CA2220512A1 - Frozen cocktails made from a flavor concentrate - Google Patents

Frozen cocktails made from a flavor concentrate Download PDF

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Publication number
CA2220512A1
CA2220512A1 CA002220512A CA2220512A CA2220512A1 CA 2220512 A1 CA2220512 A1 CA 2220512A1 CA 002220512 A CA002220512 A CA 002220512A CA 2220512 A CA2220512 A CA 2220512A CA 2220512 A1 CA2220512 A1 CA 2220512A1
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frozen
range
concentrate
solid content
slush
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CA002220512A
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J. Michael Herbert
William Shazer Jr.
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G9/00Frozen sweets, e.g. ice confectionery, ice-cream; Mixtures therefor
    • A23G9/32Frozen sweets, e.g. ice confectionery, ice-cream; Mixtures therefor characterised by the composition containing organic or inorganic compounds
    • A23G9/42Frozen sweets, e.g. ice confectionery, ice-cream; Mixtures therefor characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G9/00Frozen sweets, e.g. ice confectionery, ice-cream; Mixtures therefor
    • A23G9/04Production of frozen sweets, e.g. ice-cream
    • A23G9/045Production of frozen sweets, e.g. ice-cream of slush-ice, e.g. semi-frozen beverage
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/005Solid or pasty alcoholic beverage-forming compositions
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • C12G3/06Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with flavouring ingredients

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Genetics & Genomics (AREA)
  • Zoology (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Wood Science & Technology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Botany (AREA)
  • Inorganic Chemistry (AREA)
  • Confectionery (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Alcoholic Beverages (AREA)

Abstract

A liquid frozen cocktail concentrate has a solid content, preferably entirely carbohydrates, such that when it is frozen in a freezer compartment of a conventional refrigerator, it is frozen to a solid, but softly ("quiescently") frozen. A suitable solid content produces a measured Brix value, measured on a disacharride scale, in the range of 10~ to 25~. The solid content preferably consists of 1) pure or artificial flavors, particularly natural fruit juice and fruit fiber and 2) a sweetener, whether a natural sugar, or a high potency sweetener, or some combination thereof. The process includes producing such a concentrate, freezing such a concentrate to a quiescently frozen state, and mechanically blending it, e.g. using a conventional home food blender, with liquid diluent added in a weight ratio (w/w) of 1:1 to 3:1 frozen solid to liquid, and preferably in the range 1:1 to 2:1. For cocktails, the diluent is preferably a mixture of water and a distilled 80 proof distilled spirit in a volume ratio (v/v) of 2:1 to 4:1 water to spirit. The Brix of the concentrate can vary from 10~ to 25~, but for most drink types is in the range of 16~ to 22~, and preferably 18~ to 21~. The Brix of the blended, finished cocktail is in the range of 9.0~ to 15.0~, but for most drink types is preferably in the range of 11.0~ to 13.5~.

Description

CA 022205l2 l997-l2-l7 W O96/37120 PCTrUS~JOCq~2 TTTT.~ OF l~n~ INV~ l'lON
FROZEN COCIKTAILS MADE FROM A FLAVOR CONCENTRATE

