CH151569A - Process for the preparation of a dye of the thioindigo series. - Google Patents
Process for the preparation of a dye of the thioindigo series.Info
- Publication number
- CH151569A CH151569A CH151569DA CH151569A CH 151569 A CH151569 A CH 151569A CH 151569D A CH151569D A CH 151569DA CH 151569 A CH151569 A CH 151569A
- Authority
- CH
- Switzerland
- Prior art keywords
- dye
- preparation
- thioindigo series
- chloro
- methyl
- Prior art date
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- Coloring (AREA)
Description
Verfahren zur Darstellung eines Farbstoffes der Thioindigoreihe. Gegenstand des vorliegenden Zusatzpaten tes ist ein Verfahren zur Darstellung von 4 Methyl-6-4'-dichlorbisthionaphtenindigo, wel ches dadurch gekennzeichnet ist, dass ein reaktionsfähiges 2-Derivat des 4-Methyl-6- chlor-2.3-diketodihydrothionaphtenchinons mit 4-Clilor-3-oxythionaphten kondensiert wird.
Der so erhaltene Farbstoff ist ein rotes Pulver und färbt Baumwolle in klaren roten Tönen von guten Echtheitseigenschaften an. <I>Beispiel:</I> 32 Gewichtsteile 4-Methyl - 6 -chlor- 2 . 3 diketödihydrothiotiaphtenchirion-2-(p-dimethyl- amino)-anil werden mit 18,5 Gewichtsteilen 4-Chlor-3-oxythionaphten in 600 Gewichts teilen Eisessig zum Sieden erhitzt. Der nach dem Erkalten abgesaugte und neutral ge- waschene- Farbstoff färbt Baumwolle in klaren roten Tönen von guten Echtheits eigenschaften an.
Process for the preparation of a dye of the thioindigo series. The subject of the present additional patent is a process for the preparation of 4 methyl-6-4'-dichlorobisthionaphthene indigo, wel ches is characterized in that a reactive 2-derivative of 4-methyl-6-chloro-2,3-diketodihydrothionaphtenquinone with 4-Clilor- 3-oxythionaphten is condensed.
The dye thus obtained is a red powder and dyes cotton in clear red shades with good fastness properties. <I> Example: </I> 32 parts by weight of 4-methyl-6-chloro-2. 3 diketödihydrothiotiaphtenchirion-2- (p-dimethyl-amino) -anil are heated to the boil with 18.5 parts by weight of 4-chloro-3-oxythionaphtene in 600 parts by weight of glacial acetic acid. The dye, which is sucked off after cooling and washed neutrally, dyes cotton in clear red shades with good fastness properties.
Claims (1)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE151569X | 1929-05-18 | ||
CH148503T | 1930-05-14 |
Publications (1)
Publication Number | Publication Date |
---|---|
CH151569A true CH151569A (en) | 1931-12-15 |
Family
ID=25715228
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CH151569D CH151569A (en) | 1929-05-18 | 1930-05-14 | Process for the preparation of a dye of the thioindigo series. |
Country Status (1)
Country | Link |
---|---|
CH (1) | CH151569A (en) |
-
1930
- 1930-05-14 CH CH151569D patent/CH151569A/en unknown
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