CA1059733A - Apparatus for the production of sugars from hemi-cellulose-containing raw materials - Google Patents
Apparatus for the production of sugars from hemi-cellulose-containing raw materialsInfo
- Publication number
- CA1059733A CA1059733A CA240,898A CA240898A CA1059733A CA 1059733 A CA1059733 A CA 1059733A CA 240898 A CA240898 A CA 240898A CA 1059733 A CA1059733 A CA 1059733A
- Authority
- CA
- Canada
- Prior art keywords
- vessel
- raw material
- impregnating
- steam
- reaction vessel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000002994 raw material Substances 0.000 title claims abstract description 86
- 235000000346 sugar Nutrition 0.000 title claims abstract description 27
- 229920002488 Hemicellulose Polymers 0.000 title claims abstract description 12
- 150000008163 sugars Chemical class 0.000 title claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 title abstract description 11
- 238000006243 chemical reaction Methods 0.000 claims abstract description 63
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000002253 acid Substances 0.000 claims abstract description 23
- 238000000605 extraction Methods 0.000 claims description 42
- 238000013022 venting Methods 0.000 claims description 41
- 230000007062 hydrolysis Effects 0.000 claims description 23
- 238000006460 hydrolysis reaction Methods 0.000 claims description 23
- 239000011148 porous material Substances 0.000 claims description 10
- 238000003860 storage Methods 0.000 claims description 9
- 238000010924 continuous production Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000004062 sedimentation Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 abstract description 17
- SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 abstract description 14
- 239000002245 particle Substances 0.000 abstract description 9
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 abstract description 7
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 abstract description 7
- 229920001221 xylan Polymers 0.000 abstract description 3
- 150000004823 xylans Chemical class 0.000 abstract description 3
- 239000000047 product Substances 0.000 description 15
- 238000000034 method Methods 0.000 description 6
- 239000000945 filler Substances 0.000 description 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 230000005484 gravity Effects 0.000 description 3
- 229920000136 polysorbate Polymers 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 241001070947 Fagus Species 0.000 description 2
- 235000010099 Fagus sylvatica Nutrition 0.000 description 2
- 208000036366 Sensation of pressure Diseases 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 238000005470 impregnation Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 101100119767 Caenorhabditis elegans fat-4 gene Proteins 0.000 description 1
- 101100468762 Caenorhabditis elegans ric-3 gene Proteins 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 230000036647 reaction Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K13/00—Sugars not otherwise provided for in this class
- C13K13/002—Xylose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Extraction Or Liquid Replacement (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH1599974A CH585794A5 (enExample) | 1974-12-03 | 1974-12-03 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1059733A true CA1059733A (en) | 1979-08-07 |
Family
ID=4413683
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA240,898A Expired CA1059733A (en) | 1974-12-03 | 1975-12-02 | Apparatus for the production of sugars from hemi-cellulose-containing raw materials |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4023982A (enExample) |
| CA (1) | CA1059733A (enExample) |
| CH (1) | CH585794A5 (enExample) |
| DE (1) | DE2458386C3 (enExample) |
| FI (1) | FI58655C (enExample) |
| NL (1) | NL164093C (enExample) |
