CH125389A - Process for the preparation of a soluble tin compound. - Google Patents
Process for the preparation of a soluble tin compound.Info
- Publication number
- CH125389A CH125389A CH125389DA CH125389A CH 125389 A CH125389 A CH 125389A CH 125389D A CH125389D A CH 125389DA CH 125389 A CH125389 A CH 125389A
- Authority
- CH
- Switzerland
- Prior art keywords
- preparation
- tin compound
- soluble tin
- water
- tin
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 5
- 150000003606 tin compounds Chemical class 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- 208000035473 Communicable disease Diseases 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- CVNKFOIOZXAFBO-UHFFFAOYSA-J tin(4+);tetrahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[Sn+4] CVNKFOIOZXAFBO-UHFFFAOYSA-J 0.000 claims description 2
- 230000007935 neutral effect Effects 0.000 claims 1
- 229910052787 antimony Inorganic materials 0.000 description 4
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical class [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 description 2
- 229910021626 Tin(II) chloride Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- UGECXIBKSDDQDH-UHFFFAOYSA-L disodium;3,4-dihydroxybenzene-1,2-disulfonate Chemical compound [Na+].[Na+].OC1=CC=C(S([O-])(=O)=O)C(S([O-])(=O)=O)=C1O UGECXIBKSDDQDH-UHFFFAOYSA-L 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 230000009931 harmful effect Effects 0.000 description 1
- 230000035876 healing Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 229940079877 pyrogallol Drugs 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/003—Compounds containing elements of Groups 4 or 14 of the Periodic Table without C-Metal linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Description
Verfahren zur Herstellung eüier löslichen Zinnverbindung. Im Hauptpatent ist ein Verfahren be schrieben, nach dem man eine Komplexver bindung von Antimon mit Pyrogalloldisulfo- säui-e erhält. Verbindungen dieser Art unter scheiden sich voll gewöhnlichen Salzen des Antimons dadurch, dass sie eine Reihe von Iiealitioneir dieser Salze nicht haben. Sie enthalten nämlich das Antimon in festerer sogenannter Komplexverbindung.
Diese Stoffe sind als Heilmittel verwendbar, da in ihnen infolge der festere Bindung des Antimons die schädliche Wirkung gegenüber der Heil wirkung zurückgedrängt ist.
Es wurde gefunden, dass die gleichen Ver hältnisse obwalten, wenn man brenzkatechin- disrilfosaui-es Natrium mit Zirinhydroxyd um setzt.
Die Ausführung des Verfahrens erfolgt ani besten in der Weise, dass man brenz- katechindisulfosaures Natrium mit der erfor derlichen iSTerge der Zinnverbindung in wässe riger Lösung, gegebenenfalls unter Erwärmen umsetzt..
<I>Beispiel:</I> 35 gr brerizkatecliiridisulfosaui-es -Natrium werden in 200 cm' Wasser gelöst und eine wässerige Suspension von Zinnhydroxy dul zu gegeben, die man aus einer Lösung von 14 gr Zinnsalz in Wasser d urch Ausfällen mit Am moniak, Auswaschen und Anrühren mit Wasser hergestellt hat. Es tritt Lösung ein. Man neutralisiert mit .verdünnter Natronlauge, fil triert und dampft das Filtrat im Vakuum ein. Das Zinnkomplexsalz bleibt als ein leicht gefärbtes Pulver zurück, das sich leicht-in Wasser ' löst.
Die Darstellung und Aufbewah- rung muss unter möglichstem Ausschluss voll Luft geschehen, da das Präparat langsam Sauerstoff aufnimmt. Es dient als Mittel gegen Infektionskrankheiten.
Process for the preparation of a soluble tin compound. The main patent describes a process by which a complex connection of antimony with pyrogallol disulfo acid is obtained. Compounds of this kind differ entirely from ordinary salts of antimony in that they do not have a number of alloys of these salts. They contain the antimony in a more solid so-called complex compound.
These substances can be used as remedies, because in them, due to the stronger bond of the antimony, the harmful effect is suppressed compared to the healing effect.
It has been found that the same conditions prevail if catechol-disilfosaui-es sodium is reacted with zirine hydroxide.
The method is best carried out in such a way that sodium pyrocatechol disulphonate is reacted with the required iSTerge of the tin compound in an aqueous solution, if necessary with heating.
<I> Example: </I> 35 grams of brerizkatecliiridisulfosaui-es sodium are dissolved in 200 cm of water and an aqueous suspension of tin hydroxide is added, which is obtained from a solution of 14 grams of tin salt in water by precipitation with ammonia , Washing out and mixing with water. Solution occurs. It is neutralized with dilute sodium hydroxide solution, filtered and the filtrate is evaporated in vacuo. The tin complex salt remains as a lightly colored powder that dissolves easily in water.
The presentation and storage must be carried out with the greatest possible exclusion of air, since the preparation slowly absorbs oxygen. It is used as a remedy for infectious diseases.
Claims (1)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH125389T | 1926-01-29 | ||
| CH125392T | 1926-01-29 | ||
| CH123233T | 1926-01-29 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH125389A true CH125389A (en) | 1928-04-16 |
Family
ID=27176813
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH125389D CH125389A (en) | 1926-01-29 | 1926-01-29 | Process for the preparation of a soluble tin compound. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH125389A (en) |
-
1926
- 1926-01-29 CH CH125389D patent/CH125389A/en unknown
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