CA2059398A1 - Agent d'extraction en phase solide - Google Patents

Agent d'extraction en phase solide

Info

Publication number
CA2059398A1
CA2059398A1 CA2059398A CA2059398A CA2059398A1 CA 2059398 A1 CA2059398 A1 CA 2059398A1 CA 2059398 A CA2059398 A CA 2059398A CA 2059398 A CA2059398 A CA 2059398A CA 2059398 A1 CA2059398 A1 CA 2059398A1
Authority
CA
Canada
Prior art keywords
extraction medium
solid phase
particles
phase extraction
organic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA2059398A
Other languages
English (en)
Other versions
CA2059398C (fr
Inventor
Craig G. Markell
Donald F. Hagen
James D. Luedtke
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Co
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2059398A1 publication Critical patent/CA2059398A1/fr
Application granted granted Critical
Publication of CA2059398C publication Critical patent/CA2059398C/fr
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28028—Particles immobilised within fibres or filaments
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
    • B01D15/1864—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns using two or more columns
    • B01D15/1871—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns using two or more columns placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28033—Membrane, sheet, cloth, pad, lamellar or mat
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28052—Several layers of identical or different sorbents stacked in a housing, e.g. in a column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/36—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving ionic interaction
    • B01D15/361—Ion-exchange
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • G01N30/52—Physical parameters
    • G01N2030/524—Physical parameters structural properties
    • G01N2030/527—Physical parameters structural properties sorbent material in form of a membrane
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • G01N30/52—Physical parameters
    • G01N2030/524—Physical parameters structural properties
    • G01N2030/528—Monolithic sorbent material

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Laminated Bodies (AREA)
CA002059398A 1991-02-07 1992-01-15 Agent d'extraction en phase solide Expired - Fee Related CA2059398C (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US65179191A 1991-02-07 1991-02-07
US07/651,791 1991-02-07

Publications (2)

Publication Number Publication Date
CA2059398A1 true CA2059398A1 (fr) 1992-08-08
CA2059398C CA2059398C (fr) 1999-05-25

Family

ID=24614241

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002059398A Expired - Fee Related CA2059398C (fr) 1991-02-07 1992-01-15 Agent d'extraction en phase solide

Country Status (6)

Country Link
US (1) US5279742A (fr)
EP (1) EP0498557B1 (fr)
JP (1) JP3102593B2 (fr)
KR (1) KR100198010B1 (fr)
CA (1) CA2059398C (fr)
DE (1) DE69209109T2 (fr)

Families Citing this family (56)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5328758A (en) * 1991-10-11 1994-07-12 Minnesota Mining And Manufacturing Company Particle-loaded nonwoven fibrous article for separations and purifications
US5391298B1 (en) * 1993-03-05 1997-10-28 Minnesota Mining & Mfg Method for performing a solid-phase extraction under pressurized conditions
US5403489A (en) * 1993-06-24 1995-04-04 Minnesota Mining And Manufacturing Company Solid phase extraction method and apparatus
DE69412286T2 (de) * 1993-12-22 1998-12-03 Minnesota Mining & Mfg Verwendung von blattförmigen materialien für festphasenextraktionen und festphasenreaktionen
US6207251B1 (en) 1994-01-10 2001-03-27 Minnesota Mining And Manufacturing Company Reinforced particle-loaded fibrillated PTFE web
US5653875A (en) * 1994-02-04 1997-08-05 Supelco, Inc. Nucleophilic bodies bonded to siloxane and use thereof for separations from sample matrices
US5496741A (en) * 1994-04-14 1996-03-05 University Of Waterloo Device and process for increasing analyte concentration in a sorbent
AU2198395A (en) * 1994-05-05 1995-11-29 Minnesota Mining And Manufacturing Company Chemically modified solid phase extraction particles and articles containing same
US5529686A (en) * 1994-07-15 1996-06-25 Minnesota Mining And Manufacturing Company Composite membranes for solid phase extractions and reactions
US5595653A (en) * 1994-07-15 1997-01-21 Cera, Inc. Microcolumn for extraction of analytes from liquids
WO1996014931A1 (fr) * 1994-11-10 1996-05-23 Minnesota Mining And Manufacturing Company Extraction en phase solide avec une feuille composite permettant la mesure directe de la radioactivite
US5472600A (en) * 1995-02-01 1995-12-05 Minnesota Mining And Manufacturing Company Gradient density filter
WO1996029146A1 (fr) 1995-03-22 1996-09-26 Minnesota Mining And Manufacturing Company Membrane d'extraction de phase solide
US5531899A (en) * 1995-06-06 1996-07-02 Millipore Investment Holdings Limited Ion exchange polyethylene membrane and process
DE69627337D1 (de) * 1995-07-14 2003-05-15 Us Environmental Prot Agency W Mit adsorbierendem material gefüllte membranen zur entfernung flüchtiger verbindungen aus abwasser
US5833860A (en) * 1995-08-28 1998-11-10 Millipore Investment Holdings Limited Centrifugal adsorptive sample preparation device and method
US20020115585A1 (en) * 1996-06-07 2002-08-22 Hei Derek J. Method and devices for the removal of psoralens from blood products
AU725939B2 (en) * 1996-07-30 2000-10-26 3M Innovative Properties Company Filter sheet and process for purifying photoresist composition employing the filter sheet
US5911883A (en) * 1996-10-04 1999-06-15 Minnesota Mining And Manufacturing Company Flow-by solid phase extraction method
US20010009756A1 (en) 1998-01-06 2001-07-26 Derek Hei Flow devices for the reduction of compounds from biological compositions and methods of use
US20010018179A1 (en) 1998-01-06 2001-08-30 Derek J. Hei Batch devices for the reduction of compounds from biological compositions containing cells and methods of use
US5897779A (en) * 1997-02-13 1999-04-27 Minnesota Mining And Manufacturing Company Spiral wound extraction cartridge
US6998047B1 (en) 1997-02-26 2006-02-14 Millipore Corporation Cast membrane structures for sample preparation
US7611831B2 (en) * 1998-01-06 2009-11-03 Cerus Corporation Adsorbing pathogen-inactivating compounds with porous particles immobilized in a matrix
US6492183B1 (en) 1998-09-14 2002-12-10 3M Innovative Properties Company Extraction articles and methods
EP1033572A4 (fr) * 1998-09-18 2001-02-07 Eisai Co Ltd Colonne pour concentrer un composant dans un echantillon
US6071410A (en) * 1998-11-16 2000-06-06 Varian, Inc. Recovery of organic solutes from aqueous solutions
GB9920170D0 (en) * 1999-08-25 1999-10-27 Univ Portsmouth A passive sampling device
US6383783B1 (en) 1999-09-21 2002-05-07 3M Innovative Properties Company Nucleic acid isolation by adhering to hydrophobic solid phase and removing with nonionic surfactant
US6602414B2 (en) * 2000-03-30 2003-08-05 Formulations Pro Molecule separation device and method combining multiple filtration media
US20020034827A1 (en) * 2000-08-01 2002-03-21 Rajendra Singh Methods for solid phase nanoextraction and desorption
US7300801B2 (en) * 2003-09-12 2007-11-27 3M Innovative Properties Company Welded sample preparation articles and methods
US20060115383A1 (en) * 2003-09-16 2006-06-01 Vici Gig Harbor Group, Inc. Flow through well plate surface sorption extarction
US20060115384A1 (en) * 2003-09-16 2006-06-01 Vici Gig Harbor Group, Inc. Pipette tip surface sorption extraction
US7087437B2 (en) * 2003-09-16 2006-08-08 Vici Gig Harbor Group, Inc. Direct vial surface sorbent micro extraction device and method
US20060110295A1 (en) * 2003-09-16 2006-05-25 Vici Gig Harbor Group, Inc. Closed well plate surface sorption extraction
US20050130177A1 (en) * 2003-12-12 2005-06-16 3M Innovative Properties Company Variable valve apparatus and methods
US20050142571A1 (en) * 2003-12-24 2005-06-30 3M Innovative Properties Company Methods for nucleic acid isolation and kits using solid phase material
US7939249B2 (en) * 2003-12-24 2011-05-10 3M Innovative Properties Company Methods for nucleic acid isolation and kits using a microfluidic device and concentration step
US7727710B2 (en) * 2003-12-24 2010-06-01 3M Innovative Properties Company Materials, methods, and kits for reducing nonspecific binding of molecules to a surface
US7452412B2 (en) * 2004-08-24 2008-11-18 Midwest Research Institute, Inc. High-efficiency filter device and method for making same
KR20070057266A (ko) * 2004-10-01 2007-06-04 쓰리엠 이노베이티브 프로퍼티즈 컴파니 복합 여과 제품
US7311825B2 (en) 2005-05-02 2007-12-25 Varian, Inc. Polymer modified porous substrate for solid phase extraction
US20070102358A1 (en) * 2005-11-09 2007-05-10 Cera Inc. Solid phase extraction column
US20070272606A1 (en) * 2006-05-25 2007-11-29 Freese Donald T Multi-functional coatings on microporous substrates
JP5410971B2 (ja) 2006-07-21 2014-02-05 アムジエン・インコーポレーテツド サンプル中のヘプシジンを検出および／または測定する方法
WO2008134470A2 (fr) * 2007-04-25 2008-11-06 3M Innovative Properties Company Procédés d'amplification d'acides nucléiques
WO2009032293A1 (fr) * 2007-09-06 2009-03-12 Waters Investments Limited Procédés de séparation de macromolécules fonctionnalisées
CN102933296A (zh) * 2010-06-08 2013-02-13 3M创新有限公司 固相萃取介质
US9056316B2 (en) 2010-06-25 2015-06-16 3M Innovative Properties Company Semi-interpenetrating polymer network
EP2532421A1 (fr) * 2011-06-10 2012-12-12 Süd-Chemie AG Matériau composite en polymère contenant du fluor, particules de zéolithe hydrophobes et matière première métallique
CN102350327A (zh) * 2011-08-12 2012-02-15 天津博纳艾杰尔科技有限公司 新型亲水c18填料及其固相萃取柱
WO2013158858A1 (fr) 2012-04-19 2013-10-24 New Objective, Inc. Préparation d'échantillon et spectrométrie de masse à ionisation par nano-électronébulisation
US10453664B2 (en) 2015-04-21 2019-10-22 Battelle Memorial Institute Collection, release, and detection of analytes with polymer composite sampling materials
US10254248B2 (en) 2015-04-21 2019-04-09 Battelle Memorial Institute Collection, release, and detection of analytes with polymer composite sampling materials
CA3034049A1 (fr) * 2016-10-28 2018-05-03 Preomics Gmbh Prevention de flux a base d'hydrophobicite dans la preparation d'echantillons