| SE (1) | SE425406B (enExample) |
Families Citing this family (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH622029A5 (enExample) * | 1976-07-01 | 1981-03-13 | Sulzer Ag | |
| GB1548500A (en) * | 1977-05-17 | 1979-07-18 | Inst Voor Bewaring | Process for obtaining xylose by hydrolysis of residues of annuals |
| US4279663A (en) * | 1979-01-12 | 1981-07-21 | American Can Company | Reactor system and pump apparatus therein |
| US4201596A (en) * | 1979-01-12 | 1980-05-06 | American Can Company | Continuous process for cellulose saccharification |
| US4205673A (en) * | 1979-02-05 | 1980-06-03 | Mine Safety Appliances Company | Breathing apparatus with an automatic firing mechanism |
| US4237226A (en) * | 1979-02-23 | 1980-12-02 | Trustees Of Dartmouth College | Process for pretreating cellulosic substrates and for producing sugar therefrom |
| CA1173380A (en) * | 1980-02-19 | 1984-08-28 | Michael I. Sherman | Acid hydrolysis of biomass for ethanol production |
| ES8201627A1 (es) | 1980-02-23 | 1981-12-16 | Reitter Franz Johann | Procedimiento e instalacion para la hidrolisis continua de hemicelulosas que contienen pentosanas de celulosa. |
| DE3048802A1 (de) * | 1980-12-23 | 1982-07-08 | Werner & Pfleiderer, 7000 Stuttgart | Verfahren zur hydrolyse von zellulose pflanzlicher rohstoffe zu glukose und vorrichtung zur durchfuehrung des verfahrens |
| US4370172A (en) * | 1981-03-17 | 1983-01-25 | Compagnie De Construction Mecanique Sulzer, French Societe Anonyme | Controlled vortex pump feed for supplying cellulose-containing material to reaction vessel |
| US4831127A (en) * | 1983-07-12 | 1989-05-16 | Sbp, Inc. | Parenchymal cell cellulose and related materials |
| NZ209527A (en) * | 1984-09-13 | 1988-10-28 | Jack Tama Haigh Just | Process for the continuous hydrolysis of cellulose-containing material |
| FR2655661B1 (fr) * | 1989-12-07 | 1994-06-03 | Inst Francais Du Petrole | Procede et unite de production en continu d'un melange de sucres contenant au moins 80% de xylose a partir d'un substrat lignocellulosique. |
| FR2656000B1 (fr) * | 1989-12-20 | 1992-04-24 | Inst Francais Du Petrole | Reacteur en continu et sous pression d'impregnation et d'hydrolyse du substrat lignocellulosique, procede et unite de production d'un melange de sucres a base de xylose. |
| US5338366A (en) * | 1993-01-04 | 1994-08-16 | Kamyr, Inc. | Acid pre-hydrolysis reactor system |
| US7812153B2 (en) * | 2004-03-11 | 2010-10-12 | Rayonier Products And Financial Services Company | Process for manufacturing high purity xylose |
| US7815876B2 (en) | 2006-11-03 | 2010-10-19 | Olson David A | Reactor pump for catalyzed hydrolytic splitting of cellulose |
| US7815741B2 (en) | 2006-11-03 | 2010-10-19 | Olson David A | Reactor pump for catalyzed hydrolytic splitting of cellulose |
| JP4427583B2 (ja) | 2008-02-01 | 2010-03-10 | 三菱重工業株式会社 | バイオマスの水熱分解装置及び方法、バイオマス原料を用いた有機原料の製造システム |
| JP4524351B2 (ja) | 2008-02-01 | 2010-08-18 | 三菱重工業株式会社 | バイオマス原料を用いた有機原料の製造システム及び方法 |
| CA2638157C (en) * | 2008-07-24 | 2013-05-28 | Sunopta Bioprocess Inc. | Method and apparatus for conveying a cellulosic feedstock |
| CA2638160C (en) * | 2008-07-24 | 2015-02-17 | Sunopta Bioprocess Inc. | Method and apparatus for conveying a cellulosic feedstock |
| US9127325B2 (en) | 2008-07-24 | 2015-09-08 | Abengoa Bioenergy New Technologies, Llc. | Method and apparatus for treating a cellulosic feedstock |
| US8915644B2 (en) | 2008-07-24 | 2014-12-23 | Abengoa Bioenergy New Technologies, Llc. | Method and apparatus for conveying a cellulosic feedstock |
| CA2638159C (en) * | 2008-07-24 | 2012-09-11 | Sunopta Bioprocess Inc. | Method and apparatus for treating a cellulosic feedstock |
| CA2650913C (en) * | 2009-01-23 | 2013-10-15 | Sunopta Bioprocess Inc. | Method and apparatus for conveying a cellulosic feedstock |
| CA2650919C (en) * | 2009-01-23 | 2014-04-22 | Sunopta Bioprocess Inc. | Method and apparatus for conveying a cellulosic feedstock |
| CA2638150C (en) * | 2008-07-24 | 2012-03-27 | Sunopta Bioprocess Inc. | Method and apparatus for conveying a cellulosic feedstock |
| PL2467532T3 (pl) | 2009-08-24 | 2014-11-28 | Abengoa Bioenergy New Tech Llc | Sposób wytwarzania etanolu i współproduktów z biomasy celulozowej |
| BRPI1006899B1 (pt) | 2010-03-10 | 2021-11-09 | Mitsubishi Power Environmental Solutions, Ltd | Aparelho de decomposição hidrotérmica de biomassa e sistema de produção de matériaprima orgânica que usa material de biomassa |
| JP5854586B2 (ja) | 2010-07-06 | 2016-02-09 | 三菱重工メカトロシステムズ株式会社 | 糖液を用いた発酵システム及び方法 |
| BRPI1009203B1 (pt) | 2010-07-09 | 2020-10-06 | Mitsubishi Hitachi Power Systems Environmental Solutions, Ltd. | Sistema de decomposição hidrotérmica da biomassa e método de produção da solução de sacarídeo empregando material de biomassa |
| WO2012004895A1 (ja) | 2010-07-09 | 2012-01-12 | 三菱重工業株式会社 | バイオマスの処理システム及びバイオマス原料を用いた糖液生産方法 |
| BRPI1005516B1 (pt) | 2010-09-03 | 2019-12-03 | Mitsubishi Heavy Ind Ltd | aparelho de decomposição de biomassa |
| AU2011355013B2 (en) | 2011-01-13 | 2014-03-27 | Mitsubishi Power Environmental Solutions, Ltd. | Device for producing sugar solution, fermentation system, method for producing sugar solution and fermentation method |
| WO2013145236A1 (ja) * | 2012-03-29 | 2013-10-03 | 三菱重工メカトロシステムズ株式会社 | バイオマスの処理システム、バイオマス原料を用いた糖液生産方法、アルコール製造方法 |
| JP5999759B2 (ja) * | 2012-06-21 | 2016-09-28 | 月島機械株式会社 | バイオマスの処理方法 |
| SE538725C2 (sv) * | 2014-06-26 | 2016-11-01 | Valmet Oy | Ångavskiljningsenhet och system för hydrolysförfarande innefattande en ångavskiljningsenhet |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2508884A (en) * | 1945-07-26 | 1950-05-23 | Herong Andre | Hydrolysis tower |
| US2739086A (en) * | 1952-06-14 | 1956-03-20 | Tennessee Coal & Iron Division | Method and apparatus for hydrolyzing cellulosic materials |
| US2801939A (en) * | 1955-04-04 | 1957-08-06 | Tennessee Valley Authority | Hydrolysis of hemicellulose and alphacellulose to produce sugar |
| US3251716A (en) * | 1964-05-28 | 1966-05-17 | Allied Chem | Hydrolysis of lignocellulose materials with concentrated hydrochloric acid |
| US3479248A (en) * | 1965-07-30 | 1969-11-18 | Ledoga Spa | Process for solubilizing the hemicellulose of vegetable materials and for recovering the sugars from the solubilized hemicellulose |
| DE1567335C3 (de) * | 1967-10-17 | 1979-03-29 | Rudolf Dipl.-Ing. 8000 Muenchen Eickemeyer | Verfahren und Vorrichtung zum chemischen Aufschluß cellulosehaltigen Materials |
| US3523911A (en) * | 1969-02-26 | 1970-08-11 | Harald F Funk | Method of separating components of cellulosic material |
-
1974
- 1974-12-03 CH CH1599974A patent/CH585794A5/xx not_active IP Right Cessation
- 1974-12-10 DE DE2458386A patent/DE2458386C3/de not_active Expired
-
1975
- 1975-01-30 NL NL7501121.A patent/NL164093C/xx not_active IP Right Cessation
- 1975-11-20 FI FI753276A patent/FI58655C/fi not_active IP Right Cessation
- 1975-11-28 SE SE7513441A patent/SE425406B/xx not_active IP Right Cessation
- 1975-12-01 US US05/636,743 patent/US4023982A/en not_active Expired - Lifetime
- 1975-12-02 CA CA240,898A patent/CA1059733A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| SE7513441L (sv) | 1976-06-04 |
| SE425406B (sv) | 1982-09-27 |
| FI753276A7 (enExample) | 1976-06-04 |
| CH585794A5 (enExample) | 1977-03-15 |
| DE2458386A1 (de) | 1976-06-10 |
| DE2458386B2 (de) | 1978-12-21 |
| FI58655B (fi) | 1980-11-28 |
| NL164093C (nl) | 1980-11-17 |
| NL7501121A (nl) | 1976-06-08 |
| NL164093B (nl) | 1980-06-16 |
| FI58655C (fi) | 1981-03-10 |
| DE2458386C3 (de) | 1979-09-06 |
| US4023982A (en) | 1977-05-17 |
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