CA1326755C - Process for concentrating sulphuric acid - Google Patents
Process for concentrating sulphuric acidInfo
- Publication number
- CA1326755C CA1326755C CA000547576A CA547576A CA1326755C CA 1326755 C CA1326755 C CA 1326755C CA 000547576 A CA000547576 A CA 000547576A CA 547576 A CA547576 A CA 547576A CA 1326755 C CA1326755 C CA 1326755C
- Authority
- CA
- Canada
- Prior art keywords
- sulphuric acid
- evaporator
- evaporation
- acid
- heated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title claims abstract description 40
- 235000011149 sulphuric acid Nutrition 0.000 title claims abstract description 40
- 239000001117 sulphuric acid Substances 0.000 title claims abstract description 32
- 238000000034 method Methods 0.000 title claims abstract description 28
- 230000008569 process Effects 0.000 title claims abstract description 26
- 238000001704 evaporation Methods 0.000 claims abstract description 31
- 230000008020 evaporation Effects 0.000 claims abstract description 30
- 230000004087 circulation Effects 0.000 claims abstract description 16
- 239000011552 falling film Substances 0.000 claims abstract description 7
- 229910052715 tantalum Inorganic materials 0.000 claims description 9
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims description 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 229910002804 graphite Inorganic materials 0.000 claims description 6
- 239000010439 graphite Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000004809 Teflon Substances 0.000 claims description 4
- 229920006362 Teflon® Polymers 0.000 claims description 4
- 238000009835 boiling Methods 0.000 claims description 3
- 239000002253 acid Substances 0.000 description 32
- 150000002500 ions Chemical class 0.000 description 11
- 239000000498 cooling water Substances 0.000 description 10
- 241000196324 Embryophyta Species 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 238000001816 cooling Methods 0.000 description 6
- 239000000446 fuel Substances 0.000 description 4
- 244000046052 Phaseolus vulgaris Species 0.000 description 2
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 239000002826 coolant Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 238000004094 preconcentration Methods 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 101100109406 Neurospora crassa (strain ATCC 24698 / 74-OR23-1A / CBS 708.71 / DSM 1257 / FGSC 987) aga-1 gene Proteins 0.000 description 1
- RSPISYXLHRIGJD-UHFFFAOYSA-N OOOO Chemical compound OOOO RSPISYXLHRIGJD-UHFFFAOYSA-N 0.000 description 1
- 241001425800 Pipa Species 0.000 description 1
- 241001208007 Procas Species 0.000 description 1
- 244000166490 Tetrameles nudiflora Species 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229940037003 alum Drugs 0.000 description 1
- CEJLBZWIKQJOAT-UHFFFAOYSA-N dichloroisocyanuric acid Chemical compound ClN1C(=O)NC(=O)N(Cl)C1=O CEJLBZWIKQJOAT-UHFFFAOYSA-N 0.000 description 1
- 239000010408 film Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/88—Concentration of sulfuric acid
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEP3632623.2 | 1986-09-25 | ||
| DE19863632623 DE3632623A1 (de) | 1986-09-25 | 1986-09-25 | Verfahren zum aufkonzentrieren von schwefelsaeure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1326755C true CA1326755C (en) | 1994-02-08 |
Family
ID=6310346
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000547576A Expired - Fee Related CA1326755C (en) | 1986-09-25 | 1987-09-23 | Process for concentrating sulphuric acid |
Country Status (4)
| Country | Link |
|---|---|
| EP (1) | EP0262510B1 (enrdf_load_stackoverflow) |
| JP (1) | JPS6389410A (enrdf_load_stackoverflow) |
| CA (1) | CA1326755C (enrdf_load_stackoverflow) |
| DE (2) | DE3632623A1 (enrdf_load_stackoverflow) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3935892C2 (de) * | 1989-10-27 | 1994-08-25 | Metallgesellschaft Ag | Verfahren und Vorrichtung zum Konzentrieren einer Schwefelsäure und Wasser enthaltenden Flüssigkeit |
| DE3938915C1 (enrdf_load_stackoverflow) * | 1989-11-24 | 1991-05-08 | Bayer Ag, 5090 Leverkusen, De | |
| DE4029737C1 (enrdf_load_stackoverflow) * | 1990-09-20 | 1991-12-05 | Metallgesellschaft Ag, 6000 Frankfurt, De | |
| DE4114334A1 (de) * | 1991-05-02 | 1992-11-05 | Buss Ag | Duennschichtverdampfer aus korrosionsbestaendigem material |
| DE19741511A1 (de) * | 1997-09-20 | 1999-04-01 | Metallgesellschaft Ag | Verfahren zur Aufkonzentrierung von Dünnsäure durch Ausnutzung von Prozeßwärme in einer Zwangsumlaufverdampferanlage |
| DE19963509A1 (de) * | 1999-12-28 | 2001-07-05 | Merck Patent Gmbh | Verfahren zur Herstellung hochreiner Schwefelsäure |
| WO2008003297A2 (de) * | 2006-07-03 | 2008-01-10 | Lailach Guenter | Verfahren und anlage zum konzentrieren metallsulfathaltiger schwefelsäure |
| CN101935077B (zh) * | 2010-08-27 | 2012-06-20 | 南通京通石墨设备有限公司 | 废酸浓缩多级处理方法 |
| JP6001328B2 (ja) * | 2012-05-23 | 2016-10-05 | パンパシフィック・カッパー株式会社 | 硫酸酸性液の濃縮装置、硫酸酸性液の濃縮方法及び粗硫酸ニッケルの回収方法 |
| CN106477531B (zh) * | 2016-12-01 | 2018-08-21 | 上海佳麟泵阀有限公司 | 防止运行时产生电化学腐蚀的废硫酸浓缩回收装置 |
| US20230117014A1 (en) * | 2020-03-16 | 2023-04-20 | Dupont Safety & Construction, Inc. | Concentration of sulfuric acid |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3015957A1 (de) * | 1980-04-25 | 1981-11-05 | Hoechst Ag, 6000 Frankfurt | Verfahren und vorrichtung zur konzentrierung und reinigung von abfallschwefelsaeure |
| DE3409717C2 (de) * | 1984-03-16 | 1994-03-31 | Bayer Ag | Verfahren zur Herstellung von Nitrobenzol |
-
1986
- 1986-09-25 DE DE19863632623 patent/DE3632623A1/de not_active Withdrawn
-
1987
- 1987-09-16 EP EP19870113514 patent/EP0262510B1/de not_active Expired - Lifetime
- 1987-09-16 DE DE8787113514T patent/DE3774821D1/de not_active Expired - Lifetime
- 1987-09-23 CA CA000547576A patent/CA1326755C/en not_active Expired - Fee Related
- 1987-09-25 JP JP23907287A patent/JPS6389410A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6389410A (ja) | 1988-04-20 |
| EP0262510B1 (de) | 1991-11-27 |
| EP0262510A3 (en) | 1988-10-19 |
| DE3632623A1 (de) | 1988-03-31 |
| JPH0476326B2 (enrdf_load_stackoverflow) | 1992-12-03 |
| EP0262510A2 (de) | 1988-04-06 |
| DE3774821D1 (de) | 1992-01-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKLA | Lapsed |