CA2823217C - Sterilisation de contenants d'aliments et de boissons par vapeur d'acide peracetique - Google Patents
Sterilisation de contenants d'aliments et de boissons par vapeur d'acide peracetique Download PDFInfo
- Publication number
- CA2823217C CA2823217C CA2823217A CA2823217A CA2823217C CA 2823217 C CA2823217 C CA 2823217C CA 2823217 A CA2823217 A CA 2823217A CA 2823217 A CA2823217 A CA 2823217A CA 2823217 C CA2823217 C CA 2823217C
- Authority
- CA
- Canada
- Prior art keywords
- ppm
- paa
- bottles
- peracetic acid
- vapor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 title claims abstract description 185
- 230000001954 sterilising effect Effects 0.000 title claims abstract description 21
- 238000004659 sterilization and disinfection Methods 0.000 title abstract description 12
- 235000013361 beverage Nutrition 0.000 title description 6
- 235000013305 food Nutrition 0.000 title description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 48
- 238000000034 method Methods 0.000 claims abstract description 31
- 229920000139 polyethylene terephthalate Polymers 0.000 claims abstract description 21
- -1 polyethylene terephthalate Polymers 0.000 claims abstract description 4
- 239000003999 initiator Substances 0.000 claims abstract description 3
- 239000005020 polyethylene terephthalate Substances 0.000 claims abstract description 3
- 239000004033 plastic Substances 0.000 claims description 11
- 229920003023 plastic Polymers 0.000 claims description 11
- 239000012808 vapor phase Substances 0.000 claims description 11
- 239000007789 gas Substances 0.000 claims description 10
- 238000011282 treatment Methods 0.000 claims description 10
- 229920006395 saturated elastomer Polymers 0.000 claims description 4
- 238000012360 testing method Methods 0.000 description 45
- 239000000243 solution Substances 0.000 description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 13
- 239000002054 inoculum Substances 0.000 description 12
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
- 238000010790 dilution Methods 0.000 description 9
- 239000012895 dilution Substances 0.000 description 9
- 238000002360 preparation method Methods 0.000 description 9
- 239000008367 deionised water Substances 0.000 description 8
- 229910021641 deionized water Inorganic materials 0.000 description 8
- 230000008016 vaporization Effects 0.000 description 7
- 235000014469 Bacillus subtilis Nutrition 0.000 description 6
- 241000894006 Bacteria Species 0.000 description 6
- 230000003472 neutralizing effect Effects 0.000 description 6
- 229910001220 stainless steel Inorganic materials 0.000 description 6
- 239000010935 stainless steel Substances 0.000 description 6
- 239000000725 suspension Substances 0.000 description 6
- 239000011521 glass Substances 0.000 description 5
- 239000006200 vaporizer Substances 0.000 description 5
- 239000012190 activator Substances 0.000 description 4
- 239000000356 contaminant Substances 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000004448 titration Methods 0.000 description 4
- 241000193410 Bacillus atrophaeus Species 0.000 description 3
- 230000003115 biocidal effect Effects 0.000 description 3
- 239000003139 biocide Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 description 3
- 235000019345 sodium thiosulphate Nutrition 0.000 description 3
- 238000010998 test method Methods 0.000 description 3
- 238000009834 vaporization Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 241000193830 Bacillus <bacterium> Species 0.000 description 2
- 241001457800 Bacillus atrophaeus ATCC 9372 Species 0.000 description 2
