CH155340A - Process for the production of a nitrogenous vat dye. - Google Patents
Process for the production of a nitrogenous vat dye.Info
- Publication number
- CH155340A CH155340A CH155340DA CH155340A CH 155340 A CH155340 A CH 155340A CH 155340D A CH155340D A CH 155340DA CH 155340 A CH155340 A CH 155340A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- nitrogenous
- vat dye
- dye
- vat
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- 238000000034 method Methods 0.000 title claims description 3
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 title claims description 3
- 239000000984 vat dye Substances 0.000 title claims description 3
- 239000000975 dye Substances 0.000 claims description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 3
- 229920000742 Cotton Polymers 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- -1 1-benzanthronyl-1-amino-5-p-tolylaminoanthraquinone Chemical compound 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 235000011118 potassium hydroxide Nutrition 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Paper (AREA)
- Coloring (AREA)
Description
Yerfaliren zur Herstellung eines stiehstofflialtigen ILüpenfarbstoffes. Vorliegendes Patent bezieht sich auf ein Verfahren zur Herstellung eines stickstoffhal tigen Küpenfarbstoffes, dadurch gekennzeich- riet, dass man Bz.-1-Benzanthronyl-l-amino- 5-p-tolylaminoanthrachinon mit einem alkali schen Kondensationsmittel behandelt.
Der neue Farbstoff löst sich in konzen trierter Schwefelsäure mit grüner Farbe und färbt Baumwolle aus violettblauer Küpe in echten graublauen Tönen.
Beispiel: 50 Teile Bz.-1-Benzantbronyl-l-amino-5- p-tolylaminoarithrachinon (ein nicht vei-küp- barer Körper, der sich in konzentrierter Schwefelsäure mit braungelber Farbe löst und durch Kondensation von Bz.-1-Brombenzan- thron mit 1-Amino-5-p-tolylaminoanthrachirion erhalten wird werden allmählich in eine auf 1ä0-160 gehaltene Schmelze von 300 Teilen Ätzkali und 50 Teilen Alkohol eingetragen.
Die Reaktionstemperatur lässt man hierauf auf 180-2000 steigen und verdünnt nach etwa 1 Stunde die Schmelze reit Wasser. Der Farbstoff wird durch Ausblasen mit Luft abgeschieden und gewaschen.
Yerfaliren for the production of a pulp dye containing nitrogen. The present patent relates to a process for the preparation of a nitrogen-containing vat dye, characterized in that 1-benzanthronyl-1-amino-5-p-tolylaminoanthraquinone is treated with an alkaline condensing agent.
The new dye dissolves in concentrated sulfuric acid with a green color and dyes cotton from a violet-blue vat in real gray-blue tones.
Example: 50 parts of Bz.-1-Benzantbronyl-l-amino-5-p-tolylaminoarithraquinone (a non-kneadable body, which dissolves in concentrated sulfuric acid with a brownish yellow color and is produced by the condensation of Bz.-1-Brombenzan thrones obtained with 1-amino-5-p-tolylaminoanthrachirion are gradually introduced into a melt of 300 parts of caustic potash and 50 parts of alcohol kept at 1-0-160.
The reaction temperature is then allowed to rise to 180-2000 and, after about 1 hour, the melt is diluted with water. The dye is separated by blowing with air and washed.
Claims (1)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE155340X | 1930-02-04 | ||
| DE301230X | 1930-12-30 | ||
| CH152887T | 1931-01-29 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH155340A true CH155340A (en) | 1932-06-15 |
Family
ID=27177317
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH155340D CH155340A (en) | 1930-02-04 | 1931-01-29 | Process for the production of a nitrogenous vat dye. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH155340A (en) |
-
1931
- 1931-01-29 CH CH155340D patent/CH155340A/en unknown
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