CA1112930A - Line injection hardening using glutaraldehyde derivatives - Google Patents
Line injection hardening using glutaraldehyde derivativesInfo
- Publication number
- CA1112930A CA1112930A CA289,557A CA289557A CA1112930A CA 1112930 A CA1112930 A CA 1112930A CA 289557 A CA289557 A CA 289557A CA 1112930 A CA1112930 A CA 1112930A
- Authority
- CA
- Canada
- Prior art keywords
- glutaraldehyde
- hardening
- hardener
- added
- emulsion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- SXRSQZLOMIGNAQ-UHFFFAOYSA-N Glutaraldehyde Chemical class O=CCCCC=O SXRSQZLOMIGNAQ-UHFFFAOYSA-N 0.000 title claims abstract description 19
- 238000002347 injection Methods 0.000 title 1
- 239000007924 injection Substances 0.000 title 1
- 239000000839 emulsion Substances 0.000 claims abstract description 34
- 238000000034 method Methods 0.000 claims abstract description 20
- 229910052709 silver Inorganic materials 0.000 claims abstract description 11
- 239000004332 silver Substances 0.000 claims abstract description 11
- 239000004848 polyfunctional curative Substances 0.000 claims description 26
- 108010010803 Gelatin Proteins 0.000 claims description 13
- 229920000159 gelatin Polymers 0.000 claims description 13
- 239000008273 gelatin Substances 0.000 claims description 13
- 235000019322 gelatine Nutrition 0.000 claims description 13
- 235000011852 gelatine desserts Nutrition 0.000 claims description 13
- -1 silver halide Chemical class 0.000 claims description 10
- 150000003839 salts Chemical class 0.000 claims description 5
- JEHKKBHWRAXMCH-UHFFFAOYSA-N benzenesulfinic acid Chemical compound O[S@@](=O)C1=CC=CC=C1 JEHKKBHWRAXMCH-UHFFFAOYSA-N 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 3
- 125000001931 aliphatic group Chemical group 0.000 claims description 2
- 239000011248 coating agent Substances 0.000 claims description 2
- 238000000576 coating method Methods 0.000 claims description 2
- BUUPQKDIAURBJP-UHFFFAOYSA-N sulfinic acid Chemical compound OS=O BUUPQKDIAURBJP-UHFFFAOYSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- 238000005266 casting Methods 0.000 abstract description 12
- 239000000243 solution Substances 0.000 description 9
- LEQAOMBKQFMDFZ-UHFFFAOYSA-N alpha-ketodiacetal Natural products O=CC=O LEQAOMBKQFMDFZ-UHFFFAOYSA-N 0.000 description 8
- 230000035945 sensitivity Effects 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 4
- 229940015043 glyoxal Drugs 0.000 description 4
- 238000002844 melting Methods 0.000 description 4
- 230000008018 melting Effects 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- PCSMJKASWLYICJ-UHFFFAOYSA-N Succinic aldehyde Chemical compound O=CCCC=O PCSMJKASWLYICJ-UHFFFAOYSA-N 0.000 description 3
- 125000003172 aldehyde group Chemical group 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000011156 evaluation Methods 0.000 description 3
- 230000002349 favourable effect Effects 0.000 description 3
- 239000003381 stabilizer Substances 0.000 description 3
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- OIPQUBBCOVJSNS-UHFFFAOYSA-L bromo(iodo)silver Chemical compound Br[Ag]I OIPQUBBCOVJSNS-UHFFFAOYSA-L 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 238000010517 secondary reaction Methods 0.000 description 2
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 2
- 150000003455 sulfinic acids Chemical class 0.000 description 2
- IQKPRZPVTQHVOY-UHFFFAOYSA-N 2-methylpentanedial Chemical compound O=CC(C)CCC=O IQKPRZPVTQHVOY-UHFFFAOYSA-N 0.000 description 1
- ZNZYKNKBJPZETN-WELNAUFTSA-N Dialdehyde 11678 Chemical compound N1C2=CC=CC=C2C2=C1[C@H](C[C@H](/C(=C/O)C(=O)OC)[C@@H](C=C)C=O)NCC2 ZNZYKNKBJPZETN-WELNAUFTSA-N 0.000 description 1
- 229910003252 NaBO2 Inorganic materials 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 229910021607 Silver chloride Inorganic materials 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- NVSONFIVLCXXDH-UHFFFAOYSA-N benzylsulfinic acid Chemical class O[S@@](=O)CC1=CC=CC=C1 NVSONFIVLCXXDH-UHFFFAOYSA-N 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000266 injurious effect Effects 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 description 1
- NVIFVTYDZMXWGX-UHFFFAOYSA-N sodium metaborate Chemical compound [Na+].[O-]B=O NVIFVTYDZMXWGX-UHFFFAOYSA-N 0.000 description 1
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 1
- 235000010265 sodium sulphite Nutrition 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/005—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
- G03C1/06—Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein with non-macromolecular additives
- G03C1/30—Hardeners
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S430/00—Radiation imagery chemistry: process, composition, or product thereof
- Y10S430/136—Coating process making radiation sensitive element
Landscapes
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- General Physics & Mathematics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEP2648286.0 | 1976-10-26 | ||
| DE2648286A DE2648286C3 (de) | 1976-10-26 | 1976-10-26 | Verfahren zum Härten von photographischen Silberhalogenidemulsionen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1112930A true CA1112930A (en) | 1981-11-24 |
Family
ID=5991344
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA289,557A Expired CA1112930A (en) | 1976-10-26 | 1977-10-26 | Line injection hardening using glutaraldehyde derivatives |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4124397A (Direct) |
| JP (1) | JPS5355022A (Direct) |
| BE (1) | BE860099A (Direct) |
| CA (1) | CA1112930A (Direct) |
| DE (1) | DE2648286C3 (Direct) |
| FR (1) | FR2369588A1 (Direct) |
| GB (1) | GB1541816A (Direct) |
| IT (1) | IT1087647B (Direct) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4175970A (en) * | 1978-07-24 | 1979-11-27 | E. I. Du Pont De Nemours And Company | Process for sensitizing photographic silver halide emulsions |
| US4241171A (en) * | 1979-02-21 | 1980-12-23 | Polaroid Corporation | Hardener in carrier layer |
| US4383030A (en) * | 1981-04-27 | 1983-05-10 | E. I. Du Pont De Nemours And Company | Low coating weight silver halide element using mix sensitization techniques |
| US4499182A (en) * | 1983-10-11 | 1985-02-12 | E. I. Du Pont De Nemours And Company | In situ film hardening with pyridinium chlorochromate and aldehyde precursor alcohol |
| EP0318909B1 (en) | 1987-11-30 | 1993-09-15 | E.I. Du Pont De Nemours And Company | Photographic film antistatic backing layer with auxiliary layer having improved properties |
| US4960687A (en) | 1989-09-29 | 1990-10-02 | E. I. Du Pont De Nemours And Company | Process of making photographic silver halide element with backing layers with improved coating properties |
| JPH0649434A (ja) * | 1992-06-01 | 1994-02-22 | Eastman Kodak Co | ゼラチン溶液用迅速作用性増粘剤 |
| US5445913A (en) * | 1994-02-25 | 1995-08-29 | Eastman Kodak Company | Process for the formation of heat image separation elements of improved sensitometry |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE606528C (de) * | 1933-07-23 | 1934-12-04 | I G Farbenindustrie Akt Ges | Verfahren zur Stabilisierung photographischer Emulsionen |
| US3342605A (en) * | 1963-10-07 | 1967-09-19 | Eastman Kodak Co | Incorporation of certain addenda into aqueous gelatin solutions |
| US3232764A (en) * | 1965-05-25 | 1966-02-01 | Eastman Kodak Co | Gelatin compositions adapted for the preparation of hardened coatings |
-
1976
- 1976-10-26 DE DE2648286A patent/DE2648286C3/de not_active Expired
-
1977
- 1977-09-26 US US05/836,840 patent/US4124397A/en not_active Expired - Lifetime
- 1977-10-25 FR FR7732039A patent/FR2369588A1/fr active Granted
- 1977-10-25 IT IT28983/77A patent/IT1087647B/it active
- 1977-10-25 GB GB44444/77A patent/GB1541816A/en not_active Expired
- 1977-10-26 BE BE182046A patent/BE860099A/xx not_active IP Right Cessation
- 1977-10-26 CA CA289,557A patent/CA1112930A/en not_active Expired
- 1977-10-26 JP JP12767877A patent/JPS5355022A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| BE860099A (fr) | 1978-04-26 |
| DE2648286B2 (de) | 1981-05-21 |
| DE2648286A1 (de) | 1978-04-27 |
| DE2648286C3 (de) | 1982-01-28 |
| GB1541816A (en) | 1979-03-07 |
| FR2369588A1 (fr) | 1978-05-26 |
| JPS5355022A (en) | 1978-05-19 |
| FR2369588B1 (Direct) | 1981-12-18 |
| IT1087647B (it) | 1985-06-04 |
| JPS5648861B2 (Direct) | 1981-11-18 |
| US4124397A (en) | 1978-11-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |