CA1001655A - Separation of acrylic acid from the reaction gases from propylene or acrolein oxidation - Google Patents

Separation of acrylic acid from the reaction gases from propylene or acrolein oxidation

Info

Publication number
CA1001655A
CA1001655A CA179,316A CA179316A CA1001655A CA 1001655 A CA1001655 A CA 1001655A CA 179316 A CA179316 A CA 179316A CA 1001655 A CA1001655 A CA 1001655A
Authority
CA
Canada
Prior art keywords
propylene
separation
acrylic acid
reaction gases
acrolein oxidation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA179,316A
Other languages
English (en)
Other versions
CA179316S (en
Inventor
Walter Frey
Heinz Engelbach
Gerd Duembgen
Carl-Heinz Willersinn
Fritz Thiessen
Ulrich Lebert
Richard Krabetz
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of CA1001655A publication Critical patent/CA1001655A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1487Removing organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1493Selection of liquid materials for use as absorbents
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00Distillation: processes, separatory
    • Y10S203/22Accessories

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treating Waste Gases (AREA)
CA179,316A 1972-08-24 1973-08-21 Separation of acrylic acid from the reaction gases from propylene or acrolein oxidation Expired CA1001655A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE2241714A DE2241714A1 (de) 1972-08-24 1972-08-24 Verfahren zur abtrennung von acrylsaeure aus den reaktionsgasen der propylenoder acroleinoxydation

Publications (1)

Publication Number Publication Date
CA1001655A true CA1001655A (en) 1976-12-14

Family

ID=5854458

Family Applications (1)

Application Number Title Priority Date Filing Date
CA179,316A Expired CA1001655A (en) 1972-08-24 1973-08-21 Separation of acrylic acid from the reaction gases from propylene or acrolein oxidation

Country Status (10)

Country Link
US (1) US3868417A (US06653308-20031125-C00199.png)
JP (1) JPS5621010B2 (US06653308-20031125-C00199.png)
BE (1) BE803985A (US06653308-20031125-C00199.png)
CA (1) CA1001655A (US06653308-20031125-C00199.png)
CH (1) CH581598A5 (US06653308-20031125-C00199.png)
DE (1) DE2241714A1 (US06653308-20031125-C00199.png)
FR (1) FR2196986B1 (US06653308-20031125-C00199.png)
GB (1) GB1432190A (US06653308-20031125-C00199.png)
IT (1) IT990407B (US06653308-20031125-C00199.png)
NL (1) NL7311516A (US06653308-20031125-C00199.png)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR206439A1 (es) * 1974-10-07 1976-07-23 Celanese Corp Un metodo para la recuperacion de un acido acrilico crudo
DE2449780C3 (de) * 1974-10-19 1987-01-22 Basf Ag, 6700 Ludwigshafen Verfahren zum Abtrennen schwer- oder nichtflüchtiger Nebenprodukte der Propylen- und/oder Acroleinoxidation von den für die Absorbtion der Acrylsäure aus den Reaktionsgasen verwendeten Lösungsmitteln
FR2427117A1 (fr) * 1978-06-01 1979-12-28 Mo I Khim Procede de formation de courants dans les appareils d'echange de masse et de chaleur
US4180681A (en) * 1978-08-17 1979-12-25 Atlantic Richfield Company Preparation and recovery of methacrylic acid from an aqueous sodium methacrylate solution
US4999452A (en) * 1989-05-15 1991-03-12 Union Carbide Chemicals And Plastics Company Inc. Process for producing acrylic ester
JP3289303B2 (ja) * 1992-03-06 2002-06-04 住友化学工業株式会社 アクロレインの製造方法
DE4308087C2 (de) * 1993-03-13 1997-02-06 Basf Ag Verfahren zur Abtrennung von Acrylsäure aus den Reaktionsgasen der katalytischen Oxidation von Propylen und/oder Acrolein
US5728872A (en) * 1994-06-27 1998-03-17 Lutz Riemenschneider Stabilized acrylic acid compositions
DE4436243A1 (de) * 1994-10-11 1996-04-18 Basf Ag Verfahren zur Abtrennung von (Meth)acrylsäure aus dem Reaktionsgasgemisch der katalytischen Gasphasenoxidation C¶3¶-/C¶4¶-Verbindungen
FR2735989B1 (fr) * 1995-06-29 1997-08-14 Rhone Poulenc Nutrition Animal Procede et installation de purification d'un flux gazeux contenant de l'acroleine
FR2736912B1 (fr) * 1995-07-18 1997-08-22 Atochem Elf Sa Procede de purification de l'acide acrylique obtenu par oxydation catalytique du propylene
FR2756280B1 (fr) * 1996-11-25 1998-12-24 Atochem Elf Sa Purification de l'acide acrylique obtenu par oxydation catalytique du propylene
US6180827B1 (en) * 1998-02-03 2001-01-30 Hfm International, Inc. Recovery of acrylic acid from process or waste water streams
JP3948855B2 (ja) * 1999-06-10 2007-07-25 株式会社日本触媒 (メタ)アクリル酸の製造方法
JP4308372B2 (ja) 1999-07-06 2009-08-05 株式会社日本触媒 (メタ)アクリル酸および/または(メタ)アクロレインの吸収方法及びその装置
EG22306A (en) 1999-11-15 2002-12-31 Shell Int Research Expanding a tubular element in a wellbore
US6888025B2 (en) * 2000-02-14 2005-05-03 Nippon Shokubai, Co. Ltd. Method for absorbing acrylic acid and method for purifying acrylic acid
JP2001226320A (ja) * 2000-02-14 2001-08-21 Nippon Shokubai Co Ltd アクリル酸の捕集方法およびアクリル酸の精製方法
DE10138150A1 (de) * 2001-08-03 2003-02-13 Basf Ag Verfahren zur Herstellung wasserabsorbierender Harze
FR2861724B1 (fr) 2003-11-04 2005-12-30 Arkema Procede de purification de l'acide (meth)acrylique obtenu par oxydation d'un substrat gazeux
US9156769B2 (en) 2008-10-15 2015-10-13 Arkema Inc. Method of recovering carboxylic acids from dilute aqueous streams
WO2010044990A1 (en) * 2008-10-15 2010-04-22 Arkema Inc. Method of recovering carboxylic acids from dilute aqueous streams

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1359885A (fr) * 1963-03-21 1964-04-30 Electrochimie Soc Procédé de fabrication d'acide acrylique glacial
GB995472A (en) * 1963-05-16 1965-06-16 Distillers Co Yeast Ltd Improvements in or relating to acrylic acid production
GB997325A (en) * 1963-06-20 1965-07-07 Distillers Co Yeast Ltd Recovery of acrylic acid
US3555082A (en) * 1966-12-15 1971-01-12 Knapsack Ag Process for isolating acrylic acid from the reaction gases obtained by oxidation of propylene or acrolein
DE1618612B2 (de) * 1967-06-29 1973-03-15 Knapsack AG, 5033 Hurth Knapsack Verfahren zur gewinnung reiner acrylsaeure aus waessriger rohsaeure
US3666632A (en) * 1968-10-08 1972-05-30 Asahi Chemical Ind Method for the separation of acrylic acid from aqueous solution containing acrylic acid and acetic acid
US3527677A (en) * 1969-03-06 1970-09-08 Goodrich Co B F Process for dehydration of aqueous acrylic acid solutions by extractive - azeotropic distillation with 2-ethylhexanol or 2-ethylhexylacrylate
JPS4924898B1 (US06653308-20031125-C00199.png) * 1970-12-26 1974-06-26
BE786398A (fr) * 1971-07-21 1973-01-18 Basf Ag Procede de preparation de l'acide acrylique anhydre

Also Published As

Publication number Publication date
BE803985A (fr) 1974-02-25
CH581598A5 (US06653308-20031125-C00199.png) 1976-11-15
FR2196986A1 (US06653308-20031125-C00199.png) 1974-03-22
GB1432190A (en) 1976-04-14
FR2196986B1 (US06653308-20031125-C00199.png) 1977-02-25
US3868417A (en) 1975-02-25
JPS4956915A (US06653308-20031125-C00199.png) 1974-06-03
IT990407B (it) 1975-06-20
JPS5621010B2 (US06653308-20031125-C00199.png) 1981-05-16
DE2241714A1 (de) 1974-03-28
DE2241714B2 (US06653308-20031125-C00199.png) 1974-09-19
NL7311516A (US06653308-20031125-C00199.png) 1974-02-26

Similar Documents

Publication Publication Date Title
CA1001655A (en) Separation of acrylic acid from the reaction gases from propylene or acrolein oxidation
CA962584A (en) Reaction crystallizer
CA954533A (en) Oxidation processes
CA954880A (en) Catalytic process for the preparation of methacrolein
CA1003436A (en) Process for the production of acrolein and acrylic acid
AU474292B2 (en) Process for the catalytic oxidation of lupulones into hulupones
AU3545871A (en) Oxidation of olefinic compounds
CA1006545A (en) Separation of sulphitation reaction products
CA1024162A (en) Catalyst for the production of acrylonitrile, acrylic acid and acrolein
CA790626A (en) Process for isolating acrylic acid from the reaction gases obtained by oxidation of propylene or acrolein
CA778416A (en) Process for isolating acrylic acid from the reaction gases obtained by the oxidation of propylene or acrolein
CA982150A (en) Catalysts for the oxidation of olefines
CA859126A (en) Catalyst for the catalytic gas phase-oxidation of propylene or acrolein into acrylic acid
CA988244A (en) Catalysis of the oxirane-anhydride reaction
CA849568A (en) Process for the manufacture of acrylic acid from propylene
CA854237A (en) Process for avoiding secondary reactions in the catalytic oxidation of propylene or acrolein
CA871146A (en) Process for the recovery of an oxidation catalyst
CA884862A (en) Phthalocyanine-catalyzed oxidation of mercapto compounds
CA885486A (en) Process for the oxidation of isobutane
CA901826A (en) Oxidation process employing nitric acid catalysis for the preparation of humates from coal
CA868940A (en) Production of acrylic acid by oxidation of acrolein
CA954137A (en) Process for the total synthesis of elenolic acid, analogs thereof and intermediates
CA773143A (en) Method of processing the reaction mixture from the oxidation of cyclohexane
AU481488B2 (en) Promoted scrubbing of acid gases
CA872831A (en) Carboxylic acid function promotion of the oxidation of mononuclear aromatic compounds