CA1180677A - Bath and process for high speed nickel electroplating - Google Patents
Bath and process for high speed nickel electroplatingInfo
- Publication number
- CA1180677A CA1180677A CA000386693A CA386693A CA1180677A CA 1180677 A CA1180677 A CA 1180677A CA 000386693 A CA000386693 A CA 000386693A CA 386693 A CA386693 A CA 386693A CA 1180677 A CA1180677 A CA 1180677A
- Authority
- CA
- Canada
- Prior art keywords
- nickel
- bath
- electroplating bath
- acid
- anodes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims abstract description 37
- 238000009713 electroplating Methods 0.000 title claims abstract description 21
- 229910052759 nickel Inorganic materials 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 title claims description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000004327 boric acid Substances 0.000 claims abstract description 8
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000003792 electrolyte Substances 0.000 claims abstract description 6
- 239000000080 wetting agent Substances 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims abstract description 5
- 229910052700 potassium Inorganic materials 0.000 claims abstract description 5
- 239000011591 potassium Substances 0.000 claims abstract description 5
- -1 potassium perfluoroalkyl sulfonates Chemical class 0.000 claims abstract description 5
- SHHKMWMIKILKQW-UHFFFAOYSA-N 2-formylbenzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1C=O SHHKMWMIKILKQW-UHFFFAOYSA-N 0.000 claims abstract description 4
- 150000002815 nickel Chemical class 0.000 claims abstract description 4
- 238000004070 electrodeposition Methods 0.000 claims abstract description 3
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical group [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 claims description 3
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 claims description 3
- 239000000758 substrate Substances 0.000 claims description 2
- 125000005619 boric acid group Chemical group 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 3
- 229910000008 nickel(II) carbonate Inorganic materials 0.000 description 3
- ZULUUIKRFGGGTL-UHFFFAOYSA-L nickel(ii) carbonate Chemical compound [Ni+2].[O-]C([O-])=O ZULUUIKRFGGGTL-UHFFFAOYSA-L 0.000 description 3
- 229960003975 potassium Drugs 0.000 description 3
- 239000010936 titanium Substances 0.000 description 3
- 229910052719 titanium Inorganic materials 0.000 description 3
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000010955 niobium Substances 0.000 description 2
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 2
- 239000006259 organic additive Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- UPPLJLAHMKABPR-UHFFFAOYSA-H 2-hydroxypropane-1,2,3-tricarboxylate;nickel(2+) Chemical compound [Ni+2].[Ni+2].[Ni+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O UPPLJLAHMKABPR-UHFFFAOYSA-H 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 1
- 229940092714 benzenesulfonic acid Drugs 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- FJIUUBZGIYMKFS-UHFFFAOYSA-N dioxoruthenium oxygen(2-) titanium(4+) Chemical compound [Ru](=O)=O.[O-2].[O-2].[Ti+4] FJIUUBZGIYMKFS-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005065 mining Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052758 niobium Inorganic materials 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 1
- 239000001508 potassium citrate Substances 0.000 description 1
- 229960002635 potassium citrate Drugs 0.000 description 1
- QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 description 1
- 235000011082 potassium citrates Nutrition 0.000 description 1
- 229910052715 tantalum Inorganic materials 0.000 description 1
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/12—Electroplating: Baths therefor from solutions of nickel or cobalt
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Cosmetics (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US19989480A | 1980-10-23 | 1980-10-23 | |
| US199,894 | 1980-10-23 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1180677A true CA1180677A (en) | 1985-01-08 |
Family
ID=22739453
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000386693A Expired CA1180677A (en) | 1980-10-23 | 1981-09-25 | Bath and process for high speed nickel electroplating |
Country Status (15)
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1162505A (en) * | 1980-10-31 | 1984-02-21 | Donald R. Rosegren | Process for high speed nickel and gold electroplate system |
| US4543166A (en) * | 1984-10-01 | 1985-09-24 | Omi International Corporation | Zinc-alloy electrolyte and process |
