BR112014031838A2 - reator e processo para preparar sulfureto de hidrogênio - Google Patents

reator e processo para preparar sulfureto de hidrogênio

Info

Publication number
BR112014031838A2
BR112014031838A2 BR112014031838A BR112014031838A BR112014031838A2 BR 112014031838 A2 BR112014031838 A2 BR 112014031838A2 BR 112014031838 A BR112014031838 A BR 112014031838A BR 112014031838 A BR112014031838 A BR 112014031838A BR 112014031838 A2 BR112014031838 A2 BR 112014031838A2
Authority
BR
Brazil
Prior art keywords
reactor
hydrogen sulfide
preparing hydrogen
preparing
hydrogen
Prior art date
Application number
BR112014031838A
Other languages
English (en)
Inventor
Finkeldei Caspar-Heinrich
Kee Cheung Chiu
Van Eester Geert
Körfer Martin
Maassen Ralf
Wenner Stefan
Original Assignee
Evonik Industries Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Industries Ag filed Critical Evonik Industries Ag
Publication of BR112014031838A2 publication Critical patent/BR112014031838A2/pt

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/005Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out at high temperatures in the presence of a molten material
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/16Hydrogen sulfides
    • C01B17/161Preparation from elemental sulfur
    • C01B17/162Preparation from elemental sulfur from elemental sulfur and hydrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/2415Tubular reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/002Nozzle-type elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J7/00Apparatus for generating gases
    • B01J7/02Apparatus for generating gases by wet methods
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067Heating or cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/20Methods for preparing sulfides or polysulfides, in general
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00164Controlling or regulating processes controlling the flow
    • B01J2219/00166Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00777Baffles attached to the reactor wall horizontal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24Stationary reactors without moving elements inside

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Catalysts (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Epoxy Compounds (AREA)

Abstract

resumo patente de invenção: "reator e processo para preparar sulfureto de hidrogênio". a presente invenção refere-se a um reator e a um processo para síntese de sulfureto de hidrogênio a partir de hidrogênio e enxofre elementar em pressão elevada e temperatura elevada. a invenção refere-se adicionalmente ao uso do reator para a preparação de sulfureto de hidrogênio em alto rendimento e com um baixo teor de h2sx. 23392567v1 1/1 23392567v1
BR112014031838A 2012-06-22 2013-05-31 reator e processo para preparar sulfureto de hidrogênio BR112014031838A2 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12173241.6A EP2676927A1 (de) 2012-06-22 2012-06-22 Reaktor und Verfahren zur Herstellung von Schwefelwasserstoff
PCT/EP2013/061237 WO2013189718A1 (en) 2012-06-22 2013-05-31 Reactor and process for preparing hydrogen sulphide

Publications (1)

Publication Number Publication Date
BR112014031838A2 true BR112014031838A2 (pt) 2017-06-27

Family

ID=48576416

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112014031838A BR112014031838A2 (pt) 2012-06-22 2013-05-31 reator e processo para preparar sulfureto de hidrogênio

Country Status (12)

Country Link
US (1) US9630843B2 (pt)
EP (2) EP2676927A1 (pt)
JP (1) JP6173447B2 (pt)
KR (1) KR102022146B1 (pt)
CN (1) CN104583115B (pt)
BR (1) BR112014031838A2 (pt)
ES (1) ES2627809T3 (pt)
MX (1) MX345004B (pt)
MY (1) MY166861A (pt)
RU (1) RU2621755C2 (pt)
SG (1) SG11201408548SA (pt)
WO (1) WO2013189718A1 (pt)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2676926A1 (de) * 2012-06-22 2013-12-25 Evonik Industries AG Reaktor und Verfahren zur Herstellung von Schwefelwasserstoff
MY189842A (en) 2016-05-31 2022-03-11 Novus Int Inc Process for producing methyl mercaptan from dimethyl sulfide
EP3482824A1 (de) * 2017-11-14 2019-05-15 Umicore Ag & Co. Kg Scr-katalysator

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2965455A (en) * 1953-04-24 1960-12-20 Hooker Chemical Corp Apparatus for producing hydrogen sulfide
US2863725A (en) 1953-04-24 1958-12-09 Hooker Chemical Corp Process for making sulfur free hydrogen sulfide
US2876070A (en) 1955-03-28 1959-03-03 Chemetron Corp Method for producing hydrogen sulfide by synthesis
US2876071A (en) * 1955-05-31 1959-03-03 Chemetron Corp Method for producing hydrogen sulfide by synthesis
US3087788A (en) * 1959-04-06 1963-04-30 Fmc Corp Combined catalytic and non-catalytic process of producing hydrogen sulfide and carbon disulfide
FR1593276A (pt) * 1967-12-19 1970-05-25
SU649648A1 (ru) * 1975-07-28 1979-02-28 Н. Г. Вилесов, В. И. Калько, Б. Я. Скрипко, А. Д. Биба, В. Е. Ткаченко и В. Г. Болыиунов Способ получени сероводорода
SU833479A1 (ru) * 1979-10-29 1981-05-30 Институт Газа Академии Наук Усср Способ получени восстановительногогАзА, СОдЕРжАщЕгО СЕРОВОдОРОд и ОКиСьуглЕРОдА
JPS62162606A (ja) * 1986-01-10 1987-07-18 Tsukishima Kikai Co Ltd アルカリ硫黄化合物の熱分解処理方法
DE10245164B4 (de) 2002-09-26 2014-11-13 Evonik Degussa Gmbh Verfahren zur Umwandlung von Polysulfanen
FR2885138B1 (fr) * 2005-04-29 2007-06-15 Inst Rech Pour Le Dev I R D Et Procede de production d'acide sulfhydrique et son application, notamment a la depollution d'effluents contenant des metaux lourds
DE102006019590A1 (de) * 2006-04-27 2007-10-31 Degussa Gmbh Reaktionsbehälter für die Herstellung von Schwefelwasserstoff
CA2674734C (en) * 2007-01-16 2015-10-27 Basf Se Process and apparatus for continuously preparing hydrogen sulfide
JP5306231B2 (ja) 2007-01-16 2013-10-02 ビーエーエスエフ ソシエタス・ヨーロピア 硫化水素を製造するための反応器および方法
JP5306232B2 (ja) * 2007-01-16 2013-10-02 ビーエーエスエフ ソシエタス・ヨーロピア 硫化水素を連続的に製造するための方法および装置
DE102008040544A1 (de) * 2008-07-18 2010-01-21 Evonik Degussa Gmbh Reaktionsbehälter und Verfahren zur Verwendung
EP2676928A1 (de) * 2012-06-22 2013-12-25 Evonik Industries AG Reaktor und Verfahren zur Herstellung von Schwefelwasserstoff

Also Published As

Publication number Publication date
EP2864246B1 (en) 2017-03-15
US9630843B2 (en) 2017-04-25
KR20150036119A (ko) 2015-04-07
MX345004B (es) 2017-01-13
EP2676927A1 (de) 2013-12-25
RU2015101753A (ru) 2016-08-10
JP6173447B2 (ja) 2017-08-02
US20150175419A1 (en) 2015-06-25
CN104583115B (zh) 2017-12-12
WO2013189718A1 (en) 2013-12-27
RU2621755C2 (ru) 2017-06-07
ES2627809T3 (es) 2017-07-31
SG11201408548SA (en) 2015-01-29
MX2014015493A (es) 2015-04-08
KR102022146B1 (ko) 2019-09-17
CN104583115A (zh) 2015-04-29
MY166861A (en) 2018-07-24
EP2864246A1 (en) 2015-04-29
JP2015523956A (ja) 2015-08-20

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Legal Events

Date Code Title Description
B25A Requested transfer of rights approved

Owner name: EVONIK DEGUSSA GMBH (DE)

B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B06I Publication of requirement cancelled [chapter 6.9 patent gazette]

Free format text: ANULADA A PUBLICACAO CODIGO 6.6.1 NA RPI NO 2462 DE 13/03/2018 POR TER SIDO INDEVIDA.

B06U Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B11D Dismissal acc. art. 38, par 2 of ipl - failure to pay fee after grant in time