CA2887339A1 - Solutions and methods of making solutions to kill or deactivate spores, microorganisms, bacteria and fungus - Google Patents
Solutions and methods of making solutions to kill or deactivate spores, microorganisms, bacteria and fungus Download PDFInfo
- Publication number
- CA2887339A1 CA2887339A1 CA 2887339 CA2887339A CA2887339A1 CA 2887339 A1 CA2887339 A1 CA 2887339A1 CA 2887339 CA2887339 CA 2887339 CA 2887339 A CA2887339 A CA 2887339A CA 2887339 A1 CA2887339 A1 CA 2887339A1
- Authority
- CA
- Canada
- Prior art keywords
- solution
- water
- plasma
- acetic acid
- activated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 238000000034 method Methods 0.000 title claims abstract description 33
- 241000894006 Bacteria Species 0.000 title claims description 34
- 241000233866 Fungi Species 0.000 title claims description 22
- 244000005700 microbiome Species 0.000 title claims description 20
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 214
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 137
- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 claims abstract description 84
- 238000002156 mixing Methods 0.000 claims abstract description 15
- 125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 claims abstract description 13
- PQLVXDKIJBQVDF-UHFFFAOYSA-N acetic acid;hydrate Chemical class O.CC(O)=O PQLVXDKIJBQVDF-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000012530 fluid Substances 0.000 claims description 40
- 239000007789 gas Substances 0.000 claims description 26
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 8
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 6
- 241000700605 Viruses Species 0.000 claims description 6
- 230000003213 activating effect Effects 0.000 claims description 5
- 229910052757 nitrogen Inorganic materials 0.000 claims description 3
- 241000894007 species Species 0.000 claims description 3
- 229960001138 acetylsalicylic acid Drugs 0.000 claims description 2
- 239000004094 surface-active agent Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 4
- 125000005273 2-acetoxybenzoic acid group Chemical group 0.000 claims 1
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 claims 1
- 210000002381 plasma Anatomy 0.000 description 100
- 239000000243 solution Substances 0.000 description 93
- 241000588724 Escherichia coli Species 0.000 description 22
- 238000001994 activation Methods 0.000 description 21
- 230000004913 activation Effects 0.000 description 19
- 230000009467 reduction Effects 0.000 description 16
- 239000008399 tap water Substances 0.000 description 12
- 235000020679 tap water Nutrition 0.000 description 12
- 239000000654 additive Substances 0.000 description 7
- 230000008901 benefit Effects 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 239000003570 air Substances 0.000 description 5
- 238000002474 experimental method Methods 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 230000004888 barrier function Effects 0.000 description 4
- 238000006731 degradation reaction Methods 0.000 description 4
- 239000003595 mist Substances 0.000 description 4
- 150000003254 radicals Chemical class 0.000 description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- 230000001332 colony forming effect Effects 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- -1 superoxide anions Chemical class 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000015556 catabolic process Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000003574 free electron Substances 0.000 description 2
- 230000000415 inactivating effect Effects 0.000 description 2
- 230000002779 inactivation Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000007800 oxidant agent Substances 0.000 description 2
- 238000009832 plasma treatment Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- BSYNRYMUTXBXSQ-UHFFFAOYSA-N Aspirin Chemical compound CC(=O)OC1=CC=CC=C1C(O)=O BSYNRYMUTXBXSQ-UHFFFAOYSA-N 0.000 description 1
- 241000193163 Clostridioides difficile Species 0.000 description 1
- 108091006629 SLC13A2 Proteins 0.000 description 1
- 206010052428 Wound Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 229910021536 Zeolite Inorganic materials 0.000 description 1
- 239000012080 ambient air Substances 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000012431 aqueous reaction media Substances 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 239000007844 bleaching agent Substances 0.000 description 1
- 235000012206 bottled water Nutrition 0.000 description 1
- 239000000872 buffer Substances 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 239000000645 desinfectant Substances 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 239000003897 fog Substances 0.000 description 1
- 235000021022 fresh fruits Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000011534 incubation Methods 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 229910052816 inorganic phosphate Inorganic materials 0.000 description 1
- 229910052920 inorganic sulfate Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000006193 liquid solution Substances 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 150000002826 nitrites Chemical class 0.000 description 1
- 235000019645 odor Nutrition 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 239000002504 physiological saline solution Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000000135 prohibitive effect Effects 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 238000011012 sanitization Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000003330 sporicidal effect Effects 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000012956 testing procedure Methods 0.000 description 1
- 239000006150 trypticase soy agar Substances 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group; Thio analogues thereof
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
- Water Treatment By Electricity Or Magnetism (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261710263P | 2012-10-05 | 2012-10-05 | |
| US61/710,263 | 2012-10-05 | ||
| US13/842,574 US20140100277A1 (en) | 2012-10-05 | 2013-03-15 | Solutions and methods of making solutions to kill or deactivate spores, microorganisms, bacteria and fungus |
| US13/842,574 | 2013-03-15 | ||
| PCT/US2013/063360 WO2014055812A1 (en) | 2012-10-05 | 2013-10-04 | Solutions and methods of making solutions to kill or deactivate spores, microorganisms, bacteria and fungus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2887339A1 true CA2887339A1 (en) | 2014-04-10 |
Family
ID=50433175
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA 2887339 Abandoned CA2887339A1 (en) | 2012-10-05 | 2013-10-04 | Solutions and methods of making solutions to kill or deactivate spores, microorganisms, bacteria and fungus |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US20140100277A1 (en:Method) |
| EP (1) | EP2903443A1 (en:Method) |
| JP (1) | JP2015533828A (en:Method) |
| KR (1) | KR20150079673A (en:Method) |
| CN (1) | CN104837349A (en:Method) |
| AU (1) | AU2013327002A1 (en:Method) |
| BR (1) | BR112015007537A2 (en:Method) |
| CA (1) | CA2887339A1 (en:Method) |
| IN (1) | IN2015DN03167A (en:Method) |
| MX (1) | MX2015004342A (en:Method) |
| WO (1) | WO2014055812A1 (en:Method) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20140271354A1 (en) * | 2013-03-15 | 2014-09-18 | EP Technologies LLC | Methods and solutions for killing or deactivating bacteria |
| WO2015200907A1 (en) * | 2014-06-27 | 2015-12-30 | EP Technologies LLC | Treated sprout plants with decreased bacterial viability and methods and apparatuses for making the same |
| US20160015038A1 (en) * | 2014-07-16 | 2016-01-21 | EP Technologies LLC | Treated crop plants or plant food products with decreased bacterial viability and methods and apparatuses for making the same |
| JP6840326B2 (ja) * | 2015-02-18 | 2021-03-10 | 国立大学法人東海国立大学機構 | プラズマ殺菌水溶液とその製造方法および殺菌方法 |
| CN106241965A (zh) * | 2015-06-09 | 2016-12-21 | 松下知识产权经营株式会社 | 液体处理方法、对象物处理方法、液体处理装置、对象物处理装置及等离子体处理液 |
| WO2017019722A1 (en) | 2015-07-28 | 2017-02-02 | EP Technologies LLC | Scrubbing device for cleaning, sanitizing or disinfecting |
| WO2017040463A1 (en) | 2015-08-31 | 2017-03-09 | EP Technologies LLC | Methods of and system for generating antimicrobial wipes |
| EP3146983B1 (en) * | 2015-09-22 | 2020-11-18 | Leibniz-Institut für Plasmaforschung und Technologie e.V. | Combination method for cleaning, decontamination, disinfection and sterilization of objects |
| WO2017063817A1 (en) | 2015-10-13 | 2017-04-20 | Unilever N.V. | Method and kit for sanitising surfaces |
| EP3379929A1 (en) | 2015-11-23 | 2018-10-03 | GOJO Industries, Inc. | Methods and solutions including additives and stabilizers for killing or deactivating spores |
| CN106244584B (zh) * | 2016-09-27 | 2019-07-19 | 北京大学 | 一种快速提取细菌基因组dna的方法 |
| WO2018089577A1 (en) | 2016-11-10 | 2018-05-17 | EP Technologies LLC | Methods and systems for generating plasma activated liquid |
| DE102016123703A1 (de) * | 2016-12-07 | 2018-06-07 | Krömker Holding GmbH | Verfahren zur Desinfektion und Einrichtung zur Desinfektion von Oberflächen |
| EP3338562A1 (en) * | 2016-12-20 | 2018-06-27 | Linde Aktiengesellschaft | Process and apparatus for decontamination of food articles |
| RU2020117847A (ru) | 2017-11-07 | 2021-12-08 | Геа Фуд Сольюшнс Бакел Б.В. | Оборудование для обработки пищевых продуктов, очищаемое плазменно-активированной водой |
| US11844811B2 (en) * | 2018-05-20 | 2023-12-19 | Myfitstrip Llc | Methods and compositions for alleviating respiratory dysfunction |
| EP3895738A1 (de) | 2020-04-16 | 2021-10-20 | Erbe Elektromedizin GmbH | Einrichtung und verfahren zur plasmaaktivierung einer flüssigkeit |
| EP3904492A1 (en) * | 2020-04-29 | 2021-11-03 | Nofima AS | Method and system of pre-treating biomass, in particular biomass that is resistant to cell disruption, for improving the accessibility of cellular compounds therefrom |
| CN111511088A (zh) * | 2020-04-29 | 2020-08-07 | 西安交通大学 | 一种制备碱性等离子体活化液的制备方法、装置及用途 |
| JP7380432B2 (ja) * | 2020-06-02 | 2023-11-15 | 株式会社ニコン | ミスト発生装置、薄膜製造装置、及び薄膜製造方法 |
| ES2928251B2 (es) * | 2021-05-13 | 2025-05-22 | Consejo Superior Investigacion | Medios activados con plasma para uso en el tratamiento de enfermedades respiratorias |
| CN114271320B (zh) * | 2021-12-30 | 2023-05-12 | 浙江大学中原研究院 | 一种杨梅采后保鲜的减药处理方法 |
| CN114988554B (zh) * | 2022-06-16 | 2023-11-24 | 东华大学 | 一种利用介质阻挡放电活化过氧乙酸去除水中有机污染物的方法 |
| WO2024130722A1 (zh) * | 2022-12-23 | 2024-06-27 | 江南大学 | 一种等离子体活化水协同酒石酸处理鲜切果蔬保鲜的方法 |
| NL2035401B1 (en) * | 2023-07-17 | 2025-01-28 | Vitalfluid B V | Fertilisation and disinfection system using plasma activated water |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2378601A1 (en) * | 1999-08-05 | 2001-02-15 | Steris Inc. | Electrolytic synthesis of peracetic acid |
| US7291314B2 (en) | 2001-12-20 | 2007-11-06 | Hydro Enterprises, Inc. | Activated water apparatus and methods |
| AU2002243660A1 (en) | 2001-01-25 | 2002-08-06 | Water Works Global, Inc. | Method of activation of chemically pure and potable water |
| US8110538B2 (en) * | 2005-01-11 | 2012-02-07 | Biomed Protect, Llc | Peracid/peroxide composition and use thereof as an anti-microbial and a photosensitizer |
| EP1942951B1 (en) | 2005-10-25 | 2012-12-12 | Aseptix Technologies B.V | Method for the preparation of biocidal activated water solutions |
| CN101156955B (zh) * | 2007-11-21 | 2010-05-19 | 中山大学 | 非平衡等离子体式喷雾杀菌消毒剂发生装置 |
| JP2010187648A (ja) * | 2009-02-20 | 2010-09-02 | Gunma Univ | 空気プラズマを用いた殺菌方法 |
| WO2012018891A2 (en) | 2010-08-03 | 2012-02-09 | Drexel University | Materials for disinfection produced by non-thermal plasma |
-
2013
- 2013-03-15 US US13/842,574 patent/US20140100277A1/en not_active Abandoned
- 2013-10-04 WO PCT/US2013/063360 patent/WO2014055812A1/en not_active Ceased
- 2013-10-04 IN IN3167DEN2015 patent/IN2015DN03167A/en unknown
- 2013-10-04 AU AU2013327002A patent/AU2013327002A1/en not_active Abandoned
- 2013-10-04 CN CN201380062920.XA patent/CN104837349A/zh active Pending
- 2013-10-04 BR BR112015007537A patent/BR112015007537A2/pt not_active IP Right Cessation
- 2013-10-04 EP EP13779679.3A patent/EP2903443A1/en not_active Withdrawn
- 2013-10-04 KR KR1020157011561A patent/KR20150079673A/ko not_active Withdrawn
- 2013-10-04 MX MX2015004342A patent/MX2015004342A/es unknown
- 2013-10-04 JP JP2015535797A patent/JP2015533828A/ja active Pending
- 2013-10-04 CA CA 2887339 patent/CA2887339A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| EP2903443A1 (en) | 2015-08-12 |
| JP2015533828A (ja) | 2015-11-26 |
| BR112015007537A2 (pt) | 2017-07-04 |
| KR20150079673A (ko) | 2015-07-08 |
| CN104837349A (zh) | 2015-08-12 |
| IN2015DN03167A (en:Method) | 2015-10-02 |
| AU2013327002A1 (en) | 2015-05-14 |
| WO2014055812A1 (en) | 2014-04-10 |
| MX2015004342A (es) | 2015-10-29 |
| US20140100277A1 (en) | 2014-04-10 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Discontinued |
Effective date: 20171004 |