CA1282943C - Fiber-reinforced ceramic and process therefor - Google Patents
Fiber-reinforced ceramic and process thereforInfo
- Publication number
- CA1282943C CA1282943C CA000498957A CA498957A CA1282943C CA 1282943 C CA1282943 C CA 1282943C CA 000498957 A CA000498957 A CA 000498957A CA 498957 A CA498957 A CA 498957A CA 1282943 C CA1282943 C CA 1282943C
- Authority
- CA
- Canada
- Prior art keywords
- silicon
- composite
- array
- process according
- fibers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000034 method Methods 0.000 title claims description 27
- 230000008569 process Effects 0.000 title claims description 23
- 239000011226 reinforced ceramic Substances 0.000 title description 2
- 239000002131 composite material Substances 0.000 claims abstract description 78
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 38
- 229910052581 Si3N4 Inorganic materials 0.000 claims abstract description 35
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 claims abstract description 34
- 229910010271 silicon carbide Inorganic materials 0.000 claims abstract description 34
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 claims abstract description 31
- 239000000919 ceramic Substances 0.000 claims abstract description 22
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 22
- 239000010703 silicon Substances 0.000 claims abstract description 22
- 238000006243 chemical reaction Methods 0.000 claims abstract description 11
- 239000011863 silicon-based powder Substances 0.000 claims abstract description 10
- 238000002844 melting Methods 0.000 claims abstract description 6
- 230000008018 melting Effects 0.000 claims abstract description 6
- 239000012298 atmosphere Substances 0.000 claims description 9
- 238000010438 heat treatment Methods 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 239000000126 substance Substances 0.000 claims description 8
- 230000001427 coherent effect Effects 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 5
- 239000011261 inert gas Substances 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 3
- 239000012299 nitrogen atmosphere Substances 0.000 claims description 3
- 230000006835 compression Effects 0.000 claims 2
- 238000007906 compression Methods 0.000 claims 2
- 229920000620 organic polymer Polymers 0.000 claims 2
- 239000011174 green composite Substances 0.000 claims 1
- 239000000835 fiber Substances 0.000 abstract description 74
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 16
- 229910001873 dinitrogen Inorganic materials 0.000 abstract description 8
- 238000003825 pressing Methods 0.000 abstract description 6
- 230000003014 reinforcing effect Effects 0.000 abstract description 5
- 238000005452 bending Methods 0.000 abstract description 3
- 230000002349 favourable effect Effects 0.000 abstract 1
- 239000011159 matrix material Substances 0.000 description 26
- 239000000843 powder Substances 0.000 description 12
- 230000035882 stress Effects 0.000 description 11
- 239000000463 material Substances 0.000 description 10
- 238000012360 testing method Methods 0.000 description 10
- 238000005121 nitriding Methods 0.000 description 7
- -1 poly(vinylbutyral) Polymers 0.000 description 7
- 239000002002 slurry Substances 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
- 238000010586 diagram Methods 0.000 description 5
- 239000011888 foil Substances 0.000 description 5
- 239000010410 layer Substances 0.000 description 5
- 229920000642 polymer Polymers 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 239000004698 Polyethylene Substances 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 4
- 238000000576 coating method Methods 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 4
- 229920000573 polyethylene Polymers 0.000 description 4
- 230000035939 shock Effects 0.000 description 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- 238000003491 array Methods 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 229920005596 polymer binder Polymers 0.000 description 3
- 239000002491 polymer binding agent Substances 0.000 description 3
- 230000002787 reinforcement Effects 0.000 description 3
- 239000012783 reinforcing fiber Substances 0.000 description 3
- 230000000717 retained effect Effects 0.000 description 3
- IRIAEXORFWYRCZ-UHFFFAOYSA-N Butylbenzyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCC1=CC=CC=C1 IRIAEXORFWYRCZ-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 238000007792 addition Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000006073 displacement reaction Methods 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 description 2
- 238000007731 hot pressing Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002356 single layer Substances 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 239000002344 surface layer Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 241000422980 Marietta Species 0.000 description 1
- 206010037660 Pyrexia Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 125000006487 butyl benzyl group Chemical group 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 229960000541 cetyl alcohol Drugs 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000011222 crystalline ceramic Substances 0.000 description 1
- 229910002106 crystalline ceramic Inorganic materials 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000000280 densification Methods 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 230000005489 elastic deformation Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000003733 fiber-reinforced composite Substances 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 238000007676 flexural strength test Methods 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000002905 metal composite material Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 238000013001 point bending Methods 0.000 description 1
- 229920003257 polycarbosilane Polymers 0.000 description 1
- 229920002959 polymer blend Polymers 0.000 description 1
- 229920002689 polyvinyl acetate Polymers 0.000 description 1
- 239000011118 polyvinyl acetate Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 150000002910 rare earth metals Chemical class 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000012779 reinforcing material Substances 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 150000003377 silicon compounds Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 230000008646 thermal stress Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000003826 uniaxial pressing Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/515—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
- C04B35/58—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides
- C04B35/584—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on silicon nitride
- C04B35/591—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on borides, nitrides, i.e. nitrides, oxynitrides, carbonitrides or oxycarbonitrides or silicides based on silicon nitride obtained by reaction sintering
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/71—Ceramic products containing macroscopic reinforcing agents
- C04B35/78—Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
- C04B35/80—Fibres, filaments, whiskers, platelets, or the like
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Products (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US69244185A | 1985-01-17 | 1985-01-17 | |
| US692,441 | 1985-01-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1282943C true CA1282943C (en) | 1991-04-16 |
Family
ID=24780597
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000498957A Expired - Fee Related CA1282943C (en) | 1985-01-17 | 1986-01-03 | Fiber-reinforced ceramic and process therefor |
Country Status (4)
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4869943A (en) * | 1985-01-17 | 1989-09-26 | Norton Company | Fiber-reinforced silicon nitride ceramics |
| JPS61209975A (ja) * | 1985-03-14 | 1986-09-18 | 株式会社豊田中央研究所 | 炭化珪素セラミツクス体の強化方法 |
| DE3786105T2 (de) * | 1986-03-17 | 1993-09-16 | Sumitomo Electric Industries | Kompakter keramischer koerper, insbesondere auf basis von siliciumnitrid und keramischen fasern und sein herstellungsverfahren. |
| ATE42267T1 (de) * | 1986-11-25 | 1989-05-15 | Battelle Memorial Institute | Zusammensetzung von pulverigem siliziumnitrid, verstaerkt mit siliziumcarbid-whiskern, und verwendung derselben zur herstellung von sinterkoerpern. |
| FR2607130B1 (fr) * | 1986-11-26 | 1992-12-18 | Norton Co | Ceramiques composites de nitrure de silicium a renforcement fibreux |
| GB8828638D0 (en) * | 1988-12-08 | 1989-01-11 | Ici Plc | Production of fibre reinforced composite |
| US4970057A (en) * | 1989-04-28 | 1990-11-13 | Norton Company | Silicon nitride vacuum furnace process |
| JPH035386A (ja) * | 1989-05-31 | 1991-01-11 | Sumitomo Electric Ind Ltd | 高密度繊維強化複合材料の製造方法 |
| US5202158A (en) * | 1989-05-31 | 1993-04-13 | Sumitomo Electric Industries, Ltd. | Apparatus for and method of producing high density fiber reinforced composite material |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5833196B2 (ja) * | 1975-10-27 | 1983-07-18 | トウホクダイガクキンゾクザイリヨウケンキユウシヨチヨウ | タイネツセイセラミツクスフクゴウザイリヨウノセイゾウホウホウ |
| JPS54112909A (en) * | 1978-02-24 | 1979-09-04 | Kawasaki Heavy Ind Ltd | Silicon carbide composite material |
| US4324843A (en) * | 1980-02-13 | 1982-04-13 | United Technologies Corporation | Continuous length silicon carbide fiber reinforced ceramic composites |
| JPS5855380A (ja) * | 1981-09-24 | 1983-04-01 | 日本特殊陶業株式会社 | 繊維強化ＳｉＣ焼結体の製造方法 |
| JPS5891073A (ja) * | 1981-11-26 | 1983-05-30 | 旭硝子株式会社 | 窒化珪素質セラミツクス |
| FR2546441B1 (fr) * | 1983-05-25 | 1987-05-15 | Ceraver | Procede de fabrication d'une structure composite renforcee en matiere ceramique |
-
1986
- 1986-01-03 CA CA000498957A patent/CA1282943C/en not_active Expired - Fee Related
- 1986-01-14 EP EP86100406A patent/EP0188270B1/en not_active Expired
- 1986-01-14 DE DE8686100406T patent/DE3685660T2/de not_active Expired - Fee Related
- 1986-01-17 JP JP61007792A patent/JPS61227969A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| DE3685660T2 (de) | 1993-01-07 |
| EP0188270A2 (en) | 1986-07-23 |
| EP0188270A3 (en) | 1987-02-04 |
| JPH042544B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1992-01-20 |
| DE3685660D1 (de) | 1992-07-23 |
| EP0188270B1 (en) | 1992-06-17 |
| JPS61227969A (ja) | 1986-10-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKLA | Lapsed |