CA1120867A - Two layer wound-on-core medium filter element - Google Patents
Two layer wound-on-core medium filter elementInfo
- Publication number
- CA1120867A CA1120867A CA000319714A CA319714A CA1120867A CA 1120867 A CA1120867 A CA 1120867A CA 000319714 A CA000319714 A CA 000319714A CA 319714 A CA319714 A CA 319714A CA 1120867 A CA1120867 A CA 1120867A
- Authority
- CA
- Canada
- Prior art keywords
- filter
- layer
- particles
- particle retention
- nominal particle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002245 particle Substances 0.000 claims abstract description 93
- 239000000463 material Substances 0.000 claims abstract description 32
- 239000007788 liquid Substances 0.000 claims abstract description 31
- 238000000034 method Methods 0.000 claims abstract description 14
- 238000011001 backwashing Methods 0.000 claims abstract description 7
- 239000011248 coating agent Substances 0.000 claims abstract 2
- 238000000576 coating method Methods 0.000 claims abstract 2
- 230000014759 maintenance of location Effects 0.000 claims description 40
- 230000007423 decrease Effects 0.000 claims description 4
- 230000003247 decreasing effect Effects 0.000 claims description 3
- 230000000717 retained effect Effects 0.000 abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 28
- 239000002002 slurry Substances 0.000 description 16
- 238000004804 winding Methods 0.000 description 15
- 239000011347 resin Substances 0.000 description 13
- 229920005989 resin Polymers 0.000 description 13
- 239000000706 filtrate Substances 0.000 description 9
- 238000012546 transfer Methods 0.000 description 9
- 238000001914 filtration Methods 0.000 description 8
- 239000000428 dust Substances 0.000 description 5
- 239000012535 impurity Substances 0.000 description 5
- 238000011144 upstream manufacturing Methods 0.000 description 5
- 239000007789 gas Substances 0.000 description 4
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 3
- 229910000831 Steel Inorganic materials 0.000 description 3
- 239000003957 anion exchange resin Substances 0.000 description 3
- 239000003729 cation exchange resin Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- 238000003466 welding Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000004677 Nylon Substances 0.000 description 2
- QAHZAHIPKNLGAS-QMJNRFBBSA-N ac1l9bd4 Chemical compound C12=CC=3OCOC=3C(OC)=C2CN2[C@@H]3C[C@@H](OC)C=C[C@]31[C@H](O)C2 QAHZAHIPKNLGAS-QMJNRFBBSA-N 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 2
- 239000007900 aqueous suspension Substances 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- 239000011324 bead Substances 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 238000004891 communication Methods 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000012065 filter cake Substances 0.000 description 2
- 238000005342 ion exchange Methods 0.000 description 2
- 239000003456 ion exchange resin Substances 0.000 description 2
- 229920003303 ion-exchange polymer Polymers 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229920001778 nylon Polymers 0.000 description 2
- 239000013618 particulate matter Substances 0.000 description 2
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- 229920002972 Acrylic fiber Polymers 0.000 description 1
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical group Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 230000003292 diminished effect Effects 0.000 description 1
- SLGWESQGEUXWJQ-UHFFFAOYSA-N formaldehyde;phenol Chemical compound O=C.OC1=CC=CC=C1 SLGWESQGEUXWJQ-UHFFFAOYSA-N 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 229920002239 polyacrylonitrile Polymers 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000008149 soap solution Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J47/00—Ion-exchange processes in general; Apparatus therefor
- B01J47/12—Ion-exchange processes in general; Apparatus therefor characterised by the use of ion-exchange material in the form of ribbons, filaments, fibres or sheets, e.g. membranes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/11—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with bag, cage, hose, tube, sleeve or like filtering elements
- B01D29/111—Making filtering elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/11—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with bag, cage, hose, tube, sleeve or like filtering elements
- B01D29/13—Supported filter elements
- B01D29/15—Supported filter elements arranged for inward flow filtration
- B01D29/21—Supported filter elements arranged for inward flow filtration with corrugated, folded or wound sheets
- B01D29/216—Supported filter elements arranged for inward flow filtration with corrugated, folded or wound sheets with wound sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/50—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
- B01D29/52—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in parallel connection
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/50—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
- B01D29/56—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection
- B01D29/58—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection arranged concentrically or coaxially
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/62—Regenerating the filter material in the filter
- B01D29/66—Regenerating the filter material in the filter by flushing, e.g. counter-current air-bumps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D37/00—Processes of filtration
- B01D37/02—Precoating the filter medium; Addition of filter aids to the liquid being filtered
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2201/00—Details relating to filtering apparatus
- B01D2201/04—Supports for the filtering elements
- B01D2201/043—Filter tubes connected to plates
- B01D2201/0438—Filter tubes connected to plates mounted substantially vertically on plates at the lower side of the filter elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2201/00—Details relating to filtering apparatus
- B01D2201/18—Filters characterised by the openings or pores
- B01D2201/188—Multiple filtering elements having filtering areas of different size
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Filtration Of Liquid (AREA)
- Filtering Materials (AREA)
Abstract
TWO LAYER WOUND-ON-CORE MEDIUM FILTER ELEMENT
ABSTRACT OF THE DISCLOSURE
A filter element having a perforated tubular core and a plurality of layers of strand material wound about the tubular core. The outermost layer has the ability to retain particles smaller than those retained by the innermost layer.
The size range of particles retained by the outermost layer is from one to twenty-five microns and the size range of particles retained by the innermost layer is from twenty-five to one hundred microns, According to the method of invention, the filter element is used to purify liquids through the steps of precoating, delivering liquid through the filter, periodically backwashing the filter, and pre-coating the filter again.
ABSTRACT OF THE DISCLOSURE
A filter element having a perforated tubular core and a plurality of layers of strand material wound about the tubular core. The outermost layer has the ability to retain particles smaller than those retained by the innermost layer.
The size range of particles retained by the outermost layer is from one to twenty-five microns and the size range of particles retained by the innermost layer is from twenty-five to one hundred microns, According to the method of invention, the filter element is used to purify liquids through the steps of precoating, delivering liquid through the filter, periodically backwashing the filter, and pre-coating the filter again.
Description
1~21~8f~7 TWO LAYER WOUND-ON-CORE MEDIUM FILTER ELEMENT
BACKGROUND OF THE INVENTION
. .
The invention relates to a filter element for use in a unit used to filter or purify liquid. In particular, the invention is directed to a filter element having two types of layers of windings over a central support core, and to a method of purifying liquids with such an element.
In the prior art one type of apparatus for filtering liquids typically includes a perforated cylindrical support core and windings of strands of material around the support core, such as disclosed in Goldman U.S. Patent No. 1,751,000.
These filters are adapted to remove undissolved particles from liquid as the liquid is passed through the filters in a direction from the outside, through the wound material, and into the support co~e. The undissolved particulate matter is trapped by the wound material.
Other filter ele;ments in the prior art disclose a number of layers of material wound around a central support core, wherein the layers vary in density. As disclosed in Snow U.S. Patent No. 3,680,709, the density decreases in a radial direction away from the support core because the windings are tighter close to the support core and are gradually re-duced toward the outside.
It has been found that such prior art filter elements ha~ing a plurality of layers, wherein outermost layers are less dense than the innermost layers, present difficulties resulting from fouling tendencies, backwashing limitations, and inadequate flow distribution. These disadvantages are d~
~ --.,, ~
~ 6 7 particularly noted when the wound filter elements of the prior art are used to support a precoat of particles in the si2e range of about 60 to 400 mesh. ~he precoat particles typically are particles of cation and anion exchange resins.
These precoated filter elements are used to purify water by reducing dissolved and undissolved impurity concentrations from levels of approximately 50 parts per billion to less than 10 parts per billion.
Filter elements of the prior art having a graduated density of windings decreasing in a direction away from the central support core are easily blinded by particulate matter which infiltrates towards the center of the wound layer or layers, as liquid is passed through the filter element in a service cycle direction. Because of close spacing of windings near the support core, it is difficult to achieve velocity flows of liquid in a backwash direction through the filter element sufficient to dislodge and remove particulate matteE
which is trapped within the filter element windings.
SUMMARY OF THE INVENTION
According to the present invention there is provided a ilter element, having a plurality of layers of windings, which overcomes the disadvantages of the prior art by improving flow distribution patterns thereby facilitating backwashing of the filter element, and by reducing fouling tendencies in a service cycle direction. These advantages are obtained in the present invention which comprises a perforated tubular
BACKGROUND OF THE INVENTION
. .
The invention relates to a filter element for use in a unit used to filter or purify liquid. In particular, the invention is directed to a filter element having two types of layers of windings over a central support core, and to a method of purifying liquids with such an element.
In the prior art one type of apparatus for filtering liquids typically includes a perforated cylindrical support core and windings of strands of material around the support core, such as disclosed in Goldman U.S. Patent No. 1,751,000.
These filters are adapted to remove undissolved particles from liquid as the liquid is passed through the filters in a direction from the outside, through the wound material, and into the support co~e. The undissolved particulate matter is trapped by the wound material.
Other filter ele;ments in the prior art disclose a number of layers of material wound around a central support core, wherein the layers vary in density. As disclosed in Snow U.S. Patent No. 3,680,709, the density decreases in a radial direction away from the support core because the windings are tighter close to the support core and are gradually re-duced toward the outside.
It has been found that such prior art filter elements ha~ing a plurality of layers, wherein outermost layers are less dense than the innermost layers, present difficulties resulting from fouling tendencies, backwashing limitations, and inadequate flow distribution. These disadvantages are d~
~ --.,, ~
~ 6 7 particularly noted when the wound filter elements of the prior art are used to support a precoat of particles in the si2e range of about 60 to 400 mesh. ~he precoat particles typically are particles of cation and anion exchange resins.
These precoated filter elements are used to purify water by reducing dissolved and undissolved impurity concentrations from levels of approximately 50 parts per billion to less than 10 parts per billion.
Filter elements of the prior art having a graduated density of windings decreasing in a direction away from the central support core are easily blinded by particulate matter which infiltrates towards the center of the wound layer or layers, as liquid is passed through the filter element in a service cycle direction. Because of close spacing of windings near the support core, it is difficult to achieve velocity flows of liquid in a backwash direction through the filter element sufficient to dislodge and remove particulate matteE
which is trapped within the filter element windings.
SUMMARY OF THE INVENTION
According to the present invention there is provided a ilter element, having a plurality of layers of windings, which overcomes the disadvantages of the prior art by improving flow distribution patterns thereby facilitating backwashing of the filter element, and by reducing fouling tendencies in a service cycle direction. These advantages are obtained in the present invention which comprises a perforated tubular
- 2 ~
;~
)867 support core, an innermost layer of filter material disposed about the tubular core, and an outermost layer of filter material disposed about the inner layer. The outermost layer has the ability to trap smaller particles than the innermost layer. This ability, expressed in terms of the particle size, is called the nominal particle retention number.
In one broad aspect, the invention comprehends a filter element, precoated with particles in the size range of 60 to 400 mesh, consisting essentially of a perforated tubular core. An inner layer of strand material is wound about the core, the inner layer having a nomlnal particle retention number between twenty-five and one hundred microns, and an outer layer of strand material is wound about the inner layer, the outer layer having a nominal particle retention number between one and twenty-five microns.
A precoat of particles in the size range of 60 to 400 mesh is supported on the outer layer.
The invention further comprehends a filter element, precoated with particles in the size range of 60 to 400 mesh, comprising a perforated tubular core with a plurality of layers of strand material wound about the core. The nominal particle retention number of the innermost layer is greater than the nominal particle retention number of the outermost layer and eaah of the layers, in addition to the innermost layer, has a nominal particle retention number less than an adjacent inner layer. The filter element is provided with a plurality of layers having nominal particle retention numbers which gradually decrease from the innermost layer to the outermost layer, and a precoat of particles in the size range of 60 to 400 mesh supported on the outer layer.
,, --.
In another aspect, the lnvention comprises a method for purifying liquids comprising precoating a filter having layers of strand material with particles in the size range of about 60 to 400 mesh. The filter has an outermost layer with a nominal particle retention number less than the nominal particle retention number of the innermost layer of the ilter, with the nominal particle retention numbers gradually decreasing from the innermost layer to the outermost layer. The method delivers liquid to be filtered through the precoated particles and the fllter periodlcally backwashing the filter and removing the precoated partlcles, precoating the filter with a fresh coatlng of particles in the size range of about 60 to 400 mesh.
Such an arrangement of the windings, with the layer having the largest nominal particle retention number closest to the support core and the layer having the smallest nominal particle retention number furthest away from the support core, confines the area for filtering or purifying liquids ..~,.;~
passed through the filter elements to substantially the layer at the outer surface of the element. Such confinement of f:ilter area into a relatively thin annular volume is parti-cularly desirable when the filter element is used in filter UllitS in which the filter elements are precoated with finely divided resin particles in the size range of 60 to 400 mesh.
In precoated filter elements according to the in~ention, the area which has the tendency to foul is substantially re-duced, and undissolved particles will not be lodged tightly within the element below its outer surface so as ~o make them difficult to remove by backwash methods.
Also, if resin or other particles are forced through the outermost layer in the event of a flow surge of liquid through the element, the particles will become distributed throughout the layers of the wound element. In this manner, some particles will be trapped by the windings as a result of the circuitous path they take through the filter element, but the open area remaining for flow of liquid will not be diminished to a point where the filter's ability to pass liquid is significantly reduced.
According to the present invention, backwashing is also improved because the outermost layer presents a greater pressure barrier to backwash liquid coming from the support core than does the innermost layer of strand material.
Therefore, backwash liquid tends to distribute itself uni-formly along the length of the filter element when confronted with the increased pressure barrier produced by the outer layer.
~ 7 Other advantages, objects, and features of the present invention will become apparent upon reading the following detailed description of the preferred embodiment in con-junction with the accompanying drawings.
~RIEF DESCRIPTION OF THE DRAWINGS
FIGURE 1 is a partial cross-sectional view of a typical filter and tank having replaceable, cylindrical filter elements which embody the present invention;
FIGURE 2 is a perspective view of a filter element according to the present invention, par~ially cut away to show the wound layers of strand material and the central support core; and FIGURE 3 is a cross-sectional view of the filter element of FIGURE 2, taken along line 2-2, and illustrating the types of relationship of the wound layers of strand material to the central support core.
DESCRIPTION OF THE PREFERRED E~ODIMENT
Referring now to the drawings, and more particularly to FIGURE 1, a filtering~device which may be employed to carry out the method of the present invention is generally indicated by reference numeral 10. This device i9 of the type which i8 shown and described in U.S. Patent No~ 3,279,608, which is assigend to the assignee;of this application. The filtering device 10 is adapted to receive an influent stream, filter the influent stream, and discharge the filtrate or effluent stream.
The filter tank 10 is a generally cylindrical vessel made of steel or the like having an outwardly convex top 11 and an outwardly convex bottom 13. The tank 10 is divided ~ 8 ~ ~
into an influent zone 15 and a filtrate zone 16 by a down-wardly curved tube sheet plate 17 suitably secured to the i.nterior of the tank 10 by welding or the like. The infl~ent line 12 extends through the bottom 13 of the tank and communi-cates with the influent zone 15 so that all the influentwater is passed directly to the influent zone 15. The in-fluent pipe 12 is attached to the tube ~heet plate 17 by welding or the like. In this manner, direct communication between the influent zone 15 and the filtrate zone 16 is precluded.
Mounted within the influent zone 15 are plurality of filter elements 18 through which the influent stream must pass before entering the filtrate zone 16 and being discharged from the filter tank 10 through the outlet iine 14. The filter elements 18 are annular-shapèd wound filter elements having a plurality of layers with controlled particle re-tention ability in accordance with the presènt invention.
Each filter element 18 is held in place in the influent zone 15 of the filter tank 1~ by a holding assembly indicated generally by reference numeral 20.~ This holding assembly is - ` adapted to releasably hold the filter element 18 in place upon a filter seat means 30 which are attached to the tube sheet plate 17. The filter elements 18 are placed into and removed from the filter tank 10 through a small manhole opening 22 in the filter tank lO. The manhole opening 22 has a cover means 24 which may be removed or opened, as desired, to provide access to thq interior of the filter tank 10 .
The filter tank 10 is also provided with a vent 26 and a spare noz~le 28, which in this instance i~ capped.
The vent 26 may be of any suitable construction, the selection of appropriate vent means being dependent generally upon the use of the filter tank 10 and being within the ordinary skill of one in the art.
The filter seat means 30 comprises a small pipe made of steel or the like which extends through a hole in the tube sheet plate 17 and i8 attached to the tube sheet plate 17 by welding or other suitable means. The filter seat means 30 i5 substantially parallel to the longitudinal axis of the filter tank 10 and provides communication between the lnfluent zone 15 with the filtrate zone 16. The filter seat means 30 provides a base for the filter element 18, which i8 held in position on the seat means 30 by the holding assembly 20. The filter elements 18 are typically fifty to eighty inches in length and one to three inches in outside diameter, and may consist of a unitary element or seYeral cartridges, usually ten inches in length, which are combined to form a single element.
A filter element 18 according to the present invention is illustrated in more detail in FIGURES 2 and 3. This element 18 includes a tubular support core 82 and a plurality of layers 84 and 86 of wound strand material. The tubular support core 82 i8 preferably constructed of stainleos steel, and provided with a plurality of symmetrically-spaced apertures to produce approximately twenty percent open area on the outer surface of the support core 82. The preferred range 8~7 of percent open area or perforation of the support core 82 is from five percent to sixty-five percent, and the inside diameter of the support core ~2 preferably is between 3/4 inch and 1 3/8 inch.
An innermost layer 84 and an outermost layer 86 are formed, as is known in the art, by winding a continuous strand of yarn or other strand material, such as nylon, orlon, poly-propylene, cotton, and the Like, onto the suppor~ core 82 in a helical fashion. The cross section of the yarn or ot~Ler strand material may be round, oval, triangular, or the like, as long as the particle retention ability according to the present invention is obtained. In fact, the cross-section of ; the yarn may vary as the yarn is wound, depending upon the proximity of adjacent strands and the winding tension.
~; 15 Spacing between adjacent strands of material is 1/16-inch or less, producing less than a one percent open area,-and allowing protruding fibers or other irregularities on the yarn surface to trap particles and thereby to augment the overall particle retention ability obtained by particle contact with the relatively solid twist of each yarn strand.
The particle re~ention ability of each layer of yarn or other material is dependent upon several factors in addition to spacing. The particle retention ability may be varied, for example, by varying the tension under which the yarn is wound,~
the thickness of each~layer of yarn, or by changing the pattern which is formed as the strand is wound back and : ::
~ forth. Ability to retain particles can also vary with yarn l:ype, yarn ma~erial, and with the way the yarn is handled.
For example, nylon yarn can be napped to produce a roughened surface, which affects the particle retention ability of the ultimate filter cartridge.
The manner in which the proper particle retention ability is produced is not important in the present invention, and most o the above-mentioned techniques are well known to those skilled in the art. However, it is essential that the filter element 18 be wound to produce the varying ability to retain particles as set forth herein and described by the phrase "nominal particle retention number." As used herein the nominal particle retention number of a filter element layer is the longest dimension of the smallest particle whose percent removal by the filter element layer is 90 or greater when the particles are introduced at a flow rate of
;~
)867 support core, an innermost layer of filter material disposed about the tubular core, and an outermost layer of filter material disposed about the inner layer. The outermost layer has the ability to trap smaller particles than the innermost layer. This ability, expressed in terms of the particle size, is called the nominal particle retention number.
In one broad aspect, the invention comprehends a filter element, precoated with particles in the size range of 60 to 400 mesh, consisting essentially of a perforated tubular core. An inner layer of strand material is wound about the core, the inner layer having a nomlnal particle retention number between twenty-five and one hundred microns, and an outer layer of strand material is wound about the inner layer, the outer layer having a nominal particle retention number between one and twenty-five microns.
A precoat of particles in the size range of 60 to 400 mesh is supported on the outer layer.
The invention further comprehends a filter element, precoated with particles in the size range of 60 to 400 mesh, comprising a perforated tubular core with a plurality of layers of strand material wound about the core. The nominal particle retention number of the innermost layer is greater than the nominal particle retention number of the outermost layer and eaah of the layers, in addition to the innermost layer, has a nominal particle retention number less than an adjacent inner layer. The filter element is provided with a plurality of layers having nominal particle retention numbers which gradually decrease from the innermost layer to the outermost layer, and a precoat of particles in the size range of 60 to 400 mesh supported on the outer layer.
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In another aspect, the lnvention comprises a method for purifying liquids comprising precoating a filter having layers of strand material with particles in the size range of about 60 to 400 mesh. The filter has an outermost layer with a nominal particle retention number less than the nominal particle retention number of the innermost layer of the ilter, with the nominal particle retention numbers gradually decreasing from the innermost layer to the outermost layer. The method delivers liquid to be filtered through the precoated particles and the fllter periodlcally backwashing the filter and removing the precoated partlcles, precoating the filter with a fresh coatlng of particles in the size range of about 60 to 400 mesh.
Such an arrangement of the windings, with the layer having the largest nominal particle retention number closest to the support core and the layer having the smallest nominal particle retention number furthest away from the support core, confines the area for filtering or purifying liquids ..~,.;~
passed through the filter elements to substantially the layer at the outer surface of the element. Such confinement of f:ilter area into a relatively thin annular volume is parti-cularly desirable when the filter element is used in filter UllitS in which the filter elements are precoated with finely divided resin particles in the size range of 60 to 400 mesh.
In precoated filter elements according to the in~ention, the area which has the tendency to foul is substantially re-duced, and undissolved particles will not be lodged tightly within the element below its outer surface so as ~o make them difficult to remove by backwash methods.
Also, if resin or other particles are forced through the outermost layer in the event of a flow surge of liquid through the element, the particles will become distributed throughout the layers of the wound element. In this manner, some particles will be trapped by the windings as a result of the circuitous path they take through the filter element, but the open area remaining for flow of liquid will not be diminished to a point where the filter's ability to pass liquid is significantly reduced.
According to the present invention, backwashing is also improved because the outermost layer presents a greater pressure barrier to backwash liquid coming from the support core than does the innermost layer of strand material.
Therefore, backwash liquid tends to distribute itself uni-formly along the length of the filter element when confronted with the increased pressure barrier produced by the outer layer.
~ 7 Other advantages, objects, and features of the present invention will become apparent upon reading the following detailed description of the preferred embodiment in con-junction with the accompanying drawings.
