CA1143116A - Process for the manufacture of ceramic oxide fibers from solvent solution - Google Patents
Process for the manufacture of ceramic oxide fibers from solvent solutionInfo
- Publication number
- CA1143116A CA1143116A CA000362758A CA362758A CA1143116A CA 1143116 A CA1143116 A CA 1143116A CA 000362758 A CA000362758 A CA 000362758A CA 362758 A CA362758 A CA 362758A CA 1143116 A CA1143116 A CA 1143116A
- Authority
- CA
- Canada
- Prior art keywords
- disc
- solution
- fibers
- openings
- air
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000835 fiber Substances 0.000 title claims abstract description 89
- 238000000034 method Methods 0.000 title claims abstract description 36
- 239000002904 solvent Substances 0.000 title claims abstract description 28
- 239000000919 ceramic Substances 0.000 title claims abstract description 27
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 8
- 239000002243 precursor Substances 0.000 claims abstract description 29
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 9
- 239000001301 oxygen Substances 0.000 claims abstract description 9
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 9
- 238000009987 spinning Methods 0.000 claims abstract description 9
- 238000001354 calcination Methods 0.000 claims abstract description 5
- 239000000243 solution Substances 0.000 claims description 61
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical group Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical group [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 10
- 229910052782 aluminium Inorganic materials 0.000 claims description 10
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 8
- 239000011651 chromium Substances 0.000 claims description 8
- 229910052804 chromium Inorganic materials 0.000 claims description 7
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 5
- -1 alkyl organic acid Chemical class 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 150000003608 titanium Chemical class 0.000 claims description 4
- 229910052726 zirconium Inorganic materials 0.000 claims description 4
- DUFCMRCMPHIFTR-UHFFFAOYSA-N 5-(dimethylsulfamoyl)-2-methylfuran-3-carboxylic acid Chemical compound CN(C)S(=O)(=O)C1=CC(C(O)=O)=C(C)O1 DUFCMRCMPHIFTR-UHFFFAOYSA-N 0.000 claims description 3
- INNSZZHSFSFSGS-UHFFFAOYSA-N acetic acid;titanium Chemical compound [Ti].CC(O)=O.CC(O)=O.CC(O)=O.CC(O)=O INNSZZHSFSFSGS-UHFFFAOYSA-N 0.000 claims description 3
- CMOAHYOGLLEOGO-UHFFFAOYSA-N oxozirconium;dihydrochloride Chemical compound Cl.Cl.[Zr]=O CMOAHYOGLLEOGO-UHFFFAOYSA-N 0.000 claims description 3
- MJWPFSQVORELDX-UHFFFAOYSA-K aluminium formate Chemical compound [Al+3].[O-]C=O.[O-]C=O.[O-]C=O MJWPFSQVORELDX-UHFFFAOYSA-K 0.000 claims description 2
- MADFGXYYGXDVDA-UHFFFAOYSA-K aluminum;2-chloroacetate Chemical compound [Al+3].[O-]C(=O)CCl.[O-]C(=O)CCl.[O-]C(=O)CCl MADFGXYYGXDVDA-UHFFFAOYSA-K 0.000 claims description 2
- HDYRYUINDGQKMC-UHFFFAOYSA-M acetyloxyaluminum;dihydrate Chemical compound O.O.CC(=O)O[Al] HDYRYUINDGQKMC-UHFFFAOYSA-M 0.000 claims 1
- 235000010210 aluminium Nutrition 0.000 claims 1
- 229940009827 aluminum acetate Drugs 0.000 claims 1
- 150000003839 salts Chemical class 0.000 description 7
- 229940107218 chromium Drugs 0.000 description 6
- 235000012721 chromium Nutrition 0.000 description 6
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
- 239000012768 molten material Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000008119 colloidal silica Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000004310 lactic acid Substances 0.000 description 3
- 235000014655 lactic acid Nutrition 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical group Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 230000002238 attenuated effect Effects 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- 150000007522 mineralic acids Chemical class 0.000 description 2
- 238000003466 welding Methods 0.000 description 2
- 229910001928 zirconium oxide Inorganic materials 0.000 description 2
- 229940043774 zirconium oxide Drugs 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 101100113576 Arabidopsis thaliana CINV2 gene Proteins 0.000 description 1
- 101000878595 Arabidopsis thaliana Squalene synthase 1 Proteins 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 101000966782 Homo sapiens Lysophosphatidic acid receptor 1 Proteins 0.000 description 1
- 102100040607 Lysophosphatidic acid receptor 1 Human genes 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 229910052770 Uranium Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000005189 alkyl hydroxy group Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 229910000423 chromium oxide Inorganic materials 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000013081 microcrystal Substances 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229960005196 titanium dioxide Drugs 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/04—Manufacture of glass fibres or filaments by using centrifugal force, e.g. spinning through radial orifices; Construction of the spinner cups therefor
- C03B37/045—Construction of the spinner cups
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/04—Manufacture of glass fibres or filaments by using centrifugal force, e.g. spinning through radial orifices; Construction of the spinner cups therefor
- C03B37/048—Means for attenuating the spun fibres, e.g. blowers for spinner cups
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/62227—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
- C04B35/62231—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on oxide ceramics
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Ceramic Engineering (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Inorganic Fibers (AREA)
- Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/105,319 US4277269A (en) | 1979-12-19 | 1979-12-19 | Process for the manufacture of ceramic oxide fibers from solvent solution |
| US105,319 | 1979-12-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1143116A true CA1143116A (en) | 1983-03-22 |
Family
ID=22305157
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000362758A Expired CA1143116A (en) | 1979-12-19 | 1980-10-20 | Process for the manufacture of ceramic oxide fibers from solvent solution |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4277269A (enExample) |
| EP (1) | EP0031656B1 (enExample) |
| JP (1) | JPS5696915A (enExample) |
| AU (1) | AU539231B2 (enExample) |
| CA (1) | CA1143116A (enExample) |
| DE (1) | DE3065327D1 (enExample) |
| MX (1) | MX156048A (enExample) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4409158A (en) * | 1981-01-22 | 1983-10-11 | Pq Corporation | Spray drying method of preparing hollow fibers |
| EP0206634A3 (en) * | 1985-06-21 | 1987-08-19 | Imperial Chemical Industries Plc | Inorganic oxide fibres and their production |
| EP0206647B1 (en) * | 1985-06-21 | 1992-07-29 | Imperial Chemical Industries Plc | Fibre-reinforced metal matrix composites |
| JPH07103491B2 (ja) * | 1986-09-17 | 1995-11-08 | 三井鉱山株式会社 | α−アルミナ長繊維の連続製造方法 |
| JP2521081B2 (ja) * | 1987-03-05 | 1996-07-31 | 住友化学工業株式会社 | アルミナ質繊維の製造方法 |
| WO1994024425A1 (en) * | 1993-04-22 | 1994-10-27 | The Carborundum Company | Mounting mat for fragile structures such as catalytic converters |
| US5767022A (en) * | 1994-08-23 | 1998-06-16 | Unifrax Corporation | Friction pad containing high temperature stable continuous filament glass fibers |
| US5569629A (en) * | 1994-08-23 | 1996-10-29 | Unifrax Corporation | High temperature stable continuous filament glass ceramic fibers |
| US5686368A (en) * | 1995-12-13 | 1997-11-11 | Quantum Group, Inc. | Fibrous metal oxide textiles for spectral emitters |
| US8404187B1 (en) | 1998-03-11 | 2013-03-26 | Unifrax I Llc | Support element for fragile structures such as catalytic converters |
| WO2004003276A1 (ja) * | 2002-06-28 | 2004-01-08 | Denki Kagaku Kogyo Kabushiki Kaisha | 保持材用無機質短繊維集積体、その製造方法、及び保持材 |
| BR0314957B1 (pt) * | 2002-09-30 | 2011-11-01 | dispositivo para tratamento de gases de exaustão e método de fabricação do mesmo. | |
| CN101098744B (zh) | 2004-06-29 | 2013-11-06 | 尤尼弗瑞克斯I有限责任公司 | 废气处理装置及其制造方法 |
| KR101441910B1 (ko) * | 2005-11-10 | 2014-10-01 | 더 몰간 크루시블 캄파니 피엘시 | 고온내열성 섬유 |
| JP2010514649A (ja) * | 2006-12-21 | 2010-05-06 | スリーエム イノベイティブ プロパティズ カンパニー | ナノ粒子の製造方法 |
| MX2010002182A (es) * | 2007-08-31 | 2010-03-18 | Unifrax I Llc | Sistema de montaje para sustratos. |
| WO2009085731A1 (en) * | 2007-12-21 | 2009-07-09 | 3M Innovative Properties Company | Process for producing nanoparticles |
| JP5173579B2 (ja) * | 2008-05-16 | 2013-04-03 | 株式会社Ｉｔｍ | アルミナ繊維の製造方法、繊維化装置、ブランケット及びブロック |
| WO2011019394A1 (en) | 2009-08-14 | 2011-02-17 | Unifrax I Llc | Multiple layer substrate support and exhaust gas treatment device |
| US9174169B2 (en) | 2009-08-14 | 2015-11-03 | Unifrax I Llc | Mounting mat for exhaust gas treatment device |
| KR20120074284A (ko) | 2009-09-24 | 2012-07-05 | 유니프랙스 아이 엘엘씨 | 다층 매트 및 배기 가스 처리 장치 |
| AU2010319346B2 (en) | 2009-11-13 | 2015-02-05 | Unifrax I Llc | Multi-layer fire protection material |
| CA2780131A1 (en) | 2009-11-16 | 2011-05-19 | Unifrax I Llc | Intumescent fire protection material |
| KR101796329B1 (ko) | 2009-12-17 | 2017-11-09 | 유니프랙스 아이 엘엘씨 | 배기 가스 처리 기기용 장착 매트 |
| US9924564B2 (en) | 2010-11-11 | 2018-03-20 | Unifrax I Llc | Heated mat and exhaust gas treatment device |
| EP2638261A4 (en) | 2010-11-11 | 2014-08-06 | Unifrax I Llc | SUPPORT MAT AND DEVICE FOR TREATING EXHAUST GASES |
| CN113059135A (zh) * | 2021-03-12 | 2021-07-02 | 赣州大业金属纤维有限公司 | 一种采用熔钢抽丝法快速生产钢纤维的设备 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| USRE24708E (en) | 1946-05-31 | 1959-09-29 | Process and apparatus for the production | |
| US3177058A (en) * | 1956-04-18 | 1965-04-06 | Owens Corning Fiberglass Corp | Apparatus for processing heatsoftenable materials |
| US3485611A (en) * | 1966-05-27 | 1969-12-23 | Babcock & Wilcox Co | Rotary apparatus for making ceramic fibers |
| ZA7676B (en) * | 1975-01-27 | 1977-08-31 | Johns Manville | Method and apparatus for eliminating external hot gas attenuation in the rotary fiberization of glass |
| JPS584096B2 (ja) * | 1976-07-23 | 1983-01-25 | 東芝モノフラツクス株式会社 | 酸化物多結晶繊維の製造方法 |
-
1979
- 1979-12-19 US US06/105,319 patent/US4277269A/en not_active Expired - Lifetime
-
1980
- 1980-10-20 CA CA000362758A patent/CA1143116A/en not_active Expired
- 1980-12-09 EP EP80304434A patent/EP0031656B1/en not_active Expired
- 1980-12-09 DE DE8080304434T patent/DE3065327D1/de not_active Expired
- 1980-12-11 MX MX185178A patent/MX156048A/es unknown
- 1980-12-16 JP JP17663580A patent/JPS5696915A/ja active Granted
- 1980-12-18 AU AU65519/80A patent/AU539231B2/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| AU539231B2 (en) | 1984-09-20 |
| JPS5696915A (en) | 1981-08-05 |
| MX156048A (es) | 1988-06-21 |
| AU6551980A (en) | 1981-06-25 |
| EP0031656B1 (en) | 1983-10-12 |
| JPS6366926B2 (enExample) | 1988-12-22 |
| US4277269A (en) | 1981-07-07 |
| EP0031656A1 (en) | 1981-07-08 |
| DE3065327D1 (en) | 1983-11-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |