CA1266386A - Apparatus and process for pyrolysis and analysis of samples containing organic matter - Google Patents
Apparatus and process for pyrolysis and analysis of samples containing organic matterInfo
- Publication number
- CA1266386A CA1266386A CA000505356A CA505356A CA1266386A CA 1266386 A CA1266386 A CA 1266386A CA 000505356 A CA000505356 A CA 000505356A CA 505356 A CA505356 A CA 505356A CA 1266386 A CA1266386 A CA 1266386A
- Authority
- CA
- Canada
- Prior art keywords
- cartridge
- sample
- heating
- arm
- heating means
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000004458 analytical method Methods 0.000 title claims abstract description 38
- 239000005416 organic matter Substances 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 title claims description 16
- 238000000197 pyrolysis Methods 0.000 title claims description 11
- 239000007789 gas Substances 0.000 claims abstract description 22
- 239000012159 carrier gas Substances 0.000 claims abstract description 19
- 239000001257 hydrogen Substances 0.000 claims abstract description 8
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 8
- 238000010438 heat treatment Methods 0.000 claims description 78
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 12
- 239000008246 gaseous mixture Substances 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 9
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 6
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims description 4
- 239000004020 conductor Substances 0.000 claims description 4
- 239000012530 fluid Substances 0.000 claims description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 3
- 239000001569 carbon dioxide Substances 0.000 claims description 3
- 229910001882 dioxygen Inorganic materials 0.000 claims description 3
- 238000004891 communication Methods 0.000 claims description 2
- 238000007327 hydrogenolysis reaction Methods 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- 229910010293 ceramic material Inorganic materials 0.000 claims 2
- 239000000112 cooling gas Substances 0.000 claims 2
- 239000011435 rock Substances 0.000 abstract description 15
- 238000005553 drilling Methods 0.000 abstract description 6
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 229940090045 cartridge Drugs 0.000 description 56
- 239000000523 sample Substances 0.000 description 42
- 229930195733 hydrocarbon Natural products 0.000 description 8
- 150000002430 hydrocarbons Chemical class 0.000 description 8
- 239000002245 particle Substances 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000006227 byproduct Substances 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000001307 helium Substances 0.000 description 2
- 229910052734 helium Inorganic materials 0.000 description 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000000567 combustion gas Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000004035 construction material Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 238000002124 flame ionisation detection Methods 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/12—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using combustion
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/21—Hydrocarbon
- Y10T436/218—Total hydrocarbon, flammability, combustibility [e.g., air-fuel mixture, etc.]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/23—Carbon containing
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Combustion & Propulsion (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8505308A FR2580078B1 (enrdf_load_stackoverflow) | 1985-04-05 | 1985-04-05 | |
| FR8505308 | 1985-04-05 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1266386A true CA1266386A (en) | 1990-03-06 |
Family
ID=9318052
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000505356A Expired - Fee Related CA1266386A (en) | 1985-04-05 | 1986-03-27 | Apparatus and process for pyrolysis and analysis of samples containing organic matter |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4798805A (enrdf_load_stackoverflow) |
| CA (1) | CA1266386A (enrdf_load_stackoverflow) |
| FR (1) | FR2580078B1 (enrdf_load_stackoverflow) |
| GB (1) | GB2173305B (enrdf_load_stackoverflow) |
| IT (1) | IT1188636B (enrdf_load_stackoverflow) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2607255B1 (fr) * | 1986-11-25 | 1989-09-29 | Inst Francais Du Petrole | Procede et dispositif de determination de la quantite d'au moins un element choisi parmi le carbone, l'hydrogene, le soufre et l'azote d'au moins deux fractions d'un echantillon de matiere organique |
| US4999162A (en) * | 1988-08-26 | 1991-03-12 | Varian Associates, Inc. | High temperature flame jet for gas chromatography |
| US5241868A (en) * | 1992-01-30 | 1993-09-07 | Baker Hughes Incorporated | Sample dispersing apparatus and method for use with a pyrolisis furnace |
| US5315885A (en) * | 1992-01-30 | 1994-05-31 | Baker Hughes Incorporated | Sample dispersing apparatus and method |
| FR2739694B1 (fr) * | 1995-10-05 | 1997-11-14 | Inst Francais Du Petrole | Methode et dispositif pour determiner des caracteristiques petrolieres de sediments geologiques |
| US5866072A (en) * | 1996-02-26 | 1999-02-02 | Cds Analytical, Inc. | Analytical pyrolysis autosampler |
| US20050250209A1 (en) * | 2004-04-21 | 2005-11-10 | Petroleum Habitats, Llc | Determining metal content of source rock during well logging |
| US7153688B2 (en) * | 2004-12-07 | 2006-12-26 | Petroleum Habitats, L.L.C | Rock assay for predicting oil or gas in target reservoirs |
| WO2007082179A2 (en) * | 2006-01-06 | 2007-07-19 | Mango Frank D | In situ conversion of heavy hydrocarbons to catalytic gas |
| WO2008085560A1 (en) * | 2007-01-08 | 2008-07-17 | Mango Frank D | In situ conversion of heavy hydrocarbons to catalytic gas |
| EP2122460B1 (en) * | 2007-02-16 | 2016-02-10 | Saudi Arabian Oil Company | Method for determining volume of organic matter in reservoir rock |
| SG183177A1 (en) * | 2010-02-26 | 2012-09-27 | Perkinelmer Health Sci Inc | Jet assembly for use in detectors and other devices |
| US8727006B2 (en) | 2010-05-04 | 2014-05-20 | Petroleum Habitats, Llc | Detecting and remedying hydrogen starvation of catalytic hydrocarbon generation reactions in earthen formations |
| US20160177711A1 (en) * | 2014-12-17 | 2016-06-23 | Geolog Srl | Method and relative system for the measurement of the isotope ratio in hydrocarbons |
| KR20180114898A (ko) * | 2015-12-29 | 2018-10-19 | 토탈 라피나쥬 쉬미 | 산화성 화합물 중 산소의 검출 및 정량화 방법 |
| IL254906B (en) * | 2017-10-06 | 2021-12-01 | Mery Reuven | Device and method for burning flammable gas released from a gas chromatograph |
| KR102180627B1 (ko) * | 2017-12-04 | 2020-11-18 | 주식회사 엘지화학 | 자동화된 시료 열분해 장치 |
| US11714029B2 (en) | 2020-03-27 | 2023-08-01 | Saudi Arabian Oil Company | Core holder for real-time measurement and visualization |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3296435A (en) * | 1964-07-06 | 1967-01-03 | Dow Chemical Co | Method and apparatus for determining the total carbon content of aqueous systems |
| US3753654A (en) * | 1971-07-14 | 1973-08-21 | Shell Oil Co | Method for determining organic materials in water |
| FR2227797A5 (enrdf_load_stackoverflow) * | 1973-04-27 | 1974-11-22 | Inst Francais Du Petrole | |
| DE2442346C3 (de) * | 1974-09-04 | 1978-09-21 | Bayer Ag, 5090 Leverkusen | Verfahren und Vorrichtung zur Bestimmung von Quecksilber-Spuren in Flüssigkeiten |
| US3972682A (en) * | 1975-10-06 | 1976-08-03 | Envirotech Corporation | Pyrolysis furnace |
| DE2701782C2 (de) * | 1976-01-20 | 1987-05-14 | Institut Français du Pétrole, Rueil-Malmaison, Hauts-de-Seine | Vorrichtung zur Ermittlung von Erdöleigenschaften geologischer Sedimente |
| US3985509A (en) * | 1976-02-13 | 1976-10-12 | Varian Associates | Flame ionization detector with flame monitor |
| PL108573B1 (en) * | 1976-12-08 | 1980-04-30 | Wojskowy Inst Chem Radiomet | Burner of a detector offlame-photometric gaschromatographic apparatus |
| FR2376414A1 (fr) * | 1976-12-30 | 1978-07-28 | Inst Francais Du Petrole | Methode et dispositif d'analyse de sediments geologiques, permettant notamment de determiner leur teneur en soufre organique |
| US4116632A (en) * | 1977-05-31 | 1978-09-26 | Packard Instrument Company, Inc. | Countercurrent combustion system for preparing radioactive samples and the like |
| US4244917A (en) * | 1979-05-09 | 1981-01-13 | Conoco, Inc. | Sample pyrolysis oven |
| FR2472754A1 (fr) * | 1979-12-28 | 1981-07-03 | Inst Francais Du Petrole | Methode et dispositif pour determiner notamment la quantite de carbone organique contenue dans un echantillon |
| US4462963A (en) * | 1982-03-05 | 1984-07-31 | Leco Corporation | Analytical furnace |
| US4518699A (en) * | 1982-07-06 | 1985-05-21 | The Babcock & Wilcox Company | On-line coal analyzer |
-
1985
- 1985-04-05 FR FR8505308A patent/FR2580078B1/fr not_active Expired
-
1986
- 1986-03-24 GB GB8607281A patent/GB2173305B/en not_active Expired
- 1986-03-27 IT IT19911/86A patent/IT1188636B/it active
- 1986-03-27 CA CA000505356A patent/CA1266386A/en not_active Expired - Fee Related
- 1986-03-28 US US06/845,684 patent/US4798805A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| IT8619911A1 (it) | 1987-09-27 |
| GB8607281D0 (en) | 1986-04-30 |
| FR2580078B1 (enrdf_load_stackoverflow) | 1988-05-27 |
| GB2173305B (en) | 1989-07-05 |
| GB2173305A (en) | 1986-10-08 |
| FR2580078A1 (enrdf_load_stackoverflow) | 1986-10-10 |
| IT8619911A0 (it) | 1986-03-27 |
| IT1188636B (it) | 1988-01-20 |
| US4798805A (en) | 1989-01-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CA1266386A (en) | Apparatus and process for pyrolysis and analysis of samples containing organic matter | |
| US4680167A (en) | Controlled atmosphere oven | |
| US4409336A (en) | Method of analysis for determining very low sulfur levels in volatilizable samples | |
| US2809100A (en) | Combustion analyzer | |
| DK150999B (da) | Fremgangsmaade til bestemmelse af organisk bundet svovl i en lille proeveaf geologiske sedimenter | |
| US3694157A (en) | Method of and apparatus for forming gaseous analysis products from solid samples | |
| Dennis et al. | The effects of welding parameters on ultraviolet light emissions, ozone and CrVI formation in MIG welding | |
| NO853294L (no) | Apparat for maaling av varmeverdien av en brenngass. | |
| US5246667A (en) | Analytical furnace | |
| JPH02201156A (ja) | ガスクロマトグラフィー用熱分解装置 | |
| Lundgren et al. | A temperature-controlled graphite tube furnace for the determination of trace metals in solid biological tissue | |
| US3574549A (en) | Microanalyzer for thermal studies | |
| US3095278A (en) | Gas analysis device | |
| US4411524A (en) | Apparatus for the spectrometric analysis of the chemical composition of metallic parts | |
| US4637735A (en) | Bench-scale material flammability test apparatus and process for measuring flammability | |
| US5408316A (en) | Arrangement for electrothermally atomizing specimens to be analyzed | |
| US4784833A (en) | Apparatus for determining chemical structure | |
| JP4849010B2 (ja) | 分析用試料の燃焼方法 | |
| JP2008298608A (ja) | 分析用試料の燃焼方法 | |
| JPH1164319A (ja) | 元素分析装置 | |
| Grimbley et al. | An enclosed Curie point pyrolysis-GC technique for studying the oxidative or thermal degradation of polymers and volatile oligomeric oils | |
| US2885555A (en) | Combustibles detector | |
| Forsyth | Design and evaluation of a capillary gas chromatography-atomic absorption spectrometer interface | |
| JP2000321265A (ja) | 元素分析装置 | |
| Indrijarso et al. | Thermogravimetric studies of systems pertinent to the in-situ combustion process for enhanced oil recovery. Part 1. Development of a high-pressure thermobalance |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKLA | Lapsed |