~RIEF DESCRIPTION OF THE DRAWINGS
FIGURE 1 is a partial cross-sectional view of a typical filter and tank having replaceable, cylindrical filter elements which embody the present invention;
FIGURE 2 is a perspective view of a filter element according to the present invention, par~ially cut away to show the wound layers of strand material and the central support core; and FIGURE 3 is a cross-sectional view of the filter element of FIGURE 2, taken along line 2-2, and illustrating the types of relationship of the wound layers of strand material to the central support core.
DESCRIPTION OF THE PREFERRED E~ODIMENT
Referring now to the drawings, and more particularly to FIGURE 1, a filtering~device which may be employed to carry out the method of the present invention is generally indicated by reference numeral 10. This device i9 of the type which i8 shown and described in U.S. Patent No~ 3,279,608, which is assigend to the assignee;of this application. The filtering device 10 is adapted to receive an influent stream, filter the influent stream, and discharge the filtrate or effluent stream.
The filter tank 10 is a generally cylindrical vessel made of steel or the like having an outwardly convex top 11 and an outwardly convex bottom 13. The tank 10 is divided ~ 8 ~ ~
into an influent zone 15 and a filtrate zone 16 by a down-wardly curved tube sheet plate 17 suitably secured to the i.nterior of the tank 10 by welding or the like. The infl~ent line 12 extends through the bottom 13 of the tank and communi-cates with the influent zone 15 so that all the influentwater is passed directly to the influent zone 15. The in-fluent pipe 12 is attached to the tube ~heet plate 17 by welding or the like. In this manner, direct communication between the influent zone 15 and the filtrate zone 16 is precluded.
Mounted within the influent zone 15 are plurality of filter elements 18 through which the influent stream must pass before entering the filtrate zone 16 and being discharged from the filter tank 10 through the outlet iine 14. The filter elements 18 are annular-shapèd wound filter elements having a plurality of layers with controlled particle re-tention ability in accordance with the presènt invention.
Each filter element 18 is held in place in the influent zone 15 of the filter tank 1~ by a holding assembly indicated generally by reference numeral 20.~ This holding assembly is - ` adapted to releasably hold the filter element 18 in place upon a filter seat means 30 which are attached to the tube sheet plate 17. The filter elements 18 are placed into and removed from the filter tank 10 through a small manhole opening 22 in the filter tank lO. The manhole opening 22 has a cover means 24 which may be removed or opened, as desired, to provide access to thq interior of the filter tank 10 .
The filter tank 10 is also provided with a vent 26 and a spare noz~le 28, which in this instance i~ capped.
The vent 26 may be of any suitable construction, the selection of appropriate vent means being dependent generally upon the use of the filter tank 10 and being within the ordinary skill of one in the art.
The filter seat means 30 comprises a small pipe made of steel or the like which extends through a hole in the tube sheet plate 17 and i8 attached to the tube sheet plate 17 by welding or other suitable means. The filter seat means 30 i5 substantially parallel to the longitudinal axis of the filter tank 10 and provides communication between the lnfluent zone 15 with the filtrate zone 16. The filter seat means 30 provides a base for the filter element 18, which i8 held in position on the seat means 30 by the holding assembly 20. The filter elements 18 are typically fifty to eighty inches in length and one to three inches in outside diameter, and may consist of a unitary element or seYeral cartridges, usually ten inches in length, which are combined to form a single element.
A filter element 18 according to the present invention is illustrated in more detail in FIGURES 2 and 3. This element 18 includes a tubular support core 82 and a plurality of layers 84 and 86 of wound strand material. The tubular support core 82 i8 preferably constructed of stainleos steel, and provided with a plurality of symmetrically-spaced apertures to produce approximately twenty percent open area on the outer surface of the support core 82. The preferred range 8~7 of percent open area or perforation of the support core 82 is from five percent to sixty-five percent, and the inside diameter of the support core ~2 preferably is between 3/4 inch and 1 3/8 inch.
An innermost layer 84 and an outermost layer 86 are formed, as is known in the art, by winding a continuous strand of yarn or other strand material, such as nylon, orlon, poly-propylene, cotton, and the Like, onto the suppor~ core 82 in a helical fashion. The cross section of the yarn or ot~Ler strand material may be round, oval, triangular, or the like, as long as the particle retention ability according to the present invention is obtained. In fact, the cross-section of ; the yarn may vary as the yarn is wound, depending upon the proximity of adjacent strands and the winding tension.
~; 15 Spacing between adjacent strands of material is 1/16-inch or less, producing less than a one percent open area,-and allowing protruding fibers or other irregularities on the yarn surface to trap particles and thereby to augment the overall particle retention ability obtained by particle contact with the relatively solid twist of each yarn strand.
The particle re~ention ability of each layer of yarn or other material is dependent upon several factors in addition to spacing. The particle retention ability may be varied, for example, by varying the tension under which the yarn is wound,~
the thickness of each~layer of yarn, or by changing the pattern which is formed as the strand is wound back and : ::
~ forth. Ability to retain particles can also vary with yarn l:ype, yarn ma~erial, and with the way the yarn is handled.
For example, nylon yarn can be napped to produce a roughened surface, which affects the particle retention ability of the ultimate filter cartridge.
The manner in which the proper particle retention ability is produced is not important in the present invention, and most o the above-mentioned techniques are well known to those skilled in the art. However, it is essential that the filter element 18 be wound to produce the varying ability to retain particles as set forth herein and described by the phrase "nominal particle retention number." As used herein the nominal particle retention number of a filter element layer is the longest dimension of the smallest particle whose percent removal by the filter element layer is 90 or greater when the particles are introduced at a flow rate of
3.5 gallons per minute per square foot in the form of Fine Arizona Air Dust in aqueous suspension at about 70 F. For example, if a filter element layer has a nominal particle retention number of 25 microns, then if a quantity of Fine Arizona Air Dust is passed through a filter element in aqueous suspension as described above, 90 percent or more of the particles having a maximum dimension of 25 microns or more will be retained by the filter layer. The influent con-centration of the Fine Arizona Air Dust is not critical, and tests have been run with a concentration of 100+25 milligrams per liter. -Fine Arizona Air Dust is a commercially available material which i9 utilized for making measurements of the type made herein~ The material i9 obtained from nat~ral Arizona dust, and prepared by A. C. Sparkplug division of 5 General Motors Corporation. It has the following particle distribution:
Micron Ran~e Percenta~ae 0-5 39+2 5-10 18+3 10 10-20 16+3 20-40 18+3 40-80 9+3 Any other material having the same particle distribution could also be employed in accordance with the present in-vèntion.
In the preferred embodiment of the invention, there are provided at least two layers of strand material, an outermost layer 86 and an innermost layer 84. As used herein, the term "layer" refers to windings of strand material sufficient to produce a desired nominal particle retention number uniformly along a filter element. Thus, a "layer" may include many overlapped strands of material, depending upon the partlcle winding pattern employed.
Conversely, one layer overlying another may not have any visible discrete separation from the underlying layer, having the same nominal particle retention number.
1~.2~867 The number of passes of the winding unit along the support core and the incremental lead sittings for the winding unit are determined by the desired particle retention ability. The nominal particle retention number of the outer-most layer 86 is less than the nominal particle retentionnumber of the innermost layer 84.
If layers àre included in the filter element 18 in addition to the innermost layer 84 and the outermost layer 86, it is preferred that each of the layers in addition to the innermost layer has a nominal particle retention number less than an adjacent inner layer. In this manner, the filter element 18 is provided with a plurality of layers having nominal particle retention numbers which decrease from the innermost layer 84 to the outermost layer 86.
- For use with filter units adapted to reduce impurities in water from about fifty parts per billion to about ten parts per billion, and precoated with a mixture of cation and anion exchange resins in the size range of 60 to 4Q0 mesh, the preferred embodiment of the invention includes an outermost layer 86 having a nominal particle retention number between one and twenty-five microns, and an innermost layer 84 having a nominal particle retention number between twenty-five and one hundred microns. According to this preferred arrange-ment of the invention, the filter element 18 is a surface filter, i.e., a filter with a m~nimal depth of working filter area, effectively equivalent to the depth af the outermost element layer 86.
~ .
~lZ~8~i7 According to the present invention, the innermost layer 84 of wound material provides improved back~ash flow distribution by adding to the prPssure drop across the path which backwash liquid must take before reaching the outer-most layer 86. Furthermore, the innermost layer 84 augments the area of the surface filter provided by the outermost layer 86, in a manner which is less expensive than increasing the diameter, and therefore the amount of material involved, in the core 82. This increased area markedly increases the efficient length of the run available before exhaustion of the filter element 18 in a comparison with a filter element having a primary fllter area near a relatively small diameter support core 82. The utilization of a filter element 18 according to the invention including an outermost layer 84 : 15 with a nominal particle retention number less than the ~ innermost layer 86 also provides the advantages of an inner : volume of wound layers which trap particles forced through ~- the outer st layer 86, particularly during flow surges of influent liquid. Such l'bleed-through" particles are ::~ 20 therefore usualLy trapped but do not significantly impair ~: fLow~af liquid through the filter in a service cycle direction~
In the operation of the apparatus shown in FIGURE 1, a water slurry of the precoat medium, in this instance finely divided ion exc~ange resin particles in the size range of ~: 25 about 60 to 400 mesh, is stored in a precoat tank 32. A
slurry line 34, controlled by a slurry valve 36, connects the precoat tank with a slurry pump 38. A transfer line :.
40 connects the pump 38 with the inlet line 12 of thé filter tank 10. A transfer valve 42 adjacent the pump 38 and in the transfer line 40 controls the passage of slurry or liquid from the pump 38.
The water to be treated enters the filter system through a feed line 44 having an intake control valve 46.
The feed line 44 is connected to the transfer line 40 between the control transfer valve 42 and the inlet line 12.
The outlet line 14 from the filter tank 10 is con-nected to a service line 48 and a precoat return line 50 at a T-juncture indicated by reference numeral 52. The service line 48 is connected to service units not shown, such as a steam generator and the like, and has a service valve 54.
The precoat return line 50 is connected to the precoat tank 32 and has a return valve 56 to control the flow of liquid ~back to the precoat tank 32.
A bridge line 58 with a bridge valve 60 interconnects the precoat return line 50 and the slurry line 34. A drain line 62 with a valve 64 communicates with the inlet line 12.
20 ~ During the precoating step a precoat layer of finely divided ion exchange resin particles in the size range of about 60 to 400 meah i9 deposited upon the upstream sides of the filter elements 18, i.e., the sides where thie water is : ~, introduced into the filter element 18. Similarly, during the filtering step a filter cake builds up within and on the upstream side of the precoat layer.
:, .
l~.Z~8~7 In preparing the fil~er system for operation the :initial s~ep is to precoat the filter elements 18. To these ends, the filter tank 10 is filled with low impurity water, such as demineralized water. A slurry of precoat medium and demineralized water is prepared in the precoat tank 32, the precoat medium being ion exchange resin particles in the size range of about 60 to 400 mesh.
During the precoating step all the valves are closed, except the slurry valve 36, the transfer valve 42, the return valve 56, and the bridge valve 60. The precoating step is Lnitiated by starting the pump 38, thereby drawing the resin precoat slurry from the precoat tank 32 and through the slurry line 34 to the pump 38. The slurry is forced by the pump 38 through the transfer line 40 and the inlet line 12 into the filter tank 10. The pressure of the incoming slurry forces the demineralized water in the filter tank lO
through the filters 18 and out of the filter tank 10 via the filtrate zone 16 and the outlet line 14. A portion of ~ demineralized water enters the precoat tank 32 through the :~ 20 return line 50~ and a second portion is delivered to the s~lurry line 54 through the bridge line 58.
As cycling continues the precoat slurry i9 brought into contact with the upstream surfaces of the filter elements ~: 18. The finely divided resin particles of the precoat medium ~ 25 are separated from the slurry and deposited as the precoat ;~: layer upon the upstream surfaces of the filter elements 18.
The slurry is circulated through the filter system in this J~ J. ?~ i 7 manner until a sufficient depth of the resin precoat layer is deposited upon the upstream surface of the filter elements 18. The precoating step is terminated by closing the slurry valve 36 and the return valve 56. Then the filter system is ready to be used to treat the feed water. The thickness of the precoat layer is not critical, but it is preferred that the layer have a thickness in the range of about l/16 to 2 inches, more preferably about 1/8 to 1 inch, ~nd most preferably 1/8 to 5/8 inch.
The service run is begun by opening the service valve 54 and the intake valve 46. In this manner, untreated water enters the filter system through the feed line 44 and passes through the transfer line 40 and the inlet line 12 into the filter tank 10. The pressure of the incoming untreated water forces it through the resin precoat layer, the filters 18 and the filtrate zone 16 into the outlet line 14 Following the establishment of the service flow, the transfer valve 42 and bridge valve 60 are closed and the pump 38 is stopped.
As the untreated water passes through the precoat layer, an ion exchange reaction takes place to remove dissolved impurities from the water. In addition, undissolved im-purities are removed from the untreated water by virtue of the water passing through the precoated filter elements 18.
Filter cake? consisting of the undissolved impurities, builds up within and on the precoat Iayèr as the process continues.
The purified or treated water flows through the filtrate zone 16 and the outlet line 14 to the service line 48.
~.~867 The purified water is directed to a supply tank or suitable ~equipment by the service line 48.
Eventually the resins will become exhausted and must be regenerated or discarded. At this time the filtering or S service cycle is stopped by closing the intake valve 46 and the service valve 54. The filter tank 10 is then cleaned.
To these ends, the vent 26 and the drain valve 64 are opened, and water plus a cleansing gas, usually air, are passed into the interior of the filter element 1~ at its lower end to clean the filter element 18 progressively from top to the bottom. The air is introduced into the interior of the filter element 18 by opening a valve 66 in an air line 68 communicating with the outlet line 14. At the same time, water is introduced into the filter element 18 by opening a valve 74 in the backwash line 76. Air under pressurè and backwash water thereby enter the filtrate zone 16 and pass upwardly into the interior of the filter element 18. Pre-ferably, the flow rate of the air is in the range of about 1 to 2 standard cubic feet per minute per square foot of filter surface area, while the water flow rate is about 0.5 gallons per minute per square foot of filter. The drain valve 62 is controlled 90 that the water level falls slowly, preferably at a rate of about 10-15 inches per minute. The air and water entering the filter tank 10 therefore tend to pass first through the upper portion of the filter element 18 and remove the precoat layer therefrom.
After the filter tank 10 has been drained, the drain valve 64 is closed, and the tank begins to refill with liquid, which passes in reverse flow through the filter element 18.
After t~e tank 10 fills to a level about six inches above S the tops of the filter element 18, the valves 66, 74 in the air line 68 and backwash line 76 are closed, and the backwash water is removed from the tank 10 by opening the valve 64.
The drain valve 64 is closed, and the filter elements 18 are again backwashed by opening the valves 66, 74 on the air line 68 and backwash line 76, respectively. A somewhat higher liquid flow rate, e.g., 1-2 gallons per minute per square foot of filter, is employed during this step. Air is also delivered at about 1.5 standard cubic feet per minute per square foot. After the tank lO has filled to a level above the tops of the filter element 18, the drain valve 64 is again opened to permit the liquid level to fa~l at a rate of about ten to fifteen inches per minute, whil~
the flow of air and backwash liquid is continued. The back-wash valve 74 is closed, and draining with the introduction of air only is continued for a short time to assure complete draining. After the tank lO empties, the drain valve 6 and the air valve 66 are closed. The backwash valve 74 i5 opened, and the tank is permitted to fill for a third time.
After the tank 10 has filled, vent 26 and valve 74 on the backwash line are closed. The tank 10 is filled wit'n water, and the filter elements 18 are now ready for the application of a new precoat, as previously described.
~ 6 7 Though air has been discussed as the cleansing gas, other gases may be used a~ the cleansing gas, such as nitrogen, oxygen and the like. Air, however, is generally ~peaking, the most economical as it i~ readily available in most plants.
Similarly, liquids other than water may be used during the backwashing cycle. Exemplary of such liquid~ are alcohols, carbon tetrachloride and detergent and soap solutions. It is preferred that the liquids have a temperature in the range of about 100 to 200 F.
Typical solid cation exchange resin particles which may be employed in the specific filtering method discussed herein are the divinylbenzene-styrene copolymer type, the acrylic type, the sulfonated coal type and the phenolic type.
These may be used in the sodium, hydrogen, or ammonium form, for example. Typical solid anion exchange resin particles that may be employed are the phenolformaldehyde type, the divinylbenzene-styrene copolymer type, the acrylic type and the epoxy type. The anion resin particles may be used in the hydroxide or chloride form, for example. Suitable resins are sold co~mercially in the large bead form under the trade marks Amberline IR-120 and Amberline LRA-400, sold by Rohm & Haas Company; and Dowex HCR-S and Dowex SBR-P, sold by Dow Chemical Company. The finely divided resins are prepared by reducing the particle size of these well known large bead resins to the desired size range. These resin particles are regenerated and washed prior to use.
)867 Though the filtering method has been discussed in relation to precoat layer of finely divided ion exchange precoat particles, the method is likewise applicable where the precoat layer is treated or untreated diatomaceous earth, cellulose fibers, polyacrylonitrile fibers, or any other precoat material, as will be understood by one with ordinary skill in the art. Moreover, though the embodiments herein-before described are preferred, many modifications and refine-ments which do not depart from the true spirit and scope of the present invention may be conceived by those skilled in the art. It is intended that all such modifications be covered by the following claims.
:
:: ~
~ ~ .
.
Micron Ran~e Percenta~ae 0-5 39+2 5-10 18+3 10 10-20 16+3 20-40 18+3 40-80 9+3 Any other material having the same particle distribution could also be employed in accordance with the present in-vèntion.
In the preferred embodiment of the invention, there are provided at least two layers of strand material, an outermost layer 86 and an innermost layer 84. As used herein, the term "layer" refers to windings of strand material sufficient to produce a desired nominal particle retention number uniformly along a filter element. Thus, a "layer" may include many overlapped strands of material, depending upon the partlcle winding pattern employed.
Conversely, one layer overlying another may not have any visible discrete separation from the underlying layer, having the same nominal particle retention number.
1~.2~867 The number of passes of the winding unit along the support core and the incremental lead sittings for the winding unit are determined by the desired particle retention ability. The nominal particle retention number of the outer-most layer 86 is less than the nominal particle retentionnumber of the innermost layer 84.
If layers àre included in the filter element 18 in addition to the innermost layer 84 and the outermost layer 86, it is preferred that each of the layers in addition to the innermost layer has a nominal particle retention number less than an adjacent inner layer. In this manner, the filter element 18 is provided with a plurality of layers having nominal particle retention numbers which decrease from the innermost layer 84 to the outermost layer 86.
- For use with filter units adapted to reduce impurities in water from about fifty parts per billion to about ten parts per billion, and precoated with a mixture of cation and anion exchange resins in the size range of 60 to 4Q0 mesh, the preferred embodiment of the invention includes an outermost layer 86 having a nominal particle retention number between one and twenty-five microns, and an innermost layer 84 having a nominal particle retention number between twenty-five and one hundred microns. According to this preferred arrange-ment of the invention, the filter element 18 is a surface filter, i.e., a filter with a m~nimal depth of working filter area, effectively equivalent to the depth af the outermost element layer 86.
~ .
~lZ~8~i7 According to the present invention, the innermost layer 84 of wound material provides improved back~ash flow distribution by adding to the prPssure drop across the path which backwash liquid must take before reaching the outer-most layer 86. Furthermore, the innermost layer 84 augments the area of the surface filter provided by the outermost layer 86, in a manner which is less expensive than increasing the diameter, and therefore the amount of material involved, in the core 82. This increased area markedly increases the efficient length of the run available before exhaustion of the filter element 18 in a comparison with a filter element having a primary fllter area near a relatively small diameter support core 82. The utilization of a filter element 18 according to the invention including an outermost layer 84 : 15 with a nominal particle retention number less than the ~ innermost layer 86 also provides the advantages of an inner : volume of wound layers which trap particles forced through ~- the outer st layer 86, particularly during flow surges of influent liquid. Such l'bleed-through" particles are ::~ 20 therefore usualLy trapped but do not significantly impair ~: fLow~af liquid through the filter in a service cycle direction~
In the operation of the apparatus shown in FIGURE 1, a water slurry of the precoat medium, in this instance finely divided ion exc~ange resin particles in the size range of ~: 25 about 60 to 400 mesh, is stored in a precoat tank 32. A
slurry line 34, controlled by a slurry valve 36, connects the precoat tank with a slurry pump 38. A transfer line :.
40 connects the pump 38 with the inlet line 12 of thé filter tank 10. A transfer valve 42 adjacent the pump 38 and in the transfer line 40 controls the passage of slurry or liquid from the pump 38.
The water to be treated enters the filter system through a feed line 44 having an intake control valve 46.
The feed line 44 is connected to the transfer line 40 between the control transfer valve 42 and the inlet line 12.
The outlet line 14 from the filter tank 10 is con-nected to a service line 48 and a precoat return line 50 at a T-juncture indicated by reference numeral 52. The service line 48 is connected to service units not shown, such as a steam generator and the like, and has a service valve 54.
The precoat return line 50 is connected to the precoat tank 32 and has a return valve 56 to control the flow of liquid ~back to the precoat tank 32.
A bridge line 58 with a bridge valve 60 interconnects the precoat return line 50 and the slurry line 34. A drain line 62 with a valve 64 communicates with the inlet line 12.
20 ~ During the precoating step a precoat layer of finely divided ion exchange resin particles in the size range of about 60 to 400 meah i9 deposited upon the upstream sides of the filter elements 18, i.e., the sides where thie water is : ~, introduced into the filter element 18. Similarly, during the filtering step a filter cake builds up within and on the upstream side of the precoat layer.
:, .
l~.Z~8~7 In preparing the fil~er system for operation the :initial s~ep is to precoat the filter elements 18. To these ends, the filter tank 10 is filled with low impurity water, such as demineralized water. A slurry of precoat medium and demineralized water is prepared in the precoat tank 32, the precoat medium being ion exchange resin particles in the size range of about 60 to 400 mesh.
During the precoating step all the valves are closed, except the slurry valve 36, the transfer valve 42, the return valve 56, and the bridge valve 60. The precoating step is Lnitiated by starting the pump 38, thereby drawing the resin precoat slurry from the precoat tank 32 and through the slurry line 34 to the pump 38. The slurry is forced by the pump 38 through the transfer line 40 and the inlet line 12 into the filter tank 10. The pressure of the incoming slurry forces the demineralized water in the filter tank lO
through the filters 18 and out of the filter tank 10 via the filtrate zone 16 and the outlet line 14. A portion of ~ demineralized water enters the precoat tank 32 through the :~ 20 return line 50~ and a second portion is delivered to the s~lurry line 54 through the bridge line 58.
As cycling continues the precoat slurry i9 brought into contact with the upstream surfaces of the filter elements ~: 18. The finely divided resin particles of the precoat medium ~ 25 are separated from the slurry and deposited as the precoat ;~: layer upon the upstream surfaces of the filter elements 18.
The slurry is circulated through the filter system in this J~ J. ?~ i 7 manner until a sufficient depth of the resin precoat layer is deposited upon the upstream surface of the filter elements 18. The precoating step is terminated by closing the slurry valve 36 and the return valve 56. Then the filter system is ready to be used to treat the feed water. The thickness of the precoat layer is not critical, but it is preferred that the layer have a thickness in the range of about l/16 to 2 inches, more preferably about 1/8 to 1 inch, ~nd most preferably 1/8 to 5/8 inch.
The service run is begun by opening the service valve 54 and the intake valve 46. In this manner, untreated water enters the filter system through the feed line 44 and passes through the transfer line 40 and the inlet line 12 into the filter tank 10. The pressure of the incoming untreated water forces it through the resin precoat layer, the filters 18 and the filtrate zone 16 into the outlet line 14 Following the establishment of the service flow, the transfer valve 42 and bridge valve 60 are closed and the pump 38 is stopped.
As the untreated water passes through the precoat layer, an ion exchange reaction takes place to remove dissolved impurities from the water. In addition, undissolved im-purities are removed from the untreated water by virtue of the water passing through the precoated filter elements 18.
Filter cake? consisting of the undissolved impurities, builds up within and on the precoat Iayèr as the process continues.
The purified or treated water flows through the filtrate zone 16 and the outlet line 14 to the service line 48.
~.~867 The purified water is directed to a supply tank or suitable ~equipment by the service line 48.
Eventually the resins will become exhausted and must be regenerated or discarded. At this time the filtering or S service cycle is stopped by closing the intake valve 46 and the service valve 54. The filter tank 10 is then cleaned.
To these ends, the vent 26 and the drain valve 64 are opened, and water plus a cleansing gas, usually air, are passed into the interior of the filter element 1~ at its lower end to clean the filter element 18 progressively from top to the bottom. The air is introduced into the interior of the filter element 18 by opening a valve 66 in an air line 68 communicating with the outlet line 14. At the same time, water is introduced into the filter element 18 by opening a valve 74 in the backwash line 76. Air under pressurè and backwash water thereby enter the filtrate zone 16 and pass upwardly into the interior of the filter element 18. Pre-ferably, the flow rate of the air is in the range of about 1 to 2 standard cubic feet per minute per square foot of filter surface area, while the water flow rate is about 0.5 gallons per minute per square foot of filter. The drain valve 62 is controlled 90 that the water level falls slowly, preferably at a rate of about 10-15 inches per minute. The air and water entering the filter tank 10 therefore tend to pass first through the upper portion of the filter element 18 and remove the precoat layer therefrom.
After the filter tank 10 has been drained, the drain valve 64 is closed, and the tank begins to refill with liquid, which passes in reverse flow through the filter element 18.
After t~e tank 10 fills to a level about six inches above S the tops of the filter element 18, the valves 66, 74 in the air line 68 and backwash line 76 are closed, and the backwash water is removed from the tank 10 by opening the valve 64.
The drain valve 64 is closed, and the filter elements 18 are again backwashed by opening the valves 66, 74 on the air line 68 and backwash line 76, respectively. A somewhat higher liquid flow rate, e.g., 1-2 gallons per minute per square foot of filter, is employed during this step. Air is also delivered at about 1.5 standard cubic feet per minute per square foot. After the tank lO has filled to a level above the tops of the filter element 18, the drain valve 64 is again opened to permit the liquid level to fa~l at a rate of about ten to fifteen inches per minute, whil~
the flow of air and backwash liquid is continued. The back-wash valve 74 is closed, and draining with the introduction of air only is continued for a short time to assure complete draining. After the tank lO empties, the drain valve 6 and the air valve 66 are closed. The backwash valve 74 i5 opened, and the tank is permitted to fill for a third time.
After the tank 10 has filled, vent 26 and valve 74 on the backwash line are closed. The tank 10 is filled wit'n water, and the filter elements 18 are now ready for the application of a new precoat, as previously described.
~ 6 7 Though air has been discussed as the cleansing gas, other gases may be used a~ the cleansing gas, such as nitrogen, oxygen and the like. Air, however, is generally ~peaking, the most economical as it i~ readily available in most plants.
Similarly, liquids other than water may be used during the backwashing cycle. Exemplary of such liquid~ are alcohols, carbon tetrachloride and detergent and soap solutions. It is preferred that the liquids have a temperature in the range of about 100 to 200 F.
Typical solid cation exchange resin particles which may be employed in the specific filtering method discussed herein are the divinylbenzene-styrene copolymer type, the acrylic type, the sulfonated coal type and the phenolic type.
These may be used in the sodium, hydrogen, or ammonium form, for example. Typical solid anion exchange resin particles that may be employed are the phenolformaldehyde type, the divinylbenzene-styrene copolymer type, the acrylic type and the epoxy type. The anion resin particles may be used in the hydroxide or chloride form, for example. Suitable resins are sold co~mercially in the large bead form under the trade marks Amberline IR-120 and Amberline LRA-400, sold by Rohm & Haas Company; and Dowex HCR-S and Dowex SBR-P, sold by Dow Chemical Company. The finely divided resins are prepared by reducing the particle size of these well known large bead resins to the desired size range. These resin particles are regenerated and washed prior to use.
)867 Though the filtering method has been discussed in relation to precoat layer of finely divided ion exchange precoat particles, the method is likewise applicable where the precoat layer is treated or untreated diatomaceous earth, cellulose fibers, polyacrylonitrile fibers, or any other precoat material, as will be understood by one with ordinary skill in the art. Moreover, though the embodiments herein-before described are preferred, many modifications and refine-ments which do not depart from the true spirit and scope of the present invention may be conceived by those skilled in the art. It is intended that all such modifications be covered by the following claims.
:
:: ~
~ ~ .
.
Claims (5)
1. A filter element, precoated with particles in the size range of 60 to 400 mesh, consisting essentially of a perforated tubular core;
an inner layer of strand material wound about said core, said inner layer having a nominal particle retention number between twenty-five and one hundred microns;
an outer layer of strand material, wound about said inner layer, said outer layer having a nominal particle retention number between one and twenty-five microns;
and a precoat of particles in the size range of 60 to 400 mesh supported on said outer layer.
an inner layer of strand material wound about said core, said inner layer having a nominal particle retention number between twenty-five and one hundred microns;
an outer layer of strand material, wound about said inner layer, said outer layer having a nominal particle retention number between one and twenty-five microns;
and a precoat of particles in the size range of 60 to 400 mesh supported on said outer layer.
2. A filter element, precoated with particles in the size range of 60 to 400 mesh, comprising:
a perforated tubular core;
a plurality of layers of strand material, wound about said core, the nominal particle retention number of the innermost layer being greater than the nominal particle retention number of the outermost layer and wherein each of said layers in addition to said innermost layer has a nominal particle retention number less than an adjacent inner layer, whereby the filter element is provided with a plurality of layers having nominal particle retention numbers which gradually decrease from the innermost layer to the outermost layer; and a precoat of particles in the size range of 60 to 400 mesh supported on said outer layer.
a perforated tubular core;
a plurality of layers of strand material, wound about said core, the nominal particle retention number of the innermost layer being greater than the nominal particle retention number of the outermost layer and wherein each of said layers in addition to said innermost layer has a nominal particle retention number less than an adjacent inner layer, whereby the filter element is provided with a plurality of layers having nominal particle retention numbers which gradually decrease from the innermost layer to the outermost layer; and a precoat of particles in the size range of 60 to 400 mesh supported on said outer layer.
3. A method for purifying liquids comprising:
precoating a filter having layers of strand material with particles in the size range of about 60 to 400 mesh, said filter having an outermost layer with a nominal particle retention number less than the nominal particle retention number of the innermost layer of said filter with the nominal particle retention numbers gradually decreasing from the innermost layer to the outermost layer; delivering liquid to be filtered through said precoated particles and said filter; periodically backwashing said filter and removing said precoated particles; and precoating said filter with a fresh coating of particles in the size range of about 60 to 400 mesh.
precoating a filter having layers of strand material with particles in the size range of about 60 to 400 mesh, said filter having an outermost layer with a nominal particle retention number less than the nominal particle retention number of the innermost layer of said filter with the nominal particle retention numbers gradually decreasing from the innermost layer to the outermost layer; delivering liquid to be filtered through said precoated particles and said filter; periodically backwashing said filter and removing said precoated particles; and precoating said filter with a fresh coating of particles in the size range of about 60 to 400 mesh.
4. The method as defined in Claim 3 wherein said filter is an annular, wound filter.
5. The method as defined in Claim 3 or Claim 4, wherein the nominal particle retention number of the outermost layer is between one and twenty-five microns, and the nominal particle retention number of the innermost layer is between twenty-five and one hundred microns.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US88470778A | 1978-03-08 | 1978-03-08 | |
US884,707 | 1978-03-08 |
Publications (1)
Publication Number | Publication Date |
---|---|
CA1120867A true CA1120867A (en) | 1982-03-30 |
Family
ID=25385201
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA000319714A Expired CA1120867A (en) | 1978-03-08 | 1979-01-16 | Two layer wound-on-core medium filter element |
Country Status (11)
Country | Link |
---|---|
JP (1) | JPS54127078A (en) |
AU (1) | AU522606B2 (en) |
CA (1) | CA1120867A (en) |
DE (1) | DE2908625A1 (en) |
ES (1) | ES477868A1 (en) |
FR (1) | FR2419098A1 (en) |
GB (1) | GB2015890B (en) |
IT (1) | IT1114568B (en) |
MX (1) | MX5816E (en) |
SE (1) | SE7901870L (en) |
ZA (1) | ZA79249B (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102921207A (en) * | 2012-11-09 | 2013-02-13 | 无锡电站辅机厂 | Powdered resin covered filter |
CN110913968A (en) * | 2017-07-25 | 2020-03-24 | 罗伯特·博世有限公司 | Liquid filter and box-type filtering system with liquid filter |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0032228A3 (en) * | 1980-01-10 | 1982-03-31 | Filtrox Maschinenbau A.-G. | Use of porous filter tubes in precoat candle filters |
EP0063412A1 (en) * | 1981-04-16 | 1982-10-27 | The Duriron Company, Inc. | Filter leaf |
AU584743B2 (en) * | 1986-01-31 | 1989-06-01 | Schewitz, Jonathan | Filtering unit |
DE3763365D1 (en) * | 1986-04-16 | 1990-08-02 | Sapporo Breweries | FILTER APPARATUS. |
US4904380A (en) * | 1988-01-26 | 1990-02-27 | Pall Corporation | Precoat filter assembly |
JP2506922Y2 (en) * | 1989-09-08 | 1996-08-14 | 石垣機工株式会社 | Precision ▲ ro ▼ |
US5543047A (en) | 1992-11-06 | 1996-08-06 | Pall Corporation | Filter with over-laid pleats in intimate contact |
JPH0724226A (en) * | 1993-07-15 | 1995-01-27 | Fuji Photo Film Co Ltd | Method for filtering thixotropic liquid and filter thereof |
CN103566642B (en) * | 2013-11-12 | 2015-06-24 | 上海龙净环保科技工程有限公司 | Filter element type automatic backwash filtering device and process |
CN107427747A (en) * | 2015-03-04 | 2017-12-01 | 株式会社可乐丽 | The manufacture method and ballast water treatment system of ballast water |
SE542419C2 (en) * | 2017-02-07 | 2020-04-28 | Scania Cv Ab | Reducing agent dosing unit comprising a pump device and a liquid filter device |
CN110724556A (en) * | 2018-07-16 | 2020-01-24 | 中国石油天然气股份有限公司 | A filter sled dress device that is arranged in defeated product oil of pipe to handle mechanical impurity |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1206566A (en) * | 1968-04-22 | 1970-09-23 | F W Dwyer Mfg Co Inc | Improvements in flowmeters |
GB1271867A (en) * | 1968-10-04 | 1972-04-26 | Amf Inc | Filter element |
-
1979
- 1979-01-16 CA CA000319714A patent/CA1120867A/en not_active Expired
- 1979-01-22 ZA ZA79249A patent/ZA79249B/en unknown
- 1979-01-24 AU AU43609/79A patent/AU522606B2/en not_active Ceased
- 1979-02-20 ES ES477868A patent/ES477868A1/en not_active Expired
- 1979-02-23 FR FR7904684A patent/FR2419098A1/en active Granted
- 1979-02-28 GB GB7907075A patent/GB2015890B/en not_active Expired
- 1979-03-01 SE SE7901870A patent/SE7901870L/en unknown
- 1979-03-05 MX MX797782U patent/MX5816E/en unknown
- 1979-03-06 IT IT48224/79A patent/IT1114568B/en active
- 1979-03-06 DE DE19792908625 patent/DE2908625A1/en not_active Withdrawn
- 1979-03-08 JP JP2723579A patent/JPS54127078A/en active Granted
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102921207A (en) * | 2012-11-09 | 2013-02-13 | 无锡电站辅机厂 | Powdered resin covered filter |
CN110913968A (en) * | 2017-07-25 | 2020-03-24 | 罗伯特·博世有限公司 | Liquid filter and box-type filtering system with liquid filter |
CN110913968B (en) * | 2017-07-25 | 2022-02-22 | 罗伯特·博世有限公司 | Liquid filter and box-type filtering system with liquid filter |
US11325061B2 (en) | 2017-07-25 | 2022-05-10 | Robert Bosch Gmbh | Liquid filter and tank filter system including a liquid filter |
Also Published As
Publication number | Publication date |
---|---|
IT7948224A0 (en) | 1979-03-06 |
ES477868A1 (en) | 1980-04-01 |
GB2015890A (en) | 1979-09-19 |
GB2015890B (en) | 1982-06-23 |
AU4360979A (en) | 1979-09-13 |
IT1114568B (en) | 1986-01-27 |
FR2419098A1 (en) | 1979-10-05 |
FR2419098B3 (en) | 1981-12-11 |
MX5816E (en) | 1984-07-27 |
SE7901870L (en) | 1979-09-09 |
ZA79249B (en) | 1980-04-30 |
JPS6240048B2 (en) | 1987-08-26 |
AU522606B2 (en) | 1982-06-17 |
JPS54127078A (en) | 1979-10-02 |
DE2908625A1 (en) | 1979-09-13 |
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