CA2414135C - Methode de production d'hydrogene - Google Patents
Methode de production d'hydrogene Download PDFInfo
- Publication number
- CA2414135C CA2414135C CA002414135A CA2414135A CA2414135C CA 2414135 C CA2414135 C CA 2414135C CA 002414135 A CA002414135 A CA 002414135A CA 2414135 A CA2414135 A CA 2414135A CA 2414135 C CA2414135 C CA 2414135C
- Authority
- CA
- Canada
- Prior art keywords
- water
- reaction
- aluminum
- naoh
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title claims abstract description 76
- 239000001257 hydrogen Substances 0.000 title description 40
- 229910052739 hydrogen Inorganic materials 0.000 title description 40
- 238000004519 manufacturing process Methods 0.000 title description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 348
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 132
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 120
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 117
- 238000000034 method Methods 0.000 claims abstract description 32
- 239000007864 aqueous solution Substances 0.000 claims abstract description 26
- 230000008569 process Effects 0.000 claims abstract description 25
- 230000004044 response Effects 0.000 claims description 4
- 239000000243 solution Substances 0.000 abstract description 64
- 239000002244 precipitate Substances 0.000 abstract description 40
- 239000003054 catalyst Substances 0.000 abstract description 7
- 238000002156 mixing Methods 0.000 abstract description 3
- 238000006243 chemical reaction Methods 0.000 description 150
- 238000002474 experimental method Methods 0.000 description 53
- 238000007792 addition Methods 0.000 description 20
- 239000011888 foil Substances 0.000 description 19
- 239000000523 sample Substances 0.000 description 19
- 239000007789 gas Substances 0.000 description 18
- 239000000203 mixture Substances 0.000 description 18
- 239000002245 particle Substances 0.000 description 14
- 239000011734 sodium Substances 0.000 description 13
- 239000012670 alkaline solution Substances 0.000 description 12
- 239000008399 tap water Substances 0.000 description 12
- 235000020679 tap water Nutrition 0.000 description 12
- 230000003197 catalytic effect Effects 0.000 description 11
- 239000000446 fuel Substances 0.000 description 10
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 9
- 239000001301 oxygen Substances 0.000 description 9
- 229910052760 oxygen Inorganic materials 0.000 description 9
- 239000011541 reaction mixture Substances 0.000 description 9
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 8
- 238000004458 analytical method Methods 0.000 description 8
- 239000008188 pellet Substances 0.000 description 8
- 229910052708 sodium Inorganic materials 0.000 description 8
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 description 7
- 230000015572 biosynthetic process Effects 0.000 description 7
- 230000004043 responsiveness Effects 0.000 description 7
- 229910001388 sodium aluminate Inorganic materials 0.000 description 7
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical class [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 6
- 230000005587 bubbling Effects 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 239000004033 plastic Substances 0.000 description 6
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 5
- 238000009835 boiling Methods 0.000 description 5
- 229910052749 magnesium Inorganic materials 0.000 description 5
- 239000011777 magnesium Substances 0.000 description 5
- 229910052751 metal Inorganic materials 0.000 description 5
- 239000002184 metal Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 4
- 238000006555 catalytic reaction Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 239000012047 saturated solution Substances 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 3
- 239000000956 alloy Substances 0.000 description 3
- 229910052681 coesite Inorganic materials 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 229910052906 cristobalite Inorganic materials 0.000 description 3
- 239000012847 fine chemical Substances 0.000 description 3
- 239000003517 fume Substances 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 150000002431 hydrogen Chemical class 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- 230000008929 regeneration Effects 0.000 description 3
- 238000011069 regeneration method Methods 0.000 description 3
- 229910052682 stishovite Inorganic materials 0.000 description 3
- 229910052905 tridymite Inorganic materials 0.000 description 3
- 229910000838 Al alloy Inorganic materials 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 229910021502 aluminium hydroxide Inorganic materials 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 238000001493 electron microscopy Methods 0.000 description 2
- 238000000921 elemental analysis Methods 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 239000006260 foam Substances 0.000 description 2
- 238000004868 gas analysis Methods 0.000 description 2
- 229910001679 gibbsite Inorganic materials 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 238000007614 solvation Methods 0.000 description 2
- 229910009112 xH2O Inorganic materials 0.000 description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 101100348017 Drosophila melanogaster Nazo gene Proteins 0.000 description 1
- 229910000733 Li alloy Inorganic materials 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 229940024548 aluminum oxide Drugs 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000002803 fossil fuel Substances 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 229910000103 lithium hydride Inorganic materials 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 230000009972 noncorrosive effect Effects 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000011002 quantification Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 239000011345 viscous material Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002916 wood waste Substances 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F7/00—Compounds of aluminium
- C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
- C01F7/42—Preparation of aluminium oxide or hydroxide from metallic aluminium, e.g. by oxidation
- C01F7/428—Preparation of aluminium oxide or hydroxide from metallic aluminium, e.g. by oxidation by oxidation in an aqueous solution
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J7/00—Apparatus for generating gases
- B01J7/02—Apparatus for generating gases by wet methods
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
- B01J8/002—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor with a moving instrument
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
- B01J8/003—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor in a downward flow
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
- C01B3/06—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of inorganic compounds containing electro-positively bound hydrogen, e.g. water, acids, bases, ammonia, with inorganic reducing agents
- C01B3/08—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of inorganic compounds containing electro-positively bound hydrogen, e.g. water, acids, bases, ammonia, with inorganic reducing agents with metals
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Catalysts (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Fuel Cell (AREA)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA002414135A CA2414135C (fr) | 2002-12-12 | 2002-12-12 | Methode de production d'hydrogene |
| EP03767339A EP1569868A1 (fr) | 2002-12-12 | 2003-12-10 | Procede de production d'hydrogene |
| PCT/CA2003/001908 WO2004052775A1 (fr) | 2002-12-12 | 2003-12-10 | Procede de production d'hydrogene |
| AU2003291881A AU2003291881B2 (en) | 2002-12-12 | 2003-12-10 | Method for producing hydrogen |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA002414135A CA2414135C (fr) | 2002-12-12 | 2002-12-12 | Methode de production d'hydrogene |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2414135A1 CA2414135A1 (fr) | 2004-06-12 |
| CA2414135C true CA2414135C (fr) | 2009-04-14 |
Family
ID=32477040
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA002414135A Expired - Fee Related CA2414135C (fr) | 2002-12-12 | 2002-12-12 | Methode de production d'hydrogene |
Country Status (4)
| Country | Link |
|---|---|
| EP (1) | EP1569868A1 (fr) |
| AU (1) | AU2003291881B2 (fr) |
| CA (1) | CA2414135C (fr) |
| WO (1) | WO2004052775A1 (fr) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002006153A1 (fr) * | 2000-07-13 | 2002-01-24 | Hydrogen Energy America Llc | Procede et dispositif de production commandee d'hydrogene par dissociation de l'eau |
| WO2006025511A1 (fr) * | 2004-08-30 | 2006-03-09 | Nitto Denko Corporation | Preparation generatrice d'hydrogene |
| JP2006335603A (ja) * | 2005-06-02 | 2006-12-14 | Nitto Denko Corp | 水素発生剤及び水素発生方法 |
| US7803349B1 (en) | 2005-06-08 | 2010-09-28 | University Of Central Florida Research Foundation, Inc. | Method and apparatus for hydrogen production from water |
| EP1905735B1 (fr) * | 2005-07-20 | 2011-09-14 | Hitachi Maxell Energy, Ltd. | Matière générant de l'hydrogène et procédé de production d'une matière générant de l'hydrogène |
| FR2893355A1 (fr) * | 2005-11-16 | 2007-05-18 | Fabien Lecler | Moteur a hydrogene produit par reaction chimique de l'hydroxyde de sodium et de poudre d'aluminium avec l'eau |
| WO2009018468A1 (fr) | 2007-07-31 | 2009-02-05 | Purdue Research Foundation | Système de commande pour un générateur de gaz à la demande |
| WO2013009158A1 (fr) * | 2011-07-08 | 2013-01-17 | Iturbe Garcia Jose Luis | Procédé pour la production de gaz hydrogène, d'alumine et de carbonate de sodium en une seule étape à partir de la réaction entre des particules d'aluminium et une solution aqueuse d'hydroxyde de sodium |
| WO2013150527A1 (fr) * | 2012-04-05 | 2013-10-10 | H Force Ltd | Système et procédé pour la production efficace d'hydrogène |
| RU2603802C2 (ru) * | 2015-04-30 | 2016-11-27 | федеральное государственное бюджетное образовательное учреждение высшего образования "Московский государственный машиностроительный университет (МАМИ)" (Университет машиностроения) | Установка для получения водорода и гидрооксидов алюминия |
| RU2603669C2 (ru) * | 2015-04-30 | 2016-11-27 | федеральное государственное бюджетное образовательное учреждение высшего образования "Московский государственный машиностроительный университет (МАМИ)" (Университет машиностроения) | Установка для получения водорода и гидрооксидов алюминия |
| JP6498156B2 (ja) * | 2016-07-05 | 2019-04-10 | アルハイテック株式会社 | 水素製造装置及びそれを用いた製造方法 |
| CN108426281A (zh) * | 2018-04-23 | 2018-08-21 | 苏州瑞之弘空气净化有限公司 | 一种环境工程直流式排烟装置 |
| CN112110413B (zh) * | 2019-06-19 | 2024-02-13 | 中国神华能源股份有限公司哈尔乌素露天煤矿 | 一种可水解制氢的Al-Ga基合金的水解副产物的回收方法 |
| FR3103482B1 (fr) * | 2019-11-25 | 2022-07-22 | Nebula Tech | Procédé et installation pour produire de l’hydroxyde d’aluminium |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01208301A (ja) * | 1988-02-15 | 1989-08-22 | Mitsubishi Heavy Ind Ltd | 水素発生方法 |
| EP1301433A1 (fr) * | 2000-07-20 | 2003-04-16 | Erling Reidar Andersen | Production d'hydrogene a partir d'aluminium, d'eau et d'hydroxyde de sodium |
| CN1162320C (zh) * | 2002-03-04 | 2004-08-18 | 孙元明 | 一种氢气制备装置 |
-
2002
- 2002-12-12 CA CA002414135A patent/CA2414135C/fr not_active Expired - Fee Related
-
2003
- 2003-12-10 WO PCT/CA2003/001908 patent/WO2004052775A1/fr not_active Application Discontinuation
- 2003-12-10 AU AU2003291881A patent/AU2003291881B2/en not_active Ceased
- 2003-12-10 EP EP03767339A patent/EP1569868A1/fr not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| AU2003291881B2 (en) | 2009-10-08 |
| AU2003291881A1 (en) | 2004-06-30 |
| EP1569868A1 (fr) | 2005-09-07 |
| CA2414135A1 (fr) | 2004-06-12 |
| WO2004052775A1 (fr) | 2004-06-24 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request | ||
| MKLA | Lapsed |
Effective date: 20131212 |