CA2766716C - Continuous emulsification-aggregation process for the production of particles - Google Patents
Continuous emulsification-aggregation process for the production of particles Download PDFInfo
- Publication number
- CA2766716C CA2766716C CA2766716A CA2766716A CA2766716C CA 2766716 C CA2766716 C CA 2766716C CA 2766716 A CA2766716 A CA 2766716A CA 2766716 A CA2766716 A CA 2766716A CA 2766716 C CA2766716 C CA 2766716C
- Authority
- CA
- Canada
- Prior art keywords
- reactor
- facilitating
- stage
- reactors
- continuous stirred
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
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- 239000000839 emulsion Substances 0.000 claims abstract description 29
- 238000004581 coalescence Methods 0.000 claims abstract description 18
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- 229910017604 nitric acid Inorganic materials 0.000 description 4
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- WLJVNTCWHIRURA-UHFFFAOYSA-N pimelic acid Chemical compound OC(=O)CCCCCC(O)=O WLJVNTCWHIRURA-UHFFFAOYSA-N 0.000 description 2
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- 235000011056 potassium acetate Nutrition 0.000 description 2
- WFIZEGIEIOHZCP-UHFFFAOYSA-M potassium formate Chemical compound [K+].[O-]C=O WFIZEGIEIOHZCP-UHFFFAOYSA-M 0.000 description 2
- FRMWBRPWYBNAFB-UHFFFAOYSA-M potassium salicylate Chemical compound [K+].OC1=CC=CC=C1C([O-])=O FRMWBRPWYBNAFB-UHFFFAOYSA-M 0.000 description 2
- 229960003629 potassium salicylate Drugs 0.000 description 2
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- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
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- ZNCPFRVNHGOPAG-UHFFFAOYSA-L sodium oxalate Chemical compound [Na+].[Na+].[O-]C(=O)C([O-])=O ZNCPFRVNHGOPAG-UHFFFAOYSA-L 0.000 description 2
- 229940039790 sodium oxalate Drugs 0.000 description 2
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- UZVUJVFQFNHRSY-OUTKXMMCSA-J tetrasodium;(2s)-2-[bis(carboxylatomethyl)amino]pentanedioate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CC[C@@H](C([O-])=O)N(CC([O-])=O)CC([O-])=O UZVUJVFQFNHRSY-OUTKXMMCSA-J 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
- G03G9/0802—Preparation methods
- G03G9/0804—Preparation methods whereby the components are brought together in a liquid dispersing medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
- B01F25/40—Static mixers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/14—Treatment of polymer emulsions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/14—Treatment of polymer emulsions
- C08F6/18—Increasing the size of the dispersed particles
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G9/00—Developers
- G03G9/08—Developers with toner particles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Dispersion Chemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Developing Agents For Electrophotography (AREA)
- Colloid Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Glanulating (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13/025,664 | 2011-02-11 | ||
| US13/025,664 US8663565B2 (en) | 2011-02-11 | 2011-02-11 | Continuous emulsification—aggregation process for the production of particles |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2766716A1 CA2766716A1 (en) | 2012-08-11 |
| CA2766716C true CA2766716C (en) | 2016-05-24 |
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|---|---|---|---|
| CA2766716A Expired - Fee Related CA2766716C (en) | 2011-02-11 | 2012-02-03 | Continuous emulsification-aggregation process for the production of particles |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US8663565B2 (enExample) |
| EP (1) | EP2487544B1 (enExample) |
| JP (1) | JP5836819B2 (enExample) |
| KR (1) | KR101798245B1 (enExample) |
| BR (1) | BR102012003121B1 (enExample) |
| CA (1) | CA2766716C (enExample) |
| MX (1) | MX336335B (enExample) |
| TW (1) | TWI561298B (enExample) |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US9329508B2 (en) * | 2013-03-26 | 2016-05-03 | Xerox Corporation | Emulsion aggregation process |
| US20150104742A1 (en) * | 2013-10-11 | 2015-04-16 | Xerox Corporation | Emulsion aggregation toners |
| JPWO2015080190A1 (ja) * | 2013-11-29 | 2017-03-16 | 三菱化学株式会社 | スラリーの洗浄装置及び洗浄システム |
| JP2015175913A (ja) * | 2014-03-13 | 2015-10-05 | 三菱化学株式会社 | 静電荷像現像用トナーの製造方法 |
| US9134635B1 (en) | 2014-04-14 | 2015-09-15 | Xerox Corporation | Method for continuous aggregation of pre-toner particles |
| WO2015186710A1 (ja) * | 2014-06-04 | 2015-12-10 | 三菱化学株式会社 | 連続式反応装置及びトナーの製造装置 |
| EP3154674B1 (de) * | 2014-06-16 | 2018-07-18 | Bayer Aktiengesellschaft | Reaktionskammer für einen chemischen reaktor und hieraus aufgebauter chemischer reaktor |
| US9464173B2 (en) * | 2014-12-16 | 2016-10-11 | Xerox Corporation | Latex preparation using an agitated reactor column |
| JP7292743B2 (ja) * | 2018-12-26 | 2023-06-19 | エム・テクニック株式会社 | 流体処理装置 |
| KR102077818B1 (ko) * | 2019-10-21 | 2020-02-14 | 금성이엔씨 주식회사 | 반응기장치 |
| KR102314019B1 (ko) * | 2019-12-20 | 2021-10-15 | 주식회사 포스코 | 과산화리튬의 입도 조절 방법 및 입도가 조절된 리튬산화물의 제조방법 |
| CN116832755A (zh) * | 2023-08-06 | 2023-10-03 | 陈大志 | 一种连续流反应器 |
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| US3590000A (en) | 1967-06-05 | 1971-06-29 | Xerox Corp | Solid developer for latent electrostatic images |
| US4113796A (en) | 1969-11-21 | 1978-09-12 | Bayer Aktiengesellschaft | Process for working up dispersions of elastic-thermoplastic or thermoplastic plastics |
| US3720617A (en) | 1970-05-20 | 1973-03-13 | Xerox Corp | An electrostatic developer containing modified silicon dioxide particles |
| US3800588A (en) | 1971-04-30 | 1974-04-02 | Mts System Corp | Multiple axis control system for vibration test apparatus |
| US3847604A (en) | 1971-06-10 | 1974-11-12 | Xerox Corp | Electrostatic imaging process using nodular carriers |
| US3983045A (en) | 1971-10-12 | 1976-09-28 | Xerox Corporation | Three component developer composition |
| US3944493A (en) | 1974-05-16 | 1976-03-16 | Eastman Kodak Company | Electrographic toner and developer composition |
| US4007293A (en) | 1976-03-01 | 1977-02-08 | Xerox Corporation | Mechanically viable developer materials |
| US4079014A (en) | 1976-07-21 | 1978-03-14 | Eastman Kodak Company | Electrographic toner and developer composition containing a 4-aza-1-azoniabicyclo(2.2.2) octane salt as a charge control agent |
| US4265990A (en) | 1977-05-04 | 1981-05-05 | Xerox Corporation | Imaging system with a diamine charge transport material in a polycarbonate resin |
| EP0023230B1 (de) | 1979-07-26 | 1984-05-16 | J.T. Baker Chemicals B.V. | Reagenz zur quantitativen Bestimmung von Wasser und seine Verwendung zur quantitativen Bestimmung von Wasser |
| US4394430A (en) | 1981-04-14 | 1983-07-19 | Eastman Kodak Company | Electrophotographic dry toner and developer compositions |
| US4560635A (en) | 1984-08-30 | 1985-12-24 | Xerox Corporation | Toner compositions with ammonium sulfate charge enhancing additives |
| US4584253A (en) | 1984-12-24 | 1986-04-22 | Xerox Corporation | Electrophotographic imaging system |
| US4563408A (en) | 1984-12-24 | 1986-01-07 | Xerox Corporation | Photoconductive imaging member with hydroxyaromatic antioxidant |
| US4935326A (en) | 1985-10-30 | 1990-06-19 | Xerox Corporation | Electrophotographic carrier particles coated with polymer mixture |
| US4937166A (en) | 1985-10-30 | 1990-06-26 | Xerox Corporation | Polymer coated carrier particles for electrophotographic developers |
| US4855113A (en) * | 1986-10-27 | 1989-08-08 | Pennwalt Corporation | Apparatus for removing sulfur from organic polysulfides |
| US4858884A (en) | 1988-09-22 | 1989-08-22 | Suntex Industries Incorporated | Diaphragm-actuated valve for a gear pump |
| US5236629A (en) | 1991-11-15 | 1993-08-17 | Xerox Corporation | Conductive composite particles and processes for the preparation thereof |
| US5227460A (en) | 1991-12-30 | 1993-07-13 | Xerox Corporation | Cross-linked toner resins |
| US5302486A (en) | 1992-04-17 | 1994-04-12 | Xerox Corporation | Encapsulated toner process utilizing phase separation |
| US5264315A (en) * | 1992-04-20 | 1993-11-23 | Xerox Corporation | Process for the continuous preparation of encapsulated toner |
| US5290654A (en) | 1992-07-29 | 1994-03-01 | Xerox Corporation | Microsuspension processes for toner compositions |
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| US5344738A (en) | 1993-06-25 | 1994-09-06 | Xerox Corporation | Process of making toner compositions |
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| US5405728A (en) | 1993-06-25 | 1995-04-11 | Xerox Corporation | Toner aggregation processes |
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| US5650256A (en) | 1996-10-02 | 1997-07-22 | Xerox Corporation | Toner processes |
| US5733758A (en) * | 1997-01-10 | 1998-03-31 | Nguyen; Quang A. | Tower reactors for bioconversion of lignocellulosic material |
| US5853943A (en) | 1998-01-09 | 1998-12-29 | Xerox Corporation | Toner processes |
| US6063827A (en) | 1998-07-22 | 2000-05-16 | Xerox Corporation | Polyester process |
| US6214507B1 (en) | 1998-08-11 | 2001-04-10 | Xerox Corporation | Toner compositions |
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2011
- 2011-02-11 US US13/025,664 patent/US8663565B2/en active Active
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2012
- 2012-01-26 JP JP2012014227A patent/JP5836819B2/ja active Active
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- 2012-02-07 EP EP12154299.7A patent/EP2487544B1/en active Active
- 2012-02-07 TW TW101103874A patent/TWI561298B/zh not_active IP Right Cessation
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- 2012-02-08 KR KR1020120013005A patent/KR101798245B1/ko not_active Expired - Fee Related
- 2012-02-10 BR BR102012003121-3A patent/BR102012003121B1/pt active IP Right Grant
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|---|---|
| US8663565B2 (en) | 2014-03-04 |
| TWI561298B (en) | 2016-12-11 |
| EP2487544A1 (en) | 2012-08-15 |
| KR101798245B1 (ko) | 2017-11-15 |
| BR102012003121B1 (pt) | 2019-10-29 |
| TW201238648A (en) | 2012-10-01 |
| JP2012166191A (ja) | 2012-09-06 |
| MX2012001655A (es) | 2012-08-30 |
| BR102012003121A2 (pt) | 2013-07-02 |
| US20120208123A1 (en) | 2012-08-16 |
| MX336335B (es) | 2016-01-15 |
| JP5836819B2 (ja) | 2015-12-24 |
| KR20120092514A (ko) | 2012-08-21 |
| EP2487544B1 (en) | 2016-01-20 |
| CA2766716A1 (en) | 2012-08-11 |
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