| JP4904933B2 (ja) * | 2005-09-27 | 2012-03-28 | 日立電線株式会社 | ニッケルめっき液とその製造方法、ニッケルめっき方法およびプリント配線板用銅箔 |
| KR102281132B1 (ko) * | 2019-10-24 | 2021-07-26 | 일진머티리얼즈 주식회사 | 박막형 커패시터 제조용 전해니켈박 및 그의 제조방법 |
| CN112323096A (zh) * | 2020-09-23 | 2021-02-05 | 河北东恩企业管理咨询有限公司 | 一种含硫镍圆饼的制备方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3334032A (en) * | 1964-05-08 | 1967-08-01 | Hanson Van Winkle Munning Co | Electrodeposition of nickel |
| US3697391A (en) * | 1970-07-17 | 1972-10-10 | M & T Chemicals Inc | Electroplating processes and compositions |
| ZA721964B (en) * | 1971-04-01 | 1972-12-27 | M & T Chemicals Inc | Nickel plating |
-
1981
- 1981-09-24 DK DK422181A patent/DK422181A/da not_active Application Discontinuation
- 1981-09-25 CA CA000386693A patent/CA1180677A/en not_active Expired
- 1981-09-25 AU AU75676/81A patent/AU527954B2/en not_active Ceased
- 1981-10-06 DE DE3139641A patent/DE3139641C2/de not_active Expired
- 1981-10-09 ES ES506173A patent/ES506173A0/es active Granted
- 1981-10-13 JP JP56163363A patent/JPS6020475B2/ja not_active Expired
- 1981-10-21 IT IT49529/81A patent/IT1171598B/it active
- 1981-10-22 SE SE8106250A patent/SE8106250L/ unknown
- 1981-10-22 BE BE0/206326A patent/BE890836A/fr not_active IP Right Cessation
- 1981-10-22 BR BR8106819A patent/BR8106819A/pt not_active IP Right Cessation
- 1981-10-22 FR FR8119853A patent/FR2492849A1/fr active Granted
- 1981-10-22 CH CH6755/81A patent/CH649579A5/de not_active IP Right Cessation
- 1981-10-23 NL NL8104808A patent/NL8104808A/nl not_active Application Discontinuation
- 1981-10-23 GB GB8132066A patent/GB2085924B/en not_active Expired
-
1986
- 1986-09-11 HK HK667/86A patent/HK66786A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ES8302802A1 (es) | 1983-01-16 |
| GB2085924A (en) | 1982-05-06 |
| DE3139641A1 (de) | 1982-09-30 |
| NL8104808A (nl) | 1982-05-17 |
| IT1171598B (it) | 1987-06-10 |
| HK66786A (en) | 1986-09-18 |
| IT8149529A0 (it) | 1981-10-21 |
| FR2492849A1 (fr) | 1982-04-30 |
| BE890836A (fr) | 1982-04-22 |
| GB2085924B (en) | 1983-06-02 |
| AU7567681A (en) | 1982-04-29 |
| JPS5794589A (en) | 1982-06-12 |
| DE3139641C2 (de) | 1986-07-31 |
| ES506173A0 (es) | 1983-01-16 |
| JPS6020475B2 (ja) | 1985-05-22 |
| FR2492849B1 (enrdf_load_stackoverflow) | 1984-11-23 |
| AU527954B2 (en) | 1983-03-31 |
| BR8106819A (pt) | 1982-07-06 |
| SE8106250L (sv) | 1982-04-24 |
| CH649579A5 (de) | 1985-05-31 |
| DK422181A (da) | 1982-04-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US4428802A (en) | Palladium-nickel alloy electroplating and solutions therefor | |
| CA1267631A (en) | Trivalent chromium electrolyte and process employing vanadium reducing agent | |
| TWI439580B (zh) | 用於電鍍錫合金層之焦磷酸鹽基浴 | |
| US4013523A (en) | Tin-gold electroplating bath and process | |
| EP0320081B1 (en) | Method for production of tin-cobalt, tin-nickel, or tin-lead binary alloy electroplating bath and electroplating bath produced thereby | |
| US4411965A (en) | Process for high speed nickel and gold electroplate system and article having improved corrosion resistance | |
| US3691027A (en) | Method of producing corrosion resistant chromium plated articles | |
| CA1129805A (en) | Electrodeposition of ruthenium-iridium alloy | |
| CA1180677A (en) | Bath and process for high speed nickel electroplating | |
| CA1162505A (en) | Process for high speed nickel and gold electroplate system | |
| EP0348043B1 (en) | Electroplating bath and process for depositing functional chromium | |
| US4466865A (en) | Trivalent chromium electroplating process | |
| US4265715A (en) | Silver electrodeposition process | |
| US4411744A (en) | Bath and process for high speed nickel electroplating | |
| US4487665A (en) | Electroplating bath and process for white palladium | |
| JPS6250560B2 (enrdf_load_stackoverflow) | ||
| US4297179A (en) | Palladium electroplating bath and process | |
| US3984291A (en) | Electrodeposition of tin-lead alloys and compositions therefor | |
| EP0088192A1 (en) | Control of anode gas evolution in trivalent chromium plating bath | |
| RU2133305C1 (ru) | Электролит блестящего никелирования | |
| US4836897A (en) | Baths and process for electroplating hard,adherent,smooth, wear resistant and corrosion resistant chromium deposits | |
| US3215610A (en) | Method and bath for electrodepositing bright silver | |
| JP2763072B2 (ja) | 錫‐ニツケル合金めつき液 | |
| US4428804A (en) | High speed bright silver electroplating bath and process | |
| US4401527A (en) | Process for the electrodeposition of palladium |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |