CA2932704C - Methods of microbiological control in beet sugar and other sugar-containing plant material processing - Google Patents
Methods of microbiological control in beet sugar and other sugar-containing plant material processing Download PDFInfo
- Publication number
- CA2932704C CA2932704C CA2932704A CA2932704A CA2932704C CA 2932704 C CA2932704 C CA 2932704C CA 2932704 A CA2932704 A CA 2932704A CA 2932704 A CA2932704 A CA 2932704A CA 2932704 C CA2932704 C CA 2932704C
- Authority
- CA
- Canada
- Prior art keywords
- sugar
- monochloramine
- juice
- raw material
- beet
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 235000000346 sugar Nutrition 0.000 title claims abstract description 188
- 238000000034 method Methods 0.000 title claims abstract description 114
- 241000196324 Embryophyta Species 0.000 title claims abstract description 73
- 239000000463 material Substances 0.000 title claims abstract description 58
- 230000002906 microbiologic effect Effects 0.000 title claims abstract description 27
- CZMRCDWAGMRECN-UHFFFAOYSA-N Rohrzucker Natural products OCC1OC(CO)(OC2OC(CO)C(O)C(O)C2O)C(O)C1O CZMRCDWAGMRECN-UHFFFAOYSA-N 0.000 title claims description 24
- QDHHCQZDFGDHMP-UHFFFAOYSA-N Chloramine Chemical compound ClN QDHHCQZDFGDHMP-UHFFFAOYSA-N 0.000 claims abstract description 142
- 239000002994 raw material Substances 0.000 claims abstract description 39
- 241000219310 Beta vulgaris subsp. vulgaris Species 0.000 claims abstract description 29
- 235000021536 Sugar beet Nutrition 0.000 claims abstract description 29
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 52
- 238000004519 manufacturing process Methods 0.000 claims description 44
- 238000011282 treatment Methods 0.000 claims description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 35
- 239000013078 crystal Substances 0.000 claims description 18
- 241000335053 Beta vulgaris Species 0.000 claims description 17
- 239000006188 syrup Substances 0.000 claims description 16
- 235000016068 Berberis vulgaris Nutrition 0.000 claims description 15
- 244000005700 microbiome Species 0.000 claims description 15
- 235000013379 molasses Nutrition 0.000 claims description 15
- 235000020357 syrup Nutrition 0.000 claims description 14
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 12
- 239000005708 Sodium hypochlorite Substances 0.000 claims description 10
- 235000013399 edible fruits Nutrition 0.000 claims description 10
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 claims description 10
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- 229910021529 ammonia Inorganic materials 0.000 claims description 6
- 150000003863 ammonium salts Chemical class 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 6
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- 244000017714 Prunus persica var. nucipersica Species 0.000 claims description 3
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- 235000019693 cherries Nutrition 0.000 claims description 3
- 244000144730 Amygdalus persica Species 0.000 claims 1
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- 235000015103 Malus silvestris Nutrition 0.000 claims 1
- 240000008790 Musa x paradisiaca Species 0.000 claims 1
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- 235000014443 Pyrus communis Nutrition 0.000 claims 1
- 240000001987 Pyrus communis Species 0.000 claims 1
- 235000009754 Vitis X bourquina Nutrition 0.000 claims 1
- 235000012333 Vitis X labruscana Nutrition 0.000 claims 1
- 240000006365 Vitis vinifera Species 0.000 claims 1
- 235000014787 Vitis vinifera Nutrition 0.000 claims 1
- 229930006000 Sucrose Natural products 0.000 abstract description 30
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 abstract description 30
- 230000001580 bacterial effect Effects 0.000 abstract description 11
- 230000002411 adverse Effects 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 4
- 239000000047 product Substances 0.000 description 25
- 229960004793 sucrose Drugs 0.000 description 23
- 239000005720 sucrose Substances 0.000 description 22
- 238000006243 chemical reaction Methods 0.000 description 19
- 239000007788 liquid Substances 0.000 description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 14
- 241000894006 Bacteria Species 0.000 description 13
- 239000000376 reactant Substances 0.000 description 13
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 11
- 239000002609 medium Substances 0.000 description 11
- WQYVRQLZKVEZGA-UHFFFAOYSA-N hypochlorite Chemical compound Cl[O-] WQYVRQLZKVEZGA-UHFFFAOYSA-N 0.000 description 10
- 150000008163 sugars Chemical class 0.000 description 9
- 238000003860 storage Methods 0.000 description 8
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 7
- 238000000855 fermentation Methods 0.000 description 7
- 230000004151 fermentation Effects 0.000 description 7
- 239000012530 fluid Substances 0.000 description 7
- 235000015203 fruit juice Nutrition 0.000 description 7
- 239000012535 impurity Substances 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 6
- 229930091371 Fructose Natural products 0.000 description 6
- 239000005715 Fructose Substances 0.000 description 6
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 6
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 6
- 235000011114 ammonium hydroxide Nutrition 0.000 description 6
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 6
- 239000008103 glucose Substances 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 5
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- 244000205124 Acer nigrum Species 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 4
- 239000000920 calcium hydroxide Substances 0.000 description 4
- 235000011116 calcium hydroxide Nutrition 0.000 description 4
- 239000007795 chemical reaction product Substances 0.000 description 4
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- 239000000460 chlorine Substances 0.000 description 4
- 229910052801 chlorine Inorganic materials 0.000 description 4
- 230000009969 flowable effect Effects 0.000 description 4
- 229930182830 galactose Natural products 0.000 description 4
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 4
- 241000894007 species Species 0.000 description 4
- 230000000699 topical effect Effects 0.000 description 4
- 235000010328 Acer nigrum Nutrition 0.000 description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 3
- 241000233866 Fungi Species 0.000 description 3
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 3
- 235000011941 Tilia x europaea Nutrition 0.000 description 3
- WQZGKKKJIJFFOK-PHYPRBDBSA-N alpha-D-galactose Chemical compound OC[C@H]1O[C@H](O)[C@H](O)[C@@H](O)[C@H]1O WQZGKKKJIJFFOK-PHYPRBDBSA-N 0.000 description 3
- -1 at least 50.1% Chemical compound 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- JSYGRUBHOCKMGQ-UHFFFAOYSA-N dichloramine Chemical compound ClNCl JSYGRUBHOCKMGQ-UHFFFAOYSA-N 0.000 description 3
- 238000010790 dilution Methods 0.000 description 3
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- 239000004571 lime Substances 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 238000003809 water extraction Methods 0.000 description 3
- 235000010319 Acer grandidentatum Nutrition 0.000 description 2
- 235000002629 Acer saccharinum Nutrition 0.000 description 2
- 235000010157 Acer saccharum subsp saccharum Nutrition 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
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- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 description 2
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- 244000138286 Sorghum saccharatum Species 0.000 description 2
- 241000219094 Vitaceae Species 0.000 description 2
- 235000021016 apples Nutrition 0.000 description 2
- 239000012736 aqueous medium Substances 0.000 description 2
- 235000021015 bananas Nutrition 0.000 description 2
- 235000015191 beet juice Nutrition 0.000 description 2
- 235000012206 bottled water Nutrition 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 238000013375 chromatographic separation Methods 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 125000004122 cyclic group Chemical group 0.000 description 2
- 238000004042 decolorization Methods 0.000 description 2
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- 239000003651 drinking water Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 235000021021 grapes Nutrition 0.000 description 2
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- 239000002245 particle Substances 0.000 description 2
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- 238000005507 spraying Methods 0.000 description 2
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- 235000012069 sugar maple Nutrition 0.000 description 2
- AOSFMYBATFLTAQ-UHFFFAOYSA-N 1-amino-3-(benzimidazol-1-yl)propan-2-ol Chemical compound C1=CC=C2N(CC(O)CN)C=NC2=C1 AOSFMYBATFLTAQ-UHFFFAOYSA-N 0.000 description 1
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- 241000193830 Bacillus <bacterium> Species 0.000 description 1
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- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- ZKQDCIXGCQPQNV-UHFFFAOYSA-N Calcium hypochlorite Chemical compound [Ca+2].Cl[O-].Cl[O-] ZKQDCIXGCQPQNV-UHFFFAOYSA-N 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 1
- 206010061217 Infestation Diseases 0.000 description 1
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- 241000746444 Saccharum sp. Species 0.000 description 1
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- 150000007513 acids Chemical class 0.000 description 1
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- SWLVFNYSXGMGBS-UHFFFAOYSA-N ammonium bromide Chemical compound [NH4+].[Br-] SWLVFNYSXGMGBS-UHFFFAOYSA-N 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 239000000908 ammonium hydroxide Substances 0.000 description 1
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- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
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- 239000012990 dithiocarbamate Substances 0.000 description 1
- 150000004659 dithiocarbamates Chemical class 0.000 description 1
- 238000010981 drying operation Methods 0.000 description 1
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- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 229960004903 invert sugar Drugs 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
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- 229920003303 ion-exchange polymer Polymers 0.000 description 1
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- 230000000813 microbial effect Effects 0.000 description 1
- 238000011169 microbiological contamination Methods 0.000 description 1
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- 235000010755 mineral Nutrition 0.000 description 1
- 150000002772 monosaccharides Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- QEHKBHWEUPXBCW-UHFFFAOYSA-N nitrogen trichloride Chemical compound ClN(Cl)Cl QEHKBHWEUPXBCW-UHFFFAOYSA-N 0.000 description 1
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- 239000007800 oxidant agent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
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- 238000004321 preservation Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
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- 239000002689 soil Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B10/00—Production of sugar juices
- C13B10/08—Extraction of sugar from sugar beet with water
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B10/00—Production of sugar juices
- C13B10/08—Extraction of sugar from sugar beet with water
- C13B10/083—Treatment of sugar beet before extraction
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B10/00—Production of sugar juices
- C13B10/006—Conservation of sugar juices
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B10/00—Production of sugar juices
- C13B10/02—Expressing juice from sugar cane or similar material, e.g. sorghum saccharatum
- C13B10/025—Treatment of sugar cane before extraction
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B50/00—Sugar products, e.g. powdered, lump or liquid sugar; Working-up of sugar
- C13B50/002—Addition of chemicals or other foodstuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Micro-Organisms Or Cultivation Processes Thereof (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201361912037P | 2013-12-05 | 2013-12-05 | |
| US61/912,037 | 2013-12-05 | ||
| PCT/US2014/068095 WO2015084807A1 (en) | 2013-12-05 | 2014-12-02 | Methods of microbiological control in beet sugar and other sugar-containing plant material processing |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2932704A1 CA2932704A1 (en) | 2015-06-11 |
| CA2932704C true CA2932704C (en) | 2022-06-28 |
Family
ID=52232428
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2932704A Active CA2932704C (en) | 2013-12-05 | 2014-12-02 | Methods of microbiological control in beet sugar and other sugar-containing plant material processing |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US9551043B2 (enExample) |
| EP (1) | EP3076787B1 (enExample) |
| JP (2) | JP6684711B2 (enExample) |
| CN (1) | CN105979777B (enExample) |
| AU (1) | AU2014357353B2 (enExample) |
| BR (1) | BR112016012621B1 (enExample) |
| CA (1) | CA2932704C (enExample) |
| ES (1) | ES2667263T3 (enExample) |
| MX (1) | MX384048B (enExample) |
| NZ (1) | NZ720482A (enExample) |
| PT (1) | PT3076787T (enExample) |
| WO (1) | WO2015084807A1 (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2014357353B2 (en) * | 2013-12-05 | 2017-11-09 | Buckman Laboratories International, Inc. | Methods of microbiological control in beet sugar and other sugar-containing plant material processing |
| EP3392352B1 (en) * | 2017-04-21 | 2020-11-25 | Co.Pro.B. Soc. Coop. Agricola | Process for preparing raw sugar from sugar beet |
| MX2020008270A (es) * | 2018-02-07 | 2020-09-21 | Buckman Laboratories Int Inc | Combinaciones sinergicas de monocloramina y compuesto de peroxido, y metodos de uso de las mismas para control microbiano. |
| EP3628738A1 (en) * | 2018-09-25 | 2020-04-01 | KWS SAAT SE & Co. KGaA | Method for controlling weed beets and other weeds |
| EP3884072A4 (en) * | 2018-11-21 | 2022-08-17 | Buckman Laboratories International, Inc. | EFFECTIVE FOAM CONTROL IN BEET WASHING PROCESS WATER BY AUTOMATIC APPLICATION OF A DEFOAMING AGENT |
| WO2021055941A1 (en) * | 2019-09-20 | 2021-03-25 | Chemtreat, Inc. | Sanitary food washing stage in food production |
| EP4096424A1 (en) * | 2020-01-28 | 2022-12-07 | Buckman Laboratories International, Inc. | Methods of extracting starch or protein from agricultural products |
| US20230112660A1 (en) * | 2020-02-26 | 2023-04-13 | Lodaat, Llc | Sweetener and manufacturing process therefor |
| US20230270108A1 (en) * | 2020-07-31 | 2023-08-31 | Hydrite Chemical Co. | Method for Controlling Microbial Growth in Sugar Processing |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2059110A (en) | 1935-03-06 | 1936-10-27 | Pennsylvania Salt Mfg Co | Process for making high grade saccharine products and refining raw sugars |
| US4038372A (en) | 1976-05-05 | 1977-07-26 | The United States Of America As Represented By The Secretary Of The Navy | Process for manufacturing chloramine |
| US4789539A (en) | 1982-04-22 | 1988-12-06 | Hans Osborg | Process for the preparation of chloramine |
| FR2769016B1 (fr) | 1997-09-30 | 1999-10-29 | Adir | Procede de synthese de chloramine haute teneur |
| US6656287B2 (en) * | 2002-04-15 | 2003-12-02 | Co2 Solutions, Llc | System to produce sugar from plant materials |
| FR2846646B1 (fr) * | 2002-11-04 | 2005-01-21 | Isochem Sa | Procede de synthese de la monochloramine |
| JP2006506312A (ja) | 2002-11-14 | 2006-02-23 | ブリストル−マイヤーズ スクイブ カンパニー | ガス状クロラミンの製造 |
| US20100136132A1 (en) * | 2004-01-27 | 2010-06-03 | Van Der Krieken Wilhelmus Maria | Lignosulfonate compositions for control of plant pathogens |
| US20070123423A1 (en) * | 2005-11-30 | 2007-05-31 | Cheng Huai N | Solid biocidal compositions and methods of using the same |
| US7306679B1 (en) * | 2006-06-02 | 2007-12-11 | Solae, Llc | Composition and sugar refining process |
| US20080160104A1 (en) * | 2006-12-28 | 2008-07-03 | Manian Ramesh | Antimicrobial composition |
| US7935189B2 (en) | 2007-06-21 | 2011-05-03 | Cantine Foraci S.R.L. | Process and plant for producing sugar products from grapes |
| AU2010228843B2 (en) * | 2009-03-26 | 2014-08-28 | Umesh Venkatesh Kulkarni | Method for producing clarified juice, packagible juice, ethanol and sugar from sugarcane and system thereof |
| EP2603613B1 (en) * | 2010-08-13 | 2015-04-08 | RDM Empreendimentos e Participaçöes S.A. | Method and composition for reducing the color of sugar |
| JP5800618B2 (ja) * | 2011-07-22 | 2015-10-28 | 伯東株式会社 | スライム剥離方法 |
| EP3556934B1 (en) | 2012-06-05 | 2025-08-06 | Buckman Laboratories International, Inc. | Methods of controlling calcium precipitation and/or scaling |
| KR20150110554A (ko) * | 2013-01-25 | 2015-10-02 | 케미라 오와이제이 | 살생물제 조성물 및 수처리 방법 |
| AU2014357353B2 (en) * | 2013-12-05 | 2017-11-09 | Buckman Laboratories International, Inc. | Methods of microbiological control in beet sugar and other sugar-containing plant material processing |
-
2014
- 2014-12-02 AU AU2014357353A patent/AU2014357353B2/en not_active Ceased
- 2014-12-02 US US14/557,886 patent/US9551043B2/en not_active Expired - Fee Related
- 2014-12-02 ES ES14820998.4T patent/ES2667263T3/es active Active
- 2014-12-02 WO PCT/US2014/068095 patent/WO2015084807A1/en not_active Ceased
- 2014-12-02 BR BR112016012621-1A patent/BR112016012621B1/pt active IP Right Grant
- 2014-12-02 JP JP2016536590A patent/JP6684711B2/ja not_active Expired - Fee Related
- 2014-12-02 NZ NZ720482A patent/NZ720482A/en not_active IP Right Cessation
- 2014-12-02 CA CA2932704A patent/CA2932704C/en active Active
- 2014-12-02 CN CN201480074926.3A patent/CN105979777B/zh not_active Expired - Fee Related
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| US20150159230A1 (en) | 2015-06-11 |
| EP3076787B1 (en) | 2018-04-04 |
| CN105979777A (zh) | 2016-09-28 |
| WO2015084807A1 (en) | 2015-06-11 |
| BR112016012621B1 (pt) | 2021-04-13 |
| JP6684711B2 (ja) | 2020-04-22 |
| MX2016006768A (es) | 2016-10-26 |
| JP2020072657A (ja) | 2020-05-14 |
| EP3076787A1 (en) | 2016-10-12 |
| ES2667263T3 (es) | 2018-05-10 |
| JP2016540768A (ja) | 2016-12-28 |
| US9551043B2 (en) | 2017-01-24 |
| CN105979777B (zh) | 2019-01-04 |
| NZ720482A (en) | 2020-06-26 |
| CA2932704A1 (en) | 2015-06-11 |
| AU2014357353B2 (en) | 2017-11-09 |
| MX384048B (es) | 2025-03-14 |
| AU2014357353A1 (en) | 2016-06-23 |
| PT3076787T (pt) | 2018-05-14 |
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