RA~GROmND OF I~IE lNv~N~ oN
This in~ention relates to frozen slush beverages, and in parti~ular to a liquid flavor concentrate and a method of using the concentrate to form a high quality frozen slush cocktail.
Frozen cocktails ~re well known as mixtures of crushed or s~aved ice, spirits, fruit juice, and sugar that is strongly mixed until the crushed ice is reduced lo to a "snowy" ~Dr "slush''' consistency. Frozen daiquiris, margaritas and pina coladas in a variety of flavors ~uch as stra~diberry, peaLch and citrus varieties have become incre~singly popular as bar specialty drinks.
The traditional approach to making such frozen drinks begins with ordinary ice. It is then crushed, cracked, shaved or blended to form a slush to which a spirit, flavors and sweeteners are added. The traditional recipe, particularly for home use, is to use ice cubes that are pol7n~ into crushed ice, e.g.
in a canvas bag using a wooden mallet. The crushed ice is then blended into a slush. A conventional home blender can be used.
In practLce, few hosts or bartenders wish to take the time and exert the physical effort required to crush ice cubes manually . As a result, to the extent that frozen drinks are made "from scratch" at home, they use ice cubes from a home freezer that are added directly to t:he cup of a blender. The other ingredients are added to the blender cup and the blender operal:es until the ice cubes are broken up into very small pieces.
This approach, however, has several drawbacks which have siLgnificantly hindered its use. First, the noise generated by the blender in pulverizing the rock-CA 02220~l2 l997-l2-l7 W 096/37120 PCTIU~5GI~6412 hard ice cubes proAllc~ in a freezer compartment of a conventional refrigerator i8 substantial. Typical operating temperatures for home refrigerator freezer compartments are -lO-F to +lO-F, with 0- to 5-F being perhaps the most common temperature range. In contrast, ice at commercial bars i8 often ~tored at temperatures much nearer to 32-F, and as a result is "softQr" than household ice. The temperature in home freezer chests is typically colder than in refrigerator freezer compartments, a typical range of values being -15-F to 5-F.
Secol.d, fracturing and subdividing a cup full of home ice cubes produces substantial wear on the blades and the blender. A blender that is regularly used to pulverize ice cubes will perform more poorly a~ a food blender. Third, the pulverization process is fairly slow as compared to commercial blenders and specialized equipment such as the automatic frozen cocktail machines for bar use described in one of the present applicant's U.S. Patent Nos. 4,528,824 and 4,681,030 and commercial slush making ma~hi n~C which scrape ice as it forms on a chilled surface. Fourth, the various ingredients must be available at home'and measured out indiv~ y. Fifth, in practice it is difficult for the an amateur barten~er to produce frozen drinks "from scratch" and achieve a smooth consistency -- -- small ice particle of uniform size that preferably "peak"
when ~ouLed into a glass - and a good taste. Some skill and experience is useful. Moreover, it is often impossible for a home blender to reduce all the ice particles to a uniformly small size regardless of skill in any r~onAhle length of time. As the cubes are fractured, the contents of the blender becomes more viscous and the movement of ice pieces to the blades becomes more difficult. This is particularly true where the slush being formed is "thick" -- as opposed to watery -- whether due to refreezing of divided CA 02220~12 1997-12-17 W O96137120 P ~ ~U~ C6~2 particles or to insufficient addition or production (due to melting of ice~l of liquid in the slush.
To solve some of 1hese problems, various companies have cQncoct~ed and mar}ceted dry powder mixes, liquid pre-mixes, and pre-froxen products for home use that all include flavoring and sweeteni n~ ingredients in pre-mixed portions. A dry powder mixer, for example, i8 marketed by Franco'~~ Cocktail Mixes of Pompano Beach, Florida, under 1;he trade designation "Franco's".
It directs t~e user add the mix and spirits to an ice-filled cocktail ~k~rO However, the resulting drink i8 a traditional chilled cocktail, not a blended frozen drink. Heublein, Inc. of Farmington, Connecticut markets a liquid margarita mix under the trade designation "Cuervo" and Bacardi & Co., Ltd. markets a liquid margarita cQ~rltrate mix under the registered trademark "Bacardi Tropical Fruit Mixes". Theses liquid mixes are addedr with a spirit, to ice in a blender cup.
While these and like mixes avoid the inconvenience of separatel~ buying, storing, and measuring out or ~queezing out flavor and sweetener ingredients, the aforementioned problems associated with reducing ice from a lump to a slush remain. There is the added problem that chemical preservatives, freeze point depressants, and other components that affect crystallization can affect the flavor of the f;n;~h~
drink. Furtlher, the mix is portioned for a preset number of drink servings. The pre-mix product must be measured out to make single drinks, or drinks in a quantity other than that corresponAing to the use of the entire package or hottle.
Several frozen flavor mixes for frozen cocktails are also kno~n. Coca Cola Foods, for example, sells a frozen daiquiri concent:rate under the trade designation "Bacardi Mixers". Like the powder and liquid mixes, it pre-mixes flavor, sweet Dn; ng, texture and preservative CA 02220~12 1997-12-17 W O96/37120 PCT~US3~ 12 ingredients. And like the dry mixes, it also directs the use of ice. For alcoholic drinks, the user i8 instructed to add to a blender cup one cont~in~r of the mix and a half to one cont~iner of rum. The user fills the blender with ice. Bl~nA~ng then yields five frozen daiquiris in 8 fluid oz. servings. Even without addressing the important issue of taste, the product suffers from the fact that it must be stored frozen, sold frozen, and maint~ n~ in a frozen state until used. The cost of freezer ~pace in a retail store --and the total ~h~en~ of freezers in many stores that sell distilled alcoholic beverages -- make such frozen products unattractive for both cost and convenience re~onC. Also, the product is sold in a can like lS frozen concentrated orange juice, and prepared in the same way, in a single large batch. It is not con~l1cive to making single drinks to order, or any serving size other than that of a full blender.
U.S. Patent No. 3,647,472 to Speech, et al.
describes a water, sugar, glycerol, flavoring mixture that is 20 to 40% solids and which freezes in a home freezer to a slush. The water forms ice crystals and the "syrup" of glycerol, sugar and other colids ~, ~in~
liquid. A serving size of this slush is added to a glass and stirred with a spirit or water to form a chilled liquid drink -- a cocktail if alcohol is used.
The end product alcoholic drink is a liquid, not a frozen cocktail.
Heublein, Inc. has sold a complete, "ready to consume" frozen cocktail product. This product is believed to have been sold under the trade designation "Tropic Freezer~" and made according to U.S. Patent No.
4,790,999 to Ashmont, et al. assigned to Heublein, Inc.
The Ashmont cocktail product includes flavor and ~wee~Dn~ ng ingredients, alcohol, and carboxymethylcellulose (CMC), all premixed. The CMC is described in this patent as a "critical" component in CA 02220~12 1997-12-17 W 096137~20 PCrIU~G/C6~2 producing the desired consistency when the product is frozen. The ~Einal product has a Brix value of 18- to 25 . once frozen, it can be eaten directly from a con~i n~r or ~roo~ into a glass for a slush-type drink; It i~ not blended, let alone blended with an added liquid. To drink this product, it must be warmed to a ~ri nk~hle~ consistency.
As a gerleral rule, artificial additives degrade flavor. Whi~Le organoleptic qualities are to some degree subjec1:ive, flavor and consistency of the fully pre-mixed fros~en cocktails do not compare favorably to those of frox~an drinks made fresh from crushed or shaved ice at bars (such as those made using the aforementioned automatic ice shaving and bl~n~; n~
machine and t:he frozen cocktail fruit juice mixes manufa~L~d 2md sold by the Island Oasis Frozen Cocktail r , ny of Walpole, Mas~achu~etts under the registered trzldemark "Island Oasis-"). Dry, liquid and frozen conce.,l~ates without distilled spirits continue to dominate t:he home frozen cocktail market. Moreover, the market as a whole for frozen cocktail products for home use remaLns small as compared to the market for all home-use c:ocktail products.
To date, there ha~ been no frozen cocktail product which can be ~itored and sold in a liquid form at room temperature, iErozen at home in a conventional home refrigerator, and then conveniently used in a home blender, without any added ice, to produce a high quality frozel1 cocktail.
It is therefore a principal object of the present invention to provide a method of making a frozen cocktail and a flavor concentrate used in this method that is a solcl as a liquid, frozen, and then directly blended without ice.
Another principal object is to provide a method and co~centra1:e product with the forgoing advantages that blends rapidly in an ordinary home blender to form CA 02220~12 1997-12-17 W O96/37120 PCT~US~6/0~4~2 a high quality frozen cocktail, as well as non-alcoholic versions of the cocktails, in any of a wide variety of flavors and types.
Another object is to provide a flavor conc~ntrate that does not separate or hard freeze when frozen in a conventional home refrigerator.
Still another object is to provide a method and product with the foregoing advantages which is convenient to store and use and requires no Gpecial skill or equipment to make professional quality drinks quickly, quietly, and in any preselected number of drinks.
A further object is to provide a product for use in the method which can be made of all natural products, yet stored without preservatives, for ext~n~ periods of time to provide a long shelf life.

SUMMA~Y OF THE lNv~NllON
A flavor conc~ntrate used to make a frozen cocktail has a total solid content, including sweeteners and flavor ingredients, that is equivalent in depressing the freeze point of a water solution to a disaccharide aqueous sugar solution with a Brix value in the range of 10 to 25 , in the range of 16- to 22-for most drink types, and preferably in the range of18- to 21-. This Brix value is a sufficiently accurate weight measure of the solid content of the co~c~ntrate to its total weight. The desired equivalent Brix value in this range varies with factors such as the type of drinks being made and the volume and the nature of liquid additives, e.g., a distilled alcohol product and water. The solid content is preferably totally carbohydrates. Defined functionally, the total solid content should be such that 1) when frozen at temperatures typical of a home freezer (e.g., O-F + lO-F), the concentrate is softly, or "quiescently", frozen: and 2) when blended with a W 096137120 PCTAUS9C/r~2 liquid accord.Lng to this invention, will produce a frozen drink l~at blends readily to produce a drinkable slush of generally ~mall uniformly sized ice particles with ~Y~e~lenl organoleptic characteristics. The f~ drinlc preferably "peaks" when poured into a serving gla5s.. Using a conventional one c~uart home blender opera1;ing at high speed, blenA;n~ typically is completed in ~L0 to 30 ~?co~C. The ~f;n;ch~A~
~ c~h~ide. scale) Brix of the resulting frozen cocktail is preferably in the range of 11.0~ to 13.5-, but can lie wiLthin the range 9.0- to 15.0-.
The ~ ~o~i_s of this invention includes freezing a lic~uid flavor cQ~er.Lrate with ~uch a solid content to a ~olidly, but: softly, frozen state, and blending a measured port.iLon of the frozen conc~ntrate with a licluid diluent: consisting of a distilled spirit, water, or a mixture of a distilled spirit and water. The weight ratio ~,w/w) of ~olid frozen concentrate to diluent is in t~e range of 1:1 to 3:1. The preferred formulation for the diluent is a mixture of water and a di~tilled spirit (such as 80 proof rum, gin or tequila) in a 2:1 to 4:1 volume ratio (v/v) of water to spirit.
The ~on~entrate preferably is formulated from all natural produc:ts including natural sugars, sweeteners such as sucro~e, dexL,o-e and fructose and natural fruit flavors such as berry, citrus, or peach derived from the juice, fibers, and other naturally occurring nutrients in t:he selected fruit or fruit blend. The water is preferably refrigerator-chilled bottled water to avoid variations in flavor due to varying mineral contents of t.ap water and variation in its temperature.
Chilling the water before use aids in the blenA~ng.
Proportions oi~ frozen conc~ntrate, spirits or other liquid to procluce the desired flavor and texture in the f~ n~ h~-l drin}c vary with the type of drink (e.g.
daiquiri, margarita, pi~a colada) and flavor (e.g.
strawberry, peach, h;~n~n;3) and personal taste.

CA 02220~12 1997-12-17 W O96/37120 PCTrUS9610C4~2 However, the nature, solid content (expressed as a Brix value), and sweetness of the ~nnc~ntrate are mutually ad~usted to produce a smooth blended cocktail with the desired taste. For many drinks and flavors, a mix of about 4 oz. by weight of frozen ~onc~ntrate, about 3 fluid oz. of water and about 1 fluid oz. of 80 proof distilled spirit is preferred. The frozen ronc~ntrate i8 preferably blended as four separated portions each weighing about 1 oz. (28.4g).
These and other features and advantages of this invention will be more fully understood from the following detailed description which should be read in light of the accompanying drawings.

RT~TT.'F D~~ TpTTON OF T~ DRAWINGS
Fig. 1 is a block diagram showing the method of the present invention for making frozen cocktails without blen~i~g ice;
Fig. 2 is a view in perspective illustrating the blender addition steps of Fig. 1: and Figs. 3-5 are graphs of the pressure applied to a cube of softly frozen conc~ntrate by a shear press pi~ton as a function of time/distance for low, medium and high solid contents in the concentrate.

n~ATTT.~n DESCRIPTION OF THE ~K~ EMBODIMENT
Fig. 1 gives an overview of the method of the present invention for making high quality frozen cocktails 10 at home. The present invention supplies a water based co~c~ntrate 12 that is a liquid at room temperature, freezes it at typical home freezer temperatures, as represented at block 14, to form a solid concentrate 16 that is softly frozen, and adds the frozen concentrate to a blender cup 18 along with a liquid diluent 20. A blender 22, preferably a conventional home kitchen blender used for food W O9613~120 PCTrUS96/06442 processing 1:]nen operate~ to blend the frozen conc~ntrate 16 and the liquid 20 into a slushy suspension of finely divided particles of the frozen D conc~trate.
~he meçh:~nical re~istance of the frozen concentrate 1:o being blended and the texture or smoo~hn~c of the final drink ~p~nA ~L~ ly on the level of solid content in the ronGentrate and on the temperature 1:o which it is frozen. The ability of the process to produce a ~ooth good-tasting end product drinlc also ~p~n~ strcngly on the volume ratio of the frozen conc~r-l:rate to the diluent, and the nature of the ingredienl: forming the concentrate and the diluent.
The type of ~olids is also a factor. As a general rule, except where taste considerations override, the solids should be carbohydrates. ~o make an alcoholic cocktail dilllent can b~e exclusively a distilled spirit. Howe~rer, blendability is usually improved if the liquid vo:Lume i8 increased by s~; ng water. Water content in the slurry is al80 influenced by warming of the ice in the frozen cQncentrate due to the warmer temperatures of the admixed liquid, the blender cup the ambient a:ir, as well as the merh~n-cal working of the mixture by the rotating blades 24 of the blender as it operates. Therefore these temperatures and the bl~n~; n~ time. and speed are also factors that affect texture, but 1;o a lesser degree than the other factors noted above as strongly affecting blendability and finished drinlc quality.
The conc~ntrate 12 in its simplest form is a solution of wzlter 26 a flavor ingredient or ingredients 28, and a sweetener or sweeteners 30. The flavor ingredLent 28 is typically a fruit flavor, preferably one provided by a natural fruit juice a blend of frui1: juices or a combination of fruit juice and crushed nzltural fruit or fruit pieces. The natural juice and crushed fruit also introduce to the CA 02220~12 1997-12-17 W 096/37120 PCTrUS~6/OC~2 co~centrate natural fruit fibre and small amounts of naturally occurring nutrients found in the natural fruit being used. Solids in the co~centrate which do not add positively to the flavor of the f~nish~ drink are referred to herein as other ingredients 32. The other ingredient 32 includes not only unflavored fibre and naturally occurring non-flavoring protein and fat nutrients, but also natural and artificial solids such as glycerol, p-glycerol, salts, gums and preservatives.
Typical flavors are varieties of citrus, varieties of berry, h~nA~A, and peach. While a natural fruit juice, with or without crushed fruit or fruit pulp, is preferred, it is possible to use artificial flavors, or combinations of natural and artificial flavors, as is well known in the food industry. Non-fruit flavors, or blends using fruit flavors only in part, can also be used. Examples of such flavors are piha colada and ice cream. However, regardless of the flavor, as noted above, it is essential that the conc~ntrate have a total solid content that is softly frozen at freezer temperatures available to, and selected by, the user.
The liquid frozen cocktail mix now sold for commercial bar use by the Island Oasis Frozen Cocktail Co. of Walpole, Massachusetts under its registered trademark "Island Oasis" is preferred. It is made and sold in a variety of natural flavors for numerous drink types, e.g. strawberry, h~n~n~ ice cream, and peach daiquiri, regular flavor margarita and piha colada.
The sweetener 30 is likewise preferably a natural sugar such as sucrose, glucose, or fructose. The flavor ingredient 28, particularly of a naturally sweet fruit, will often itself have a measure of naturally occurring sugar, but for the flavors and frozen drink types now popular it is necessary to add the sweetener 30. The amount of sweetener to be added ultimately ~ep~n~ in part on the taste and texture of the final blended frozen cocktail.

CA 02220~12 1997-12-17 WO 96137~20 PCT/U::"C/OC 112 The sweetener 30, 1:he flavor ingredient 28, and the other ingredients 32, provide a total solid content in the water-lh~ ~oncentrate that yields the functional characterist~~Lcs and f;~ishe~ product of the present invention a~ de~;cribed herein.
More specifically, the total solid content of the co~c~ntrate 12 should produce a depression of the freezing poin~ of the cc)~c~ntrate that is equivalent to the freezing point depression of a solution of a disaccharide ~ugar (e.g. ~ucrose) in water having a Brix value in the range of 10- to 25-, and for most drinks a high value in t;he range of 16.0 to 22.0 , and preferably in the range of 18- to 21 . The solid content value is calculated as a weight ratio of the solid content to that of the solid content in solution, the co~ce~trate. While Brix, a measure of the specific gravity of a ~sugar solut:ion, is used as a weight measure of sucrose in a sucrose-water solution, it is known that the change in specific gravity of a sugar solution pro~ e~ by suarose is substantially the same as the change~1 pro~llce~ by other natural sugars such as glucose and f~uctose. ~oreover, the presence of non-sugar solids causes only small errors in the Brix value. Standard disaccharide Brix is therefore a r~co~hly accurate measure of total solid content of aqueous sugar and flavor solutions regardless of the exact nature of the solids, and is so used herein. The Brix measurement of the frozen cocktail product is skewed by the pre-~n~- of the ice crystals. It is measured after the ice aontent of the cocktail has melted.
The measured Brix value varies within this range dep~n~ing on factors that include (i) the nature of the ingredients, 28, 30 and 32 to produce the desired drink, (ii) whether the cocktail 10 contains alcohol or is non-alcoholic, e.g. a '~virgin dai~uiri", (iii) the temperature of which the concentrate will be frozen, CA 02220~12 1997-12-17 W O96/37120 PCTrUS96/06442 ~ 12 ~
(iv) the nature and volume of the liquid 20 in pro~o~ Lion to the volume of frozen co~centrate used, and (v) the nature of the sweetener, e.g. a simple sugar, a complex sugar, an artificial sweetener, (vi) 5 the temperature of the blended ingredients and (vii) the strength of the distilled spirit and the mineral v content of the water used as the liquid 20. In general, alcohol as a diluent greatly aids in blenAing of the frozen con~entrate to form the f;n;~h~ drink.
10 Non-alcoholic slush drinks are therefore more difficult to blend and, in general, require a longer bl~nAing time and offer less latitude in the range of portions of ingredients and other process parameters than alcoholic frozen cocktails. Other considerations 15 include (i) the characteristics of the ron~trate when it is frozen and when it is broken up in the blender, such as whether the ingredients of the co~centrate freezes to a soft solid at temperatures normally found in a home freezer, whether the frozen conc~ntrate blend 20 readily into finally divided and evenly dispersed frozen particles when blended, whether the concentrate separates when frozen at home freezer temperatures, (ii) the sweetening power of the particular sweetener, and (iii) the solid content contributed to the 25 concentrate by the sweetener 30. As is well known, a monosaccharide such as glucose or fructose is sweeter than a disaccharide such as sucrose, and certain high potency sweeteners such as aspartame, at least when used in low concentrations~ are much stronger 30 sweeteners than like amounts of natural sugars.
The following are examples of concentrates 12 and methods according to the present invention of using these concentrates. All cocktails were prepared using a conventional home blender such as an Imperial brand, 35 two speed, one quart size blender manufactured by -Osterizer, Inc. at its "high" operating speed, to produce frozen cocktails of high quality in taste and ~ 13 -texture Wit]l,DUt using ice CUbQ~ shed or crushed ice, or shav~d ice. Ingredients were weighed on an Ohaus brand triple bQa~ scalQ to the nearest O.lg (2,610g capa~-ity). The ~Qn~ntrates were mixed in a sealable pla~stic cont~in~ by ~ k;n~ until thoroughly J mixed. The cQn~entrat:e was frozQn in conventional plastic ice ~ube tray~ for 48 hours in a s~n~d 6 cubic foot capacity, c:hest-type home freezer set to a freezing te~]?erature of -15-F. Brix values were 10 measured wit~l Milton-R~oy Co. hand-held refractometer, Cat. No. 33--45-01. The concentrates were formed by diluting frozen cocktail mixes sold under the trade designation Island Oasis~ with water. The ~pirits used are 80 prooi.' and at room temperature. Rum is preferred 15 for daiquiri.~; and pina coladas. Tequila is preferred for the marg2lrita. The frozen co~o~,.L~te is added in cubes pro~ e~ by the ice-cube tray, with each cube representing about 1 fluid ounce of concentrate (about 32g). The water is bottled water chilled in a 20 conventional. refrigerator.

~xAr~PLES
Blended ~ Blend Frozen Drink Bri~ o~ Frozen Blended Blended Time TvDe Concentrate ~n~ntrate water S~;rit (sec.) (Fluid oz.) (Fl. oz.) ~Fl. oz.) Strawberry Daiquiri 19.5 4.0 3.01.015 Peach Daiguiri 19.5 4.0 3.01.015 Banana Daiquiri 20.5 4.0 3.o1.015 30Non-Alcoholic Banana Daiquiri 20.5 4.o 4.o - 15-20 Margarita 18.5 5.0 3.01.015 Piha Colada 20.8 6.0 3.01.015 Non-Alcoholic Piha Colada 20.8 6.0 4.0 - 15-20 35Ice Cream 19.8 6.0 3.01.015 Non-Alcoholic Ice Cream 20.8 6.0 4.0 - 15-20 CA 02220~12 1997-12-17 W O96/37120 PCTrUS9610C4~2 It will be understood that these values are approximate and that the user can vary from the recommended values and procedures, whether in error, out of ~Gl.vellience, or due to taste and still obtain a r 5 high-quality, good-tasting frozen drink. As reflected in these examples, a co~ce.L~te with a Brix in the range of 18- to 21- will produce an optimal flnish~
drink for most st~n~A~d drink types. As a general rule, increasing the liquid 20 added to the blender 10 without a CO~ LeS~O~ ng increase in frozen conce~trate will reduce the bl~n~l~ ng time and produce a more watery slush. A practical lower limit on the frozen cono~.Llate-to-diluent ratio is determined by the fact that the slush becomes too watery (too low of a 15 vi~cosity to blend) even at re~lce~ blending times, when too much liquid is used. On the other hand, reducing the liquid content increases the ice content in the frozen drink, making it "stiffer". (A good slush texL~Le is characterized by the finished drink ~P~Ak~ ng~ when ~o~red into a glass, but being readily pourable and drinkable with few, if any, large frozen particles.) Practical lower limits on the amount of diluent liquid added to the blender arise when the frozen co~centrate will not blend well, e.g. it will freeze to the walls of the blender cup, will not circulate to the blender blades, or will not divide uniformly and finely, e.g. "marbles" of frozen concentrate remain the slush after the recommended bl~n~ ng time. The weight ratio (w/w) of frozen co~cDntrate 16 to liquid diluent 20 is in the range of 1:1 to 3:1, but preferably closer to 1:1 for most drink types.
Large, irregularly-sized frozen particles will also result from the Brix level of the concentrate being too low. Conversely, Brix that is too high results in a watery slush. These results and taste considerations, provide practical functional guidelines CA 02220~12 1997-12-17 W 096/3712U PCT~US~'C6q12 for selecting approprialte values for particular type of ~oncentrate a~nd a particular drink. With respect to taste, a Brix ~ralue for the final product can range from 9- to 15-, but drinks with the best taste will prefer~bly ha~ve a value in the range of 11.0~ to 13 . 5- .
With res]?ect to the spirit to water ratio in the diluent liqu~, as a general rule, as noted above, increased alcohol conte.nt facilitates the bl~n~ ~ n~ .
Therefore if a higher ~lcohol content is desired, the bl~n~i n~ time is ordin~rily re~llc~. The overall liquid volume, the volume of the spirit and water, should, howe~rer, remain at or near the preferred values given, other Eactors being the same. The preferred ratio for the diluent ingredient in an alcoholic frozen cocktail is in the range of 2:1 to 4:1 water-to-spirit by volume. A~; demonstrated in the Examples above, a 3:1 ratio is preferred for many drink types.
The affect of Brix on the blendability (and therefore texlture) of the frozen co~c~ntrate is illustrated hy Figs. 3~5. Graphs showing the fracturing oiE a cube of frozen sugar water conc~ntrate over time as lthe pressure applied by an F'rC shear press. The press is a 5~n~rd instrument used to measure the resistance of a solid to a crushing force applied by a pneumatic piston. Since the piston travels at a generally constant rate, elapsed time equals distance travelled by the piston. Fig. 3 is a typical graph for a solution with a low solids content (e.g. below 1:2.5- Brix). Fig. 4 shows the typical reaction curve for a medium solid content (e.g. 15--20-Brix). Fig 5 shows the typical reaction curve for a high solid content (e.g. in ~Ycecc of 20- Brix).
In each graph the initial pressure increase reflects the ;resistance of the frozen cube to fracturing. 'rhis result is a function of solid content and the tempe;rature of the frozen cube. The curves show typical results for cubes at the same temperature.

CA 02220~12 1997-12-17 W O96137120 PCTrUS96/06442 After initial fracture indicated at F in the graphs, the shear press piston travels farther until a second resistance is encol~ntered. The degree to which the pr~-s~lre falls after the initial fracture, expressed as S a percentage pressure relief, yields an indication of how resistance to fracture varies as a function of solid content.
The r~con~ increase of pressure as the shear press piston travels to a maxi~um compression of the sample varies in smoothnCcc as a function of the solid content. Higher solid content produces a smoother crush curve, as shown.
These tests confirm that solid content of the concentrate is a key factor in the blendability of the frozen concentrate into a good slush. More specifically, softly frozen samples with a Brix below 12.5-, and certainly below 10.0 are difficult to crush and do not produce a uniform particle size in a blended frozen drink product. Conversely, solid contents much in eYc~s~ of about 20.0 Brix are too soft to produce a high quality slush drink when blended. This range of Brix values also pro~llcec~ at ordinary home freezer temperatures, a ~oftly frozen con~entrate that does not dull or damage an ordinary home blender used to of reduce frozen conc~ntrate into finely divided slush. Recall, however, that blendability varies dep~n~;ng on the type of the ingredients forming the conc~ntrate and the diluent and the relative amount of frozen concentrate and diluent. These tests do not reflect these variables; but they do demonstrate the basic relationship between Brix and fracture.
The fracture characteristics of a frozen concentrate according to this invention also lend themselves to partitioning a mass of the frozen product into pre-measured portions. This and the ability to freeze cubes of the concentrate in a conventional ice CA 022205l2 l997-l2-l7 W 096J3~120 PCTfiUS9~l~J~5~2 cube tray allows frozen drinks to be made in any of a wide variety of guantities, from a single serving to batches of mu:Ltiple servings.
There hns been described a frozen drink product aLnd process t:hat can be sold and stored as a liquid, home frozen, ~md then blended c~Lickly and quietly using aL st~AA~d h~I~e blender to produce frozen drinks, particularly ~Erozen cocktails, having a high quality taste and te~:ure. The product and ylO aLs can make a vaLriety of driLnk types in aL variety of flavors, and in a variety of serving sizes. A low skill level is required. There i8 minimal preparation time (once the concentrate i.s frozen), and the preparation is simple, comparatively ~uiet, and does not harm the blender.
The product alnd process do not require expensive or nll~llAl ingreclients, and preferably uses only natural carbohydrates as it s 801 id content in the aqueous h~rl concentrate, typically a fruit juice and a natural sugar in ac~ueous solution diluted to a Brix value in deteI~Lined accordance with this invention.
The product and process of this invention are also highly flexib].e in terms of the types of drinks -alcoholic, norl-alcoholilc, fruit based,'non-fruit based -- that can be made while enjoying all of these advantages.
While thLe invention has been described with respect to it.~; preferred embodiments, it will be understood thLat various modifications and alterations will occur to those skilled in the art from the foregoing detailed description and drawings. For example, while the invention has been described with respect to a con~ntrat,e formed by diluting an Island Oasis~ brand of cocktail mixes, the concentrate can, of course, be macle from ot~her fruit and non-fruit aqueous solutions, providing thley have the solid content to fall within the teachings of the present invention and can satisfy the flavor and sweetness reguirements CA 02220~12 1997-12-17 W O96137120 PCTrUS96/06442 inherent in making a selected frozen drink. As noted above, while it is not preferred, the solid content can include high potency sweeteners, gums, glycerol or other sugar alcohols, artificial flavors or color ingredients, preservatives, and other carbohydrate-hA~~~ ingredients. Total solid content considerations must be observed, but the main considerations are the net affect on taste, blendability, and final product texture.
Similarly, while chilled bottled water is a preferred diluent, tap water can be used, but with risks of variation in taste due to the mineral content of the tap water and some small variations in blendability and texture due to he water content and warmer ambient temperature of tap water as compared to chilled bottled water. The alcohol diluent can be any of a wide variety of spirits, and in varying proofs.
More neutral spirits such as rum, gin, vodka and tequila are preferred. Liqueurs could be added for taste or color.
Different bl~n~;ng arrangements also fall within the scope of this invention. While a st~n~Ard home blender i8 preferred, it i8 possible to use food proceQ~ors, food mixers, power stirrers, and even manually powered mechAn;cal blen~;n~ provided that the bl~n~ng implement can break apart the frozen concentrate into a finely divided state while mixing it with the diluent liquid.
These and other variations and modifications are inte~ to fall within the scope of the appen~e~
claims.

Claims

What is claimed is:
1. (Amended) A process for making a slush drink with a generally uniform consistency that peaks and remains a slush while it is consumed comprising freezing a flavor concentrate solution of solids, including sweeteners, in water, said solid content and the temperature of said freezing each having a values such that said flavor concentrate solution is softly frozen, and said flavor concentrate solution having a measured Brix value equivalent in its effect in depressing the freezing point of said flavor concentrate solution to that of a standard disaccharide Brix value in the range of 10° to 25°, adding a liquid diluent wherein the weight/weight ratio of said softly frozen flavor concentrate to say diluent is in the range of 1:1 to 3:1, and strongly mechanically blending the frozen concentrate with said liquid diluent to produce the slush drink.
2. (Cancelled).
3. The slush drink making process of claim 1 wherein said solid content of said flavor concentrate solution has a Brix value in the range of 16° to 22°.
4. The slush drink making process of claim 1 wherein said solid content of said flavor concentrate solution has a Brix value in the range of 18° to 21°.
5. The slush drink making process of claim 1 wherein said freezing temperature is in the range produced in conventional home refrigerator freezer compartments. 6. (Cancelled).
7. The slush drink making process of claim 1 wherein said strongly mechanical blending comprises providing a conventional food blender with a blender cup, placing said frozen flavor concentrate in said blender cup, and operating the blender until the frozen said component of frozen flavor concentrate is of a generally uniform, generally small size.

8. The slush drink making process of claim 1 wherein said liquid diluent is selected from the group consisting of water, a distilled spirit, and a mixture of water and a distilled spirit.
9. The slush drink making process of claim 8 wherein said liquid diluent is a mixture of water and a distilled spirit in a volume ratio in the range of 2:1 to 4:1.
10. The slush drink making process of claim 1 wherein said solid content consists of carbohydrates.
11. The slush drink making process of claim 10 wherein said carbohydrate are selected from the group consisting of sucrose, glucose, fructose, a high-potency sweetener, natural and artificial fruit flavors, fruit: fiber, and combinations of these substances.
12. The slush drink making process of claim 1 wherein the blended slush drink has a Brix value in the range of 11.0° to 13.5°.
13. A liquid frozen cocktail concentrate that can be soft frozen, before use, comprising, a solution of water and a solid content including a flavor ingredient and a sweetener, where said solid content has a Brix value in the range of 16° to 22°.
14. The concentrate of claim 12 wherein said Brix value is in the range of 18° to 21°.
15. The frozen cocktail concentrate of claims 13 or 14 wherein said solid content consists of carbohydrates.
16. The frozen concentrate of claim 15 wherein said carbohydrates are selected from the group consisting of sucrose, glucose, fructose, a high-potency sweetener, sugar alcohol, natural and artificial fruit flavors, fiber, and combinations of these substance.
17. A frozen drink made by the process of claims 1-12.
CA002220512A 1995-05-08 1996-05-08 Frozen cocktails made from a flavor concentrate Abandoned CA2220512A1 (en)

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US20030129282A1 (en) * 2001-08-31 2003-07-10 Solorio Hector A. Frozen drink mixes
AU2003261270A1 (en) * 2002-07-31 2004-02-25 Rich Products Corporation Reduced-calorie freezable beverage
MXPA05010044A (en) 2003-03-20 2006-03-10 Rich Products Corp A non-dairy whippable food product.
CN1787746B (en) 2003-05-14 2011-05-18 里奇产品有限公司 A whippable food product having improved stability
JP5102934B2 (en) * 2004-05-19 2012-12-19 株式会社ロッテ New liquor
GB2414915A (en) * 2004-06-08 2005-12-14 Elizabeth Acton Method and apparatus for making an iced food or drink product
US8181824B2 (en) * 2008-10-15 2012-05-22 The Coca-Cola Company Systems and methods for predilution of sweetener
GB0910624D0 (en) 2009-06-19 2009-08-05 Diageo Great Britain Ltd A slush
US8293299B2 (en) 2009-09-11 2012-10-23 Kraft Foods Global Brands Llc Containers and methods for dispensing multiple doses of a concentrated liquid, and shelf stable Concentrated liquids
CA2847383A1 (en) * 2010-09-01 2013-03-15 Adrian Spiers Method of storing produce and producing a beverage
US11013248B2 (en) 2012-05-25 2021-05-25 Kraft Foods Group Brands Llc Shelf stable, concentrated, liquid flavorings and methods of preparing beverages with the concentrated liquid flavorings
JP6405300B2 (en) * 2013-02-13 2018-10-17 アサヒ飲料株式会社 Method for mitigating sweetness change or color change upon thawing of frozen beverage
ES2579978B2 (en) 2015-02-16 2017-04-07 Smart Spirits, S.L. Alcoholic beverage infuser
FR3063418A1 (en) * 2017-03-06 2018-09-07 Hadrien Durieux NON-ALCOHOLIC FOOD PREPARATION FOR GRANITE OR SORBET WITH GRANITE EFFECT
ES2616284B2 (en) * 2017-03-21 2018-05-23 Smart Spirits, S.L. PERFECTED INFUSOR FOR ALCOHOLIC BEVERAGES

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US3647472A (en) * 1970-05-08 1972-03-07 Gen Mills Inc Beverage mix
US3897571A (en) * 1972-12-04 1975-07-29 Gen Foods Corp Process for producing slush beverage concentrate and product
US4790999A (en) * 1986-10-31 1988-12-13 Heublein, Inc. Alcoholic soft ice

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MX9708526A (en) 1998-08-30

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