farbtönen an. <I>Beispiel:</I> <B>216</B> Teile '2)-Amino-5-nitrophenylmethyl- sulfon werden in konzentrierter Schwefel säure mit<B>69</B> Teilen Natriumnitrit diazotiert und die Lösung in Eiswasser gegossen.
In diese Diazolösung trägt man eine neutrale Lösung von<B>9-39</B> Teilen 29-Amino-8-oxynaph- t3 thalin-6-sulfonsä,ure ein und beschleunigt die Reaktion gegebenenfalls durch Zugabe von Natriumacetat. Der Farbstoff wird nun ab- filtriert, ausgewaschen und getrocknet.
Additional patent to main patent no. <B> 178224. </B> Process for producing a new dye. It has been found that a new dye is obtained when diazotized 2-amino-5-nitrophenylmethylsulfone is combined with 9-amino-8-oxynaphthalene-6-sulfonic acid in an acidic medium. The new dye forms a blue powder that dissolves in water with a blue-violet color.
It stains wool # ai -is acid bath in real blue tinged violet shades. <I> Example: </I> <B> 216 </B> parts of '2) -amino-5-nitrophenylmethylsulfone are diazotized in concentrated sulfuric acid with <B> 69 </B> parts of sodium nitrite and the solution in Poured ice water.
A neutral solution of 9-39 parts of 29-amino-8-oxynaph-t3 thalin-6-sulfonic acid is introduced into this diazo solution and the reaction is accelerated, if necessary, by adding sodium acetate. The dye is then filtered off, washed out and dried.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH180296T | 1934-03-24 | ||
| CH178224T | 1934-03-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH180296A true CH180296A (en) | 1935-10-15 |
Family
ID=25720090
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH180296D CH180296A (en) | 1934-03-24 | 1934-03-24 | Process for the production of a new dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH180296A (en) |
-
1934
- 1934-03-24 CH CH180296D patent/CH180296A/en unknown
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