CA1172454A - Process for the preparation of aluminum-containing high-energy explosive compositions - Google Patents
Process for the preparation of aluminum-containing high-energy explosive compositionsInfo
- Publication number
- CA1172454A CA1172454A CA000369656A CA369656A CA1172454A CA 1172454 A CA1172454 A CA 1172454A CA 000369656 A CA000369656 A CA 000369656A CA 369656 A CA369656 A CA 369656A CA 1172454 A CA1172454 A CA 1172454A
- Authority
- CA
- Canada
- Prior art keywords
- wax
- tnt
- process according
- granules
- rdx
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- SPSSULHKWOKEEL-UHFFFAOYSA-N 2,4,6-trinitrotoluene Chemical compound CC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O SPSSULHKWOKEEL-UHFFFAOYSA-N 0.000 claims abstract description 46
- 239000000015 trinitrotoluene Substances 0.000 claims abstract description 46
- 239000000203 mixture Substances 0.000 claims abstract description 41
- 239000008187 granular material Substances 0.000 claims abstract description 35
- 239000001993 wax Substances 0.000 claims abstract description 31
- 239000002360 explosive Substances 0.000 claims abstract description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000024 RDX Substances 0.000 claims abstract description 24
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 21
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims abstract description 18
- 229940067606 lecithin Drugs 0.000 claims abstract description 18
- 235000010445 lecithin Nutrition 0.000 claims abstract description 18
- 239000000787 lecithin Substances 0.000 claims abstract description 18
- 239000000028 HMX Substances 0.000 claims abstract description 15
- 238000003756 stirring Methods 0.000 claims abstract description 15
- 238000002844 melting Methods 0.000 claims abstract description 14
- 230000008018 melting Effects 0.000 claims abstract description 14
- 238000001816 cooling Methods 0.000 claims abstract description 6
- 239000006185 dispersion Substances 0.000 claims abstract description 6
- 239000013078 crystal Substances 0.000 claims abstract description 3
- 239000000020 Nitrocellulose Substances 0.000 claims abstract 8
- 229920001220 nitrocellulos Polymers 0.000 claims abstract 8
- 238000000034 method Methods 0.000 claims description 26
- 239000012170 montan wax Substances 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 5
- 239000000155 melt Substances 0.000 claims description 3
- 239000012169 petroleum derived wax Substances 0.000 claims description 2
- 235000019381 petroleum wax Nutrition 0.000 claims description 2
- BNPSSFBOAGDEEL-UHFFFAOYSA-N albuterol sulfate Chemical compound OS(O)(=O)=O.CC(C)(C)NCC(O)C1=CC=C(O)C(CO)=C1.CC(C)(C)NCC(O)C1=CC=C(O)C(CO)=C1 BNPSSFBOAGDEEL-UHFFFAOYSA-N 0.000 abstract description 8
- 239000003795 chemical substances by application Substances 0.000 abstract description 4
- 238000002156 mixing Methods 0.000 abstract description 4
- FTAFBCWHLFKBFJ-UHFFFAOYSA-N aluminum;2-methyl-1,3,5-trinitrobenzene;1,3,5,7-tetranitro-1,3,5,7-tetrazocane Chemical compound [Al].CC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O.[O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)CN([N+]([O-])=O)C1 FTAFBCWHLFKBFJ-UHFFFAOYSA-N 0.000 abstract description 3
- 239000003381 stabilizer Substances 0.000 abstract 1
- XTFIVUDBNACUBN-UHFFFAOYSA-N 1,3,5-trinitro-1,3,5-triazinane Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)C1 XTFIVUDBNACUBN-UHFFFAOYSA-N 0.000 description 20
- 239000000306 component Substances 0.000 description 15
- 239000000047 product Substances 0.000 description 14