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4153661A (en) * 1977-08-25 1979-05-08 Minnesota Mining And Manufacturing Company Method of making polytetrafluoroethylene composite sheet
US4208194A (en) * 1977-09-26 1980-06-17 Minnesota Mining And Manufacturing Company Monitoring device
ZA793272B (en) * 1978-07-07 1980-07-30 M Klein Adsorption and filtration mat for liquids
US4460642A (en) * 1981-06-26 1984-07-17 Minnesota Mining And Manufacturing Company Water-swellable composite sheet of microfibers of PTFE and hydrophilic absorptive particles
US4373519A (en) * 1981-06-26 1983-02-15 Minnesota Mining And Manufacturing Company Composite wound dressing
US4565663A (en) * 1981-06-26 1986-01-21 Minnesota Mining And Manufacturing Company Method for making water-swellable composite sheet
US4512897A (en) * 1981-07-28 1985-04-23 Amf Incorporated Molecular separation column and use thereof
US4722898A (en) * 1985-04-29 1988-02-02 Minnesota Mining And Manufacturing Company Immobilization of biological cells in polytetrafluoroethylene matrix
US4871671A (en) * 1985-04-29 1989-10-03 Minnesota Mining And Manufacturing Company Immobilization of biological cells in polytetrafluoroethylene matrix
US5009869A (en) * 1987-12-28 1991-04-23 Electrocinerator Technologies, Inc. Methods for purification of air
US4971736A (en) * 1987-12-28 1990-11-20 Minnesota Mining And Manufacturing Company Method of preparing composite chromatographic article
US4810381A (en) * 1987-12-28 1989-03-07 Minnesota Mining And Manufacturing Company Composite chromatographic article
US4906378A (en) * 1987-12-28 1990-03-06 Minnesota Mining And Manufacturing Company Composite chromatographic article
US4971697A (en) * 1989-02-23 1990-11-20 Minnesota Mining And Manufacturing Company Thin silica flakes and method of making
US4935142A (en) * 1989-06-23 1990-06-19 Memtek Corporation Apparatus for retaining variable number of sheet membrane elements and a method for the use thereof
US5019232A (en) * 1990-06-01 1991-05-28 Minnesota Mining And Manufacturing Company Medium for electrophoresis

Also Published As

Publication number Publication date
JP3102593B2 (ja) 2000-10-23
US5279742A (en) 1994-01-18
KR100198010B1 (ko) 1999-06-15
DE69209109T2 (de) 1996-11-07
CA2059398C (fr) 1999-05-25
JPH04334546A (ja) 1992-11-20
KR920016123A (ko) 1992-09-24
DE69209109D1 (de) 1996-04-25
EP0498557B1 (fr) 1996-03-20
EP0498557A1 (fr) 1992-08-12

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