- 241000193155 Clostridium botulinum Species 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000004364 calculation method Methods 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- WJJMNDUMQPNECX-UHFFFAOYSA-N dipicolinic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=N1 WJJMNDUMQPNECX-UHFFFAOYSA-N 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000011534 incubation Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000007747 plating Methods 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 239000003206 sterilizing agent Substances 0.000 description 2
- JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 description 1
- 238000012371 Aseptic Filling Methods 0.000 description 1
- 244000063299 Bacillus subtilis Species 0.000 description 1
- 241000193388 Bacillus thuringiensis Species 0.000 description 1
- 241000589876 Campylobacter Species 0.000 description 1
- 241000222120 Candida <Saccharomycetales> Species 0.000 description 1
- 102000016938 Catalase Human genes 0.000 description 1
- 108010053835 Catalase Proteins 0.000 description 1
- 241000194033 Enterococcus Species 0.000 description 1
- DBVJJBKOTRCVKF-UHFFFAOYSA-N Etidronic acid Chemical compound OP(=O)(O)C(O)(C)P(O)(O)=O DBVJJBKOTRCVKF-UHFFFAOYSA-N 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 241000235395 Mucor Species 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 241000589516 Pseudomonas Species 0.000 description 1
- 241000235527 Rhizopus Species 0.000 description 1
- 241000607142 Salmonella Species 0.000 description 1
- 238000003302 UV-light treatment Methods 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 239000003377 acid catalyst Substances 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 239000013011 aqueous formulation Substances 0.000 description 1
- 238000000071 blow moulding Methods 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000012790 confirmation Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- KEUKAQNPUBYCIC-UHFFFAOYSA-N ethaneperoxoic acid;hydrogen peroxide Chemical compound OO.CC(=O)OO KEUKAQNPUBYCIC-UHFFFAOYSA-N 0.000 description 1
- 150000002194 fatty esters Chemical class 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 230000009477 glass transition Effects 0.000 description 1
- 230000036512 infertility Effects 0.000 description 1
- 206010022000 influenza Diseases 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229910052756 noble gas Inorganic materials 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 150000004965 peroxy acids Chemical class 0.000 description 1
- 150000003009 phosphonic acids Chemical class 0.000 description 1
- 235000011007 phosphoric acid Nutrition 0.000 description 1
- 150000003016 phosphoric acids Chemical class 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- VLYWMPOKSSWJAL-UHFFFAOYSA-N sulfamethoxypyridazine Chemical compound N1=NC(OC)=CC=C1NS(=O)(=O)C1=CC=C(N)C=C1 VLYWMPOKSSWJAL-UHFFFAOYSA-N 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000012085 test solution Substances 0.000 description 1
- 238000010200 validation analysis Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
- A61L2/20—Gaseous substances, e.g. vapours
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2202/00—Aspects relating to methods or apparatus for disinfecting or sterilising materials or objects
- A61L2202/20—Targets to be treated
- A61L2202/23—Containers, e.g. vials, bottles, syringes, mail
Landscapes
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
- Food Preservation Except Freezing, Refrigeration, And Drying (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments Of Macromolecular Shaped Articles (AREA)
Abstract
La présente invention concerne un procédé de stérilisation d'une surface qui consiste à traiter une telle surface par une vapeur comportant de l'acide peracétique à une concentration d'au moins environ 3 500 ppm à une température entre environ 57° et environ 75°C. Un tel procédé, qui est de préférence conduit en l'absence d'un amorceur peroxyde d'hydrogène, est particulièrement approprié pour la stérilisation de bouteilles de poly(téréphtalate d'éthylène).
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161434515P | 2011-01-20 | 2011-01-20 | |
US61/434,515 | 2011-01-20 | ||
PCT/US2012/021720 WO2012099959A2 (fr) | 2011-01-20 | 2012-01-18 | Stérilisation de contenants d'aliments et de boissons par vapeur d'acide peracétique |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2823217A1 CA2823217A1 (fr) | 2012-07-26 |
CA2823217C true CA2823217C (fr) | 2019-07-30 |
Family
ID=46516345
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA2823217A Active CA2823217C (fr) | 2011-01-20 | 2012-01-18 | Sterilisation de contenants d'aliments et de boissons par vapeur d'acide peracetique |
Country Status (14)
Country | Link |
---|---|
US (1) | US8454890B2 (fr) |
EP (1) | EP2665496B1 (fr) |
JP (1) | JP6005662B2 (fr) |
KR (1) | KR101971743B1 (fr) |
CN (2) | CN108516154B (fr) |
AU (2) | AU2012207342A1 (fr) |
BR (1) | BR112013016896A2 (fr) |
CA (1) | CA2823217C (fr) |
DK (1) | DK2665496T3 (fr) |
ES (1) | ES2762448T3 (fr) |
HR (1) | HRP20192335T1 (fr) |
PL (1) | PL2665496T3 (fr) |
RU (1) | RU2013129819A (fr) |
WO (1) | WO2012099959A2 (fr) |
Families Citing this family (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8889081B2 (en) | 2009-10-15 | 2014-11-18 | Medivators Inc. | Room fogging disinfection system |
US8821807B2 (en) | 2009-12-03 | 2014-09-02 | Medivators Inc. | Container and system for decontaminating a medical device with a fog |
CN103702689B (zh) | 2011-05-27 | 2016-08-17 | 马尔科尔净化装置公司 | 包括使用净化物质的环境控制的净化系统 |
US9050384B2 (en) | 2013-04-03 | 2015-06-09 | Austin Grant Inc. | Means of applying peracetic acid to achieve enhanced microbial effect |
US20150305344A1 (en) * | 2014-04-28 | 2015-10-29 | American Sterilizer Company | Decontamination or sterilization process |
US10463754B2 (en) | 2014-04-28 | 2019-11-05 | American Sterilizer Company | Process for decontaminating or sterilizing an article |
US10869479B2 (en) | 2014-04-28 | 2020-12-22 | American Sterilizer Company | Wipe for killing spores |
CA3041034A1 (fr) | 2016-10-18 | 2018-04-26 | Peroxychem Llc | Traitement de sol |
MX2019015198A (es) | 2017-06-15 | 2020-08-13 | Evonik Operations Gmbh | Tratamiento antimicrobiano de las canales de animales y productos alimenticios. |
US11597664B2 (en) | 2017-11-20 | 2023-03-07 | Evonik Operations Gmbh | Disinfection method for water and wastewater |
AU2019218259A1 (en) * | 2018-02-12 | 2020-08-20 | Medivators Inc. | Peracetic acid vapor sterilization system |
MX2020008501A (es) | 2018-02-14 | 2020-09-25 | Evonik Operations Gmbh | Tratamiento de agua que contiene cianotoxinas. |
WO2019232385A1 (fr) | 2018-05-31 | 2019-12-05 | Peroxychem Llc | Procédés et compositions sporicides |
DE102018113300A1 (de) * | 2018-06-05 | 2019-12-05 | Krones Ag | Verfahren und Messvorrichtung zum Bestimmen einer Peressigsäure-Konzentration in einem peressigsäure- und wasserstoffperoxidhaltigen Sterilisierungsmedium |
CA3104103A1 (fr) * | 2018-06-22 | 2019-12-26 | Peroxychem Llc | Procede de sterilisation |
WO2020202920A1 (fr) * | 2019-04-04 | 2020-10-08 | ニッタ株式会社 | Dispositif et système de décontamination |
TW202222357A (zh) * | 2020-10-02 | 2022-06-16 | 日商新田股份有限公司 | 除污方法 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0456134A2 (fr) * | 1990-05-11 | 1991-11-13 | Abtox, Inc. | Stérilisation avec du peracide et un plasma |
CN2070629U (zh) * | 1990-07-11 | 1991-02-06 | 王宝城 | 筷子消毒器 |
US5645796A (en) * | 1990-08-31 | 1997-07-08 | Abtox, Inc. | Process for plasma sterilizing with pulsed antimicrobial agent treatment |
US6036918A (en) * | 1993-03-17 | 2000-03-14 | Enviro Medical Systems, Inc. | Vapor sterilization |
ES2186246T3 (es) * | 1997-12-12 | 2003-05-01 | Tetra Laval Holdings & Finance | Procedimiento continuo para la hiperactivacion de fluidos de esterilizacion. |
US6536188B1 (en) | 1999-02-02 | 2003-03-25 | Steuben Foods, Inc. | Method and apparatus for aseptic packaging |
CN2375308Y (zh) * | 1999-05-14 | 2000-04-26 | 山东正大福瑞达制药有限公司 | 一种过氧乙酸灭菌器 |
US20020085971A1 (en) * | 2001-01-03 | 2002-07-04 | Raniwala Subodh K. | Bottle sterilizing system and method |
DE60204543T2 (de) | 2001-02-16 | 2006-05-11 | Steris Inc., Temecula | Dekontamination von behältern mit dampf |
US7803315B2 (en) * | 2001-10-05 | 2010-09-28 | American Sterilizer Company | Decontamination of surfaces contaminated with prion-infected material with gaseous oxidizing agents |
JP4010144B2 (ja) * | 2001-12-14 | 2007-11-21 | 東洋製罐株式会社 | 容器の殺菌・洗浄方法及びそれに用いる殺菌・洗浄用噴射ノズル |
EP1374679A3 (fr) * | 2002-06-21 | 2004-01-21 | Nippon Peroxide Co., Ltd. | Composition stérilisante et procédé de stérilisation utilisant celle-ci |
JP2004313780A (ja) | 2003-03-31 | 2004-11-11 | Permelec Electrode Ltd | 過酢酸の電解合成方法及び殺菌洗浄方法及び装置 |
US7012154B2 (en) * | 2004-07-28 | 2006-03-14 | Peragen Systems, Llc | Continuous process for on-site and on-demand production of aqueous peracteic acid |
WO2006030790A1 (fr) * | 2004-09-14 | 2006-03-23 | Toyo Seikan Kaisha, Ltd. | Méthode et dispositif de stérilisation et de remplissage pour conteneurs de type tasse et boisson conditionnée en conteneur de type tasse |
FR2917624B1 (fr) * | 2007-06-19 | 2010-01-01 | Serac Group | Procede de traitement aseptique de recipients par un produit desinfectant avec traitement thermique prealable et installation correspondante |
JP5006265B2 (ja) | 2008-06-06 | 2012-08-22 | アサヒ飲料株式会社 | 滅菌装置 |
WO2010088594A2 (fr) * | 2009-02-02 | 2010-08-05 | Fmc Corporation | Procédé de stérilisation |
-
2012
- 2012-01-18 PL PL12736242T patent/PL2665496T3/pl unknown
- 2012-01-18 KR KR1020137016459A patent/KR101971743B1/ko active IP Right Grant
- 2012-01-18 CN CN201810613033.1A patent/CN108516154B/zh active Active
- 2012-01-18 BR BR112013016896A patent/BR112013016896A2/pt not_active Application Discontinuation
- 2012-01-18 WO PCT/US2012/021720 patent/WO2012099959A2/fr active Application Filing
- 2012-01-18 JP JP2013550563A patent/JP6005662B2/ja not_active Expired - Fee Related
- 2012-01-18 AU AU2012207342A patent/AU2012207342A1/en not_active Abandoned
- 2012-01-18 US US13/353,033 patent/US8454890B2/en active Active
- 2012-01-18 RU RU2013129819/15A patent/RU2013129819A/ru not_active Application Discontinuation
- 2012-01-18 ES ES12736242T patent/ES2762448T3/es active Active
- 2012-01-18 DK DK12736242.4T patent/DK2665496T3/da active
- 2012-01-18 EP EP12736242.4A patent/EP2665496B1/fr active Active
- 2012-01-18 CA CA2823217A patent/CA2823217C/fr active Active
- 2012-01-18 CN CN2012800044297A patent/CN103298491A/zh active Pending
-
2016
- 2016-04-01 AU AU2016202043A patent/AU2016202043B2/en not_active Ceased
-
2019
- 2019-12-27 HR HRP20192335TT patent/HRP20192335T1/hr unknown
Also Published As
Publication number | Publication date |
---|---|
WO2012099959A3 (fr) | 2012-09-27 |
CA2823217A1 (fr) | 2012-07-26 |
US8454890B2 (en) | 2013-06-04 |
JP2014508579A (ja) | 2014-04-10 |
JP6005662B2 (ja) | 2016-10-12 |
EP2665496A2 (fr) | 2013-11-27 |
ES2762448T3 (es) | 2020-05-25 |
AU2012207342A1 (en) | 2013-07-18 |
BR112013016896A2 (pt) | 2016-09-20 |
EP2665496B1 (fr) | 2019-10-02 |
CN108516154A (zh) | 2018-09-11 |
KR20140005190A (ko) | 2014-01-14 |
CN108516154B (zh) | 2021-04-13 |
AU2016202043A1 (en) | 2016-04-28 |
HRP20192335T1 (hr) | 2020-03-20 |
DK2665496T3 (da) | 2020-01-02 |
RU2013129819A (ru) | 2015-01-10 |
US20120189494A1 (en) | 2012-07-26 |
EP2665496A4 (fr) | 2014-08-06 |
AU2016202043B2 (en) | 2017-02-16 |
WO2012099959A2 (fr) | 2012-07-26 |
KR101971743B1 (ko) | 2019-04-23 |
PL2665496T3 (pl) | 2020-05-18 |
CN103298491A (zh) | 2013-09-11 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
EEER | Examination request |
Effective date: 20161125 |