- 229910052782 aluminium Inorganic materials 0.000 description 10
- 238000005266 casting Methods 0.000 description 10
- UZGLIIJVICEWHF-UHFFFAOYSA-N octogen Chemical compound [O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)CN([N+]([O-])=O)C1 UZGLIIJVICEWHF-UHFFFAOYSA-N 0.000 description 9
- 241000921519 Syrrhopodon sp. Species 0.000 description 8
- 239000000843 powder Substances 0.000 description 6
- 239000000428 dust Substances 0.000 description 5
- ZCSHACFHMFHFKK-UHFFFAOYSA-N 2-methyl-1,3,5-trinitrobenzene;2,4,6-trinitro-1,3,5-triazinane Chemical compound [O-][N+](=O)C1NC([N+]([O-])=O)NC([N+]([O-])=O)N1.CC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O ZCSHACFHMFHFKK-UHFFFAOYSA-N 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000007792 addition Methods 0.000 description 3
- 238000010410 dusting Methods 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 238000011068 loading method Methods 0.000 description 3
- 239000012188 paraffin wax Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- UPSVYNDQEVZTMB-UHFFFAOYSA-N 2-methyl-1,3,5-trinitrobenzene;1,3,5,7-tetranitro-1,3,5,7-tetrazocane Chemical compound CC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O.[O-][N+](=O)N1CN([N+]([O-])=O)CN([N+]([O-])=O)CN([N+]([O-])=O)C1 UPSVYNDQEVZTMB-UHFFFAOYSA-N 0.000 description 2
- 238000005422 blasting Methods 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000004880 explosion Methods 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 101100379067 Caenorhabditis elegans anc-1 gene Proteins 0.000 description 1
- 241000251729 Elasmobranchii Species 0.000 description 1
- 235000015842 Hesperis Nutrition 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 235000012633 Iberis amara Nutrition 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000005474 detonation Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B25/00—Compositions containing a nitrated organic compound
- C06B25/34—Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0033—Shaping the mixture
- C06B21/005—By a process involving melting at least part of the ingredients
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0033—Shaping the mixture
- C06B21/0066—Shaping the mixture by granulation, e.g. flaking
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Powder Metallurgy (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Ceramic Products (AREA)
- Forging (AREA)
- Developing Agents For Electrophotography (AREA)
- Medicinal Preparation (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Treatment Of Steel In Its Molten State (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NO80.0582 | 1980-02-29 | ||
| NO800582A NO144666C (no) | 1980-02-29 | 1980-02-29 | Fremgangsmaate for fremstilling av aluminiumholdige hoeyenergisprengstoffblandinger |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1172454A true CA1172454A (en) | 1984-08-14 |
Family
ID=19885355
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000369656A Expired CA1172454A (en) | 1980-02-29 | 1981-01-29 | Process for the preparation of aluminum-containing high-energy explosive compositions |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4376083A (enExample) |
| EP (1) | EP0035376B1 (enExample) |
| AT (1) | ATE13517T1 (enExample) |
| CA (1) | CA1172454A (enExample) |
| DE (1) | DE3170679D1 (enExample) |
| ES (1) | ES8202324A1 (enExample) |
| GR (1) | GR74155B (enExample) |
| NO (1) | NO144666C (enExample) |
| PT (1) | PT72476B (enExample) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ATE71927T1 (de) * | 1985-09-27 | 1992-02-15 | Nobel Kemi Ab | Verfahren zur phlegmatisierung von kristallinen sprengstoffen und sonstigen kristallinen explosiven substanzen sowie verfahren zur herstellung von kunststoffgebundenen sprengstoffmischungen und nach dem verfahren hergestellte substanzen. |
| SE452760B (sv) * | 1985-09-27 | 1987-12-14 | Nobel Kemi Ab | Sett att framstella blandsprengemnen av typen hexotonal och oktonal |
| SE8600119L (sv) * | 1986-01-10 | 1987-07-11 | Exploweld Ab | Sprengemnesmaterial |
| DE3614173C1 (de) * | 1986-04-26 | 1989-03-02 | Dynamit Nobel Ag | Granuliertes,stabilisiertes alpha- und beta-Oktogen und Verfahren zur Herstellung von alpha-Oktogen |
| US4938143A (en) * | 1987-04-29 | 1990-07-03 | Trojan Corporation | Booster shaped for high-efficiency detonating |
| US4747892A (en) * | 1987-05-22 | 1988-05-31 | The United States Of America As Represented By The Secretary Of The Air Force | Melt-castable explosive composition |
| US4915755A (en) * | 1987-10-02 | 1990-04-10 | Kim Chung S | Filler reinforcement of polyurethane binder using a neutral polymeric bonding agent |
| JPH07112537B2 (ja) * | 1987-11-27 | 1995-12-06 | ダイセル化学工業株式会社 | 発火または爆発性の高い物質の原料組成物の混合方法 |
| FR2637589B1 (fr) * | 1988-10-06 | 1990-11-30 | France Etat Armement | Compose additif antifissurant pour composition explosive |
| AU632562B2 (en) * | 1989-05-11 | 1993-01-07 | Wnc-Nitrochemie Gmbh | Process and device for producing a tribasic propellent powder |
| DE4111752C1 (enExample) * | 1991-04-11 | 1992-09-17 | Fraunhofer-Gesellschaft Zur Foerderung Der Angewandten Forschung Ev, 8000 Muenchen, De | |
| DE4233629C2 (de) * | 1992-10-06 | 1994-09-15 | Wasagchemie Sythen Gmbh | Verfahren zur Herstellung eines Pulver-Vorproduktes und Pulver-Vorprodukt |
| SE511285C2 (sv) * | 1997-04-29 | 1999-09-06 | Foersvarets Forskningsanstalt | Smältgjutna laddningar |
| RU2181713C2 (ru) * | 1997-11-26 | 2002-04-27 | Федеральное государственное унитарное предприятие "Государственный научно-исследовательский институт "Кристалл" | Способ получения чешуированных взрывчатых веществ |
| RU2186754C2 (ru) * | 1998-10-15 | 2002-08-10 | Российский федеральный ядерный центр - Всероссийский научно-исследовательский институт технической физики | Способ кристаллизации расплавов взрывчатых композиций с твердыми включениями и устройство для его осуществления |
| US6485586B1 (en) | 2000-10-27 | 2002-11-26 | The United States Of America As Represented By The Secretary Of The Navy | Lower burning rate, reduced hazard, high temperature incendiary |
| US6723190B1 (en) * | 2000-10-27 | 2004-04-20 | The United States Of America As Represented By The Secretary Of The Navy | ESD sensitivity in titanium/boron compositions |
| DE10107948A1 (de) * | 2001-02-20 | 2002-08-22 | Rheinmetall W & M Gmbh | Verfahren zur Herstellung gießfähiger kunststoffgebundener Sprengladungen oder Raketentreibstoffe |
| US6666936B1 (en) | 2002-02-28 | 2003-12-23 | The Regents Of The University Of California | Energetic powder |
| US20040231546A1 (en) * | 2003-05-23 | 2004-11-25 | Ofca William W. | Safe electrical initiation plug for electric detonators |
| US7754036B1 (en) | 2003-12-03 | 2010-07-13 | The United States Of America As Represented By The Secretary Of The Navy | Thermobaric explosives and compositions, and articles of manufacture and methods regarding the same |
| FR2878320B1 (fr) * | 2004-11-22 | 2009-05-08 | Giat Ind Sa | Munition ou composant de munition comprenant un materiau energetique structural |
| FR2934260B1 (fr) * | 2008-07-28 | 2010-08-27 | Nexter Munitions | Procede de coulee d'un materiau explosif a vulnerabilite reduite et materiau mis en oeuvre dans un tel procede |
