CA1038769A - Extraction - Google Patents
ExtractionInfo
- Publication number
- CA1038769A CA1038769A CA176,848A CA176848A CA1038769A CA 1038769 A CA1038769 A CA 1038769A CA 176848 A CA176848 A CA 176848A CA 1038769 A CA1038769 A CA 1038769A
- Authority
- CA
- Canada
- Prior art keywords
- polar
- solvent
- water
- oil
- plant material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000605 extraction Methods 0.000 title description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 38
- 229930195733 hydrocarbon Natural products 0.000 claims abstract description 36
- 150000002430 hydrocarbons Chemical class 0.000 claims abstract description 36
- 239000004215 Carbon black (E152) Substances 0.000 claims abstract description 34
- 239000000463 material Substances 0.000 claims abstract description 28
- 239000000284 extract Substances 0.000 claims abstract description 16
- 239000002904 solvent Substances 0.000 claims abstract description 15
- 238000001704 evaporation Methods 0.000 claims abstract description 13
- 230000008020 evaporation Effects 0.000 claims abstract description 13
- 239000003205 fragrance Substances 0.000 claims abstract description 12
- 239000000796 flavoring agent Substances 0.000 claims abstract description 11
- 235000019634 flavors Nutrition 0.000 claims abstract description 11
- 238000000034 method Methods 0.000 claims description 13
- 230000008569 process Effects 0.000 claims description 11
- 239000000341 volatile oil Substances 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 8
- 239000012454 non-polar solvent Substances 0.000 claims description 6
- 239000003960 organic solvent Substances 0.000 claims description 5
- DDMOUSALMHHKOS-UHFFFAOYSA-N 1,2-dichloro-1,1,2,2-tetrafluoroethane Chemical compound FC(F)(Cl)C(F)(F)Cl DDMOUSALMHHKOS-UHFFFAOYSA-N 0.000 claims description 4
- 229940087091 dichlorotetrafluoroethane Drugs 0.000 claims description 4
- 239000002798 polar solvent Substances 0.000 claims description 3
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- UMNKXPULIDJLSU-UHFFFAOYSA-N dichlorofluoromethane Chemical group FC(Cl)Cl UMNKXPULIDJLSU-UHFFFAOYSA-N 0.000 claims description 2
- 229940099364 dichlorofluoromethane Drugs 0.000 claims description 2
- 239000012260 resinous material Substances 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000003921 oil Substances 0.000 description 28
- 238000009835 boiling Methods 0.000 description 13
- 241000196324 Embryophyta Species 0.000 description 11
- 239000010410 layer Substances 0.000 description 10
- 239000000346 nonvolatile oil Substances 0.000 description 10
- 238000002474 experimental method Methods 0.000 description 9
- 235000002566 Capsicum Nutrition 0.000 description 8
- 239000006002 Pepper Substances 0.000 description 8
- 241000722363 Piper Species 0.000 description 8
- 235000016761 Piper aduncum Nutrition 0.000 description 8
- 235000017804 Piper guineense Nutrition 0.000 description 8
- 235000008184 Piper nigrum Nutrition 0.000 description 8
- 239000012071 phase Substances 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 4
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 4
- 239000003039 volatile agent Substances 0.000 description 4
- 244000269722 Thea sinensis Species 0.000 description 3
- 239000003599 detergent Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 244000223760 Cinnamomum zeylanicum Species 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 235000017803 cinnamon Nutrition 0.000 description 2
- 239000000306 component Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 2
- 235000019341 magnesium sulphate Nutrition 0.000 description 2
- 239000008601 oleoresin Substances 0.000 description 2
- 239000003208 petroleum Substances 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- LVGUZGTVOIAKKC-UHFFFAOYSA-N 1,1,1,2-tetrafluoroethane Chemical compound FCC(F)(F)F LVGUZGTVOIAKKC-UHFFFAOYSA-N 0.000 description 1
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 240000000560 Citrus x paradisi Species 0.000 description 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- XPDWGBQVDMORPB-UHFFFAOYSA-N Fluoroform Chemical compound FC(F)F XPDWGBQVDMORPB-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 244000270834 Myristica fragrans Species 0.000 description 1
- 235000009421 Myristica fragrans Nutrition 0.000 description 1
- 101100313260 Schizosaccharomyces pombe (strain 972 / ATCC 24843) tea3 gene Proteins 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 239000008373 coffee flavor Substances 0.000 description 1
- 230000002301 combined effect Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 125000001145 hydrido group Chemical class *[H] 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 239000001702 nutmeg Substances 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- MXXWOMGUGJBKIW-YPCIICBESA-N piperine Chemical compound C=1C=C2OCOC2=CC=1/C=C/C=C/C(=O)N1CCCCC1 MXXWOMGUGJBKIW-YPCIICBESA-N 0.000 description 1
- 229940075559 piperine Drugs 0.000 description 1
- WVWHRXVVAYXKDE-UHFFFAOYSA-N piperine Natural products O=C(C=CC=Cc1ccc2OCOc2c1)C3CCCCN3 WVWHRXVVAYXKDE-UHFFFAOYSA-N 0.000 description 1
- 235000019100 piperine Nutrition 0.000 description 1
- 239000003495 polar organic solvent Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 235000019633 pungent taste Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002195 soluble material Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/40—Tea flavour; Tea oil; Flavouring of tea or tea extract
- A23F3/42—Isolation or recuperation of tea flavour or tea oil
- A23F3/423—Isolation or recuperation of tea flavour or tea oil by solvent extraction; Tea flavour from tea oil
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/46—Coffee flavour; Coffee oil; Flavouring of coffee or coffee extract
- A23F5/48—Isolation or recuperation of coffee flavour or coffee oil
- A23F5/483—Isolation or recuperation of coffee flavour or coffee oil by solvent extraction of the beans, ground or not
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/11—Natural spices, flavouring agents or condiments; Extracts thereof obtained by solvent extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/12—Natural spices, flavouring agents or condiments; Extracts thereof from fruit, e.g. essential oils
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Extraction Or Liquid Replacement (AREA)
- Fats And Perfumes (AREA)
- Seasonings (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB3379572A GB1419958A (en) | 1972-07-19 | 1972-07-19 | Extraction of flavour and fragrance components from plant material |
Publications (1)
Publication Number | Publication Date |
---|---|
CA1038769A true CA1038769A (en) | 1978-09-19 |
Family
ID=10357534
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA176,848A Expired CA1038769A (en) | 1972-07-19 | 1973-07-19 | Extraction |
Country Status (9)
Country | Link |
---|---|
BE (1) | BE802504A (enrdf_load_stackoverflow) |
BR (1) | BR7305367D0 (enrdf_load_stackoverflow) |
CA (1) | CA1038769A (enrdf_load_stackoverflow) |
DE (1) | DE2336637A1 (enrdf_load_stackoverflow) |
ES (1) | ES417009A1 (enrdf_load_stackoverflow) |
FR (1) | FR2192852B3 (enrdf_load_stackoverflow) |
GB (1) | GB1419958A (enrdf_load_stackoverflow) |
NL (1) | NL7310092A (enrdf_load_stackoverflow) |
ZA (1) | ZA734741B (enrdf_load_stackoverflow) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CH609215A5 (enrdf_load_stackoverflow) | 1976-03-09 | 1979-02-28 | Nestle Sa | |
JPS56144078A (en) * | 1980-04-08 | 1981-11-10 | Lion Corp | Preparation of preservative |
FR2533118A1 (fr) * | 1982-09-20 | 1984-03-23 | Raffinage Cie Francaise | Procede et installation pour l'extraction d'aromes naturels de produits vegetaux et produits ainsi obtenus |
CH672048A5 (enrdf_load_stackoverflow) * | 1987-09-16 | 1989-10-31 | Nestle Sa | |
DK0507064T3 (da) * | 1991-03-30 | 1995-10-02 | Nestle Sa | Fremgangsmåde til opnåelse af en flydende antioxidantekstrakt fra krydderier |
GB9406423D0 (en) | 1994-03-31 | 1994-05-25 | Ici Plc | Solvent extraction process |
GB9707130D0 (en) * | 1997-04-08 | 1997-05-28 | Advanced Phytonics Ltd | Solvent extraction |
US6824789B2 (en) * | 1998-05-20 | 2004-11-30 | Kemin Industries, Inc. | Method of extracting antioxidants from lamiaceae species and the extract products thereof |
GB9927011D0 (en) * | 1999-11-16 | 2000-01-12 | Advanced Phytonics Ltd | Method for the production of particles |
GB0027047D0 (en) | 2000-11-06 | 2000-12-20 | Ici Plc | Process for reducing the concentration of undesired compounds in a composition |
-
1972
- 1972-07-19 GB GB3379572A patent/GB1419958A/en not_active Expired
-
1973
- 1973-07-12 ZA ZA734741A patent/ZA734741B/xx unknown
- 1973-07-17 ES ES417009A patent/ES417009A1/es not_active Expired
- 1973-07-17 BR BR5367/73A patent/BR7305367D0/pt unknown
- 1973-07-18 FR FR7326296A patent/FR2192852B3/fr not_active Expired
- 1973-07-18 BE BE133614A patent/BE802504A/xx unknown
- 1973-07-18 DE DE19732336637 patent/DE2336637A1/de active Pending
- 1973-07-19 NL NL7310092A patent/NL7310092A/xx not_active Application Discontinuation
- 1973-07-19 CA CA176,848A patent/CA1038769A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
ES417009A1 (es) | 1976-03-16 |
DE2336637A1 (de) | 1974-01-31 |
BE802504A (fr) | 1973-11-16 |
GB1419958A (en) | 1975-12-31 |
ZA734741B (en) | 1974-10-30 |
AU5810273A (en) | 1975-01-16 |
BR7305367D0 (pt) | 1974-08-29 |
FR2192852A1 (enrdf_load_stackoverflow) | 1974-02-15 |
NL7310092A (enrdf_load_stackoverflow) | 1974-01-22 |
FR2192852B3 (enrdf_load_stackoverflow) | 1976-07-02 |
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