| RU2448934C1 (ru) * | 2010-08-16 | 2012-04-27 | Федеральное Государственное Унитарное Предприятие "Красноармейский Научно-Исследовательский Институт Механизации" | Нанодисперсный взрывчатый состав |
| CA2861109A1 (en) * | 2012-01-13 | 2013-10-10 | Los Alamos National Security, Llc | Geologic fracturing method and resulting fractured geologic structure |
| WO2015009749A1 (en) | 2013-07-15 | 2015-01-22 | Los Alamos National Security, Llc | Casings for use in a system for fracturing rock within a bore |
| US10273792B2 (en) | 2013-07-15 | 2019-04-30 | Triad National Security, Llc | Multi-stage geologic fracturing |
| WO2015009752A1 (en) | 2013-07-15 | 2015-01-22 | Los Alamos National Security, Llc | Fluid transport systems for use in a downhole explosive fracturing system |
| PL451464A1 (pl) * | 2022-09-13 | 2025-11-24 | Agency For Defense Development | Odlewana kompozycja wysokoenergetyczna na bazie lepiszcza polisiloksanowego, kompozycja materiału wybuchowego rdzenia, kompozycja paliwa powłoki, kompozycja pojedynczego termobarycznego materiału wybuchowego oraz zawierająca je głowica bojowa |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2982641A (en) * | 1946-05-06 | 1961-05-02 | John W Dawson | Aluminized explosives |
| US2981618A (en) * | 1952-05-06 | 1961-04-25 | Selwyn R Walton | High explosive filler for naval underwater munitions |
| GB788693A (en) * | 1955-03-16 | 1958-01-08 | Bofors Ab | Manufacture of granulated mixed explosives containing trinitrotoluene |
| FR1180530A (fr) * | 1957-08-02 | 1959-06-04 | Le Secretaire D Etat A La Defe | Perfectionnements aux mélanges explosifs contenant de l'aluminium ou autres métaux ou alliages et à leur fabrication |
| FR1599069A (enExample) * | 1967-11-29 | 1970-07-15 | ||
| FR2102642A5 (en) * | 1970-08-13 | 1972-04-07 | France Etat | Wax coated tolite - granular explosive safely used in bulk and water resistant |
| US3706609A (en) * | 1970-12-29 | 1972-12-19 | Us Army | Tnt composition containing a cellulosic resin which is free from oily exudation upon storage |
| US4089715A (en) * | 1973-09-05 | 1978-05-16 | Metal Sales Company (Proprietary) Limited | Explosive grade aluminum powder |
| DE2506884C1 (de) * | 1975-02-19 | 1979-12-06 | Messerschmitt Boelkow Blohm | Behandlung von gegossenen Hochbrisanz-Sprengstofformkoerpern |
| CA1058882A (en) * | 1976-05-31 | 1979-07-24 | Kenneth S. Kalman | Prilled explosive composition |
-
1980
- 1980-02-29 NO NO800582A patent/NO144666C/no unknown
-
1981
- 1981-01-26 US US06/228,056 patent/US4376083A/en not_active Expired - Fee Related
- 1981-01-29 CA CA000369656A patent/CA1172454A/en not_active Expired
- 1981-02-09 PT PT72476A patent/PT72476B/pt not_active IP Right Cessation
- 1981-02-24 GR GR64227A patent/GR74155B/el unknown
- 1981-02-26 AT AT81300804T patent/ATE13517T1/de not_active IP Right Cessation
- 1981-02-26 EP EP81300804A patent/EP0035376B1/en not_active Expired
- 1981-02-26 DE DE8181300804T patent/DE3170679D1/de not_active Expired
- 1981-02-27 ES ES499866A patent/ES8202324A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE3170679D1 (en) | 1985-07-04 |
| GR74155B (enExample) | 1984-06-06 |
| US4376083A (en) | 1983-03-08 |
| EP0035376A2 (en) | 1981-09-09 |
| NO800582L (no) | 1981-07-06 |
| NO144666C (no) | 1981-10-14 |
| EP0035376A3 (en) | 1982-08-18 |
| PT72476A (en) | 1981-03-01 |
| ES499866A0 (es) | 1982-01-16 |
| ATE13517T1 (de) | 1985-06-15 |
| ES8202324A1 (es) | 1982-01-16 |
| PT72476B (en) | 1982-02-04 |
| NO144666B (no) | 1981-07-06 |
| EP0035376B1 (en) | 1985-05-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |