BR112014019850B1 - solução oxidante - Google Patents
solução oxidante Download PDFInfo
- Publication number
- BR112014019850B1 BR112014019850B1 BR112014019850-0A BR112014019850A BR112014019850B1 BR 112014019850 B1 BR112014019850 B1 BR 112014019850B1 BR 112014019850 A BR112014019850 A BR 112014019850A BR 112014019850 B1 BR112014019850 B1 BR 112014019850B1
- Authority
- BR
- Brazil
- Prior art keywords
- nitrate
- solution
- calcium
- oxidizing solution
- aqueous oxidizing
- Prior art date
Links
- 230000001590 oxidative effect Effects 0.000 title claims abstract description 37
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 claims abstract description 98
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 38
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 claims abstract description 37
- 239000002360 explosive Substances 0.000 claims abstract description 36
- 239000000203 mixture Substances 0.000 claims abstract description 28
- 238000002425 crystallisation Methods 0.000 claims abstract description 24
- 230000008025 crystallization Effects 0.000 claims abstract description 24
- 238000004519 manufacturing process Methods 0.000 claims abstract description 10
- 238000009472 formulation Methods 0.000 claims abstract description 8
- 238000002360 preparation method Methods 0.000 claims abstract description 3
- 239000000243 solution Substances 0.000 claims description 69
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical compound [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 claims description 48
- 229910002651 NO3 Inorganic materials 0.000 claims description 16
- -1 alkylamine nitrate Chemical class 0.000 claims description 13
- 239000000446 fuel Substances 0.000 claims description 13
- WAFNMNCIAQAQJU-UHFFFAOYSA-N 2-aminoethanol;nitric acid Chemical compound NCCO.O[N+]([O-])=O WAFNMNCIAQAQJU-UHFFFAOYSA-N 0.000 claims description 10
- PTIUDKQYXMFYAI-UHFFFAOYSA-N methylammonium nitrate Chemical group NC.O[N+]([O-])=O PTIUDKQYXMFYAI-UHFFFAOYSA-N 0.000 claims description 5
- 150000002823 nitrates Chemical class 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 2
- GWKNUWRKJUDXAY-UHFFFAOYSA-N n,n-dimethylmethanamine;nitric acid Chemical compound CN(C)C.O[N+]([O-])=O GWKNUWRKJUDXAY-UHFFFAOYSA-N 0.000 claims description 2
- KTAFYYQZWVSKCK-UHFFFAOYSA-N n-methylmethanamine;nitric acid Chemical compound CNC.O[N+]([O-])=O KTAFYYQZWVSKCK-UHFFFAOYSA-N 0.000 claims description 2
- 230000003647 oxidation Effects 0.000 claims description 2
- 238000007254 oxidation reaction Methods 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims 1
- 239000000839 emulsion Substances 0.000 abstract description 32
- WPHINMYYTFDPIA-UHFFFAOYSA-O methylazanium;nitrate Chemical compound [NH3+]C.[O-][N+]([O-])=O WPHINMYYTFDPIA-UHFFFAOYSA-O 0.000 abstract description 18
- 150000003839 salts Chemical class 0.000 abstract description 10
- 239000000017 hydrogel Substances 0.000 abstract description 9
- 239000007800 oxidant agent Substances 0.000 abstract description 7
- 239000000725 suspension Substances 0.000 abstract description 5
- 239000000499 gel Substances 0.000 abstract description 4
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 20
- 238000005086 pumping Methods 0.000 description 10
- 235000010344 sodium nitrate Nutrition 0.000 description 10
- 239000004317 sodium nitrate Substances 0.000 description 10
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 8
- 239000011575 calcium Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 239000003995 emulsifying agent Substances 0.000 description 5
- 235000019198 oils Nutrition 0.000 description 5
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 235000010333 potassium nitrate Nutrition 0.000 description 4
- 239000004323 potassium nitrate Substances 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000693 micelle Substances 0.000 description 3
- 238000005065 mining Methods 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 210000002421 cell wall Anatomy 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- HZTVIZREFBBQMG-UHFFFAOYSA-N 2-methyl-1,3,5-trinitrobenzene;[3-nitrooxy-2,2-bis(nitrooxymethyl)propyl] nitrate Chemical compound CC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O.[O-][N+](=O)OCC(CO[N+]([O-])=O)(CO[N+]([O-])=O)CO[N+]([O-])=O HZTVIZREFBBQMG-UHFFFAOYSA-N 0.000 description 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000012773 agricultural material Substances 0.000 description 1
- DVARTQFDIMZBAA-UHFFFAOYSA-O ammonium nitrate Chemical compound [NH4+].[O-][N+]([O-])=O DVARTQFDIMZBAA-UHFFFAOYSA-O 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 230000009172 bursting Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 230000000994 depressogenic effect Effects 0.000 description 1
- 238000005474 detonation Methods 0.000 description 1
- 239000002283 diesel fuel Substances 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000008041 oiling agent Substances 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000012047 saturated solution Substances 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B31/00—Compositions containing an inorganic nitrogen-oxygen salt
- C06B31/28—Compositions containing an inorganic nitrogen-oxygen salt the salt being ammonium nitrate
- C06B31/32—Compositions containing an inorganic nitrogen-oxygen salt the salt being ammonium nitrate with a nitrated organic compound
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B25/00—Compositions containing a nitrated organic compound
- C06B25/36—Compositions containing a nitrated organic compound the compound being a nitroparaffin
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B31/00—Compositions containing an inorganic nitrogen-oxygen salt
- C06B31/02—Compositions containing an inorganic nitrogen-oxygen salt the salt being an alkali metal or an alkaline earth metal nitrate
- C06B31/12—Compositions containing an inorganic nitrogen-oxygen salt the salt being an alkali metal or an alkaline earth metal nitrate with a nitrated organic compound
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B47/00—Compositions in which the components are separately stored until the moment of burning or explosion, e.g. "Sprengel"-type explosives; Suspensions of solid component in a normally non-explosive liquid phase, including a thickened aqueous phase
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Colloid Chemistry (AREA)
- Catalysts (AREA)
- Gas Separation By Absorption (AREA)
- Treatment Of Water By Oxidation Or Reduction (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1202402.2 | 2012-02-10 | ||
| GBGB1202402.2A GB201202402D0 (en) | 2012-02-10 | 2012-02-10 | Oxidizer solution |
| PCT/IB2013/051107 WO2013118103A2 (en) | 2012-02-10 | 2013-02-11 | Oxidizer solution |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| BR112014019850A2 BR112014019850A2 (enrdf_load_stackoverflow) | 2017-06-20 |
| BR112014019850A8 BR112014019850A8 (pt) | 2017-07-11 |
| BR112014019850B1 true BR112014019850B1 (pt) | 2021-03-09 |
Family
ID=45929995
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112014019850-0A BR112014019850B1 (pt) | 2012-02-10 | 2013-02-11 | solução oxidante |
Country Status (12)
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2698834C1 (ru) * | 2017-05-05 | 2019-08-30 | Рашид Ильдарович Азаматов | Промышленное взрывчатое вещество |
| CN113185372A (zh) * | 2021-04-12 | 2021-07-30 | 浙江永联民爆器材有限公司 | 乳化炸药水相溶液的制备方法 |
| CN117069549B (zh) * | 2023-07-06 | 2025-04-08 | 南京理工大学 | 一种降低硝酸铵饱和溶液析晶点的添加剂及其使用方法 |
| CN117923994A (zh) * | 2024-01-15 | 2024-04-26 | 抚顺隆烨化工南杂木有限公司 | 一种用于降低煤矿水相析晶点的工艺方法 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1195213B (de) * | 1963-06-12 | 1965-06-16 | Dynamit Nobel Ag | Zuendladung fuer zuendunwillige Sprengstoffe |
| US3586553A (en) * | 1969-04-11 | 1971-06-22 | Du Pont | Water-bearing explosive containing proten and nitrogen-base salt |
| US3645809A (en) * | 1969-12-09 | 1972-02-29 | Hercules Inc | Aqueous slurry explosives having improved oxidizer-fuel system and method of making |
| US3713917A (en) * | 1970-11-16 | 1973-01-30 | Ireco Chemicals | Blasting slurry compositions contain-ing calcium nitrate and method of preparation |
| US3996078A (en) * | 1971-05-29 | 1976-12-07 | Dynamit Nobel Aktiengesellschaft | Explosive composition and eutectic mixture therefor |
| US4294633A (en) * | 1979-06-07 | 1981-10-13 | Clay Robert B | Blasting composition |
| US4364782A (en) * | 1980-09-12 | 1982-12-21 | Ireco Chemicals | Permissible slurry explosive |
| US4356044A (en) * | 1981-03-23 | 1982-10-26 | Ireco Chemicals | Emulsion explosives containing high concentrations of calcium nitrate |
| US4718954A (en) * | 1986-03-26 | 1988-01-12 | Thermex Energy Corporation | Explosive compositions |
| AU2002346744A1 (en) * | 2001-11-15 | 2003-05-26 | Sasol Chemical Industries Limited | Manomethylamine nitrate gel containing explosive composition |
| ES2226529B1 (es) * | 2002-06-26 | 2006-06-01 | Union Española De Explosivos, S.A. | Procedimiento para la fabricacion "in situ" de mezclas explosivas. |
| US20120180915A1 (en) * | 2007-06-28 | 2012-07-19 | Maxam North America | Explosive emulsion compositions and methods of making the same |
-
2012
- 2012-02-10 GB GBGB1202402.2A patent/GB201202402D0/en not_active Ceased
-
2013
- 2013-02-11 EP EP13714699.9A patent/EP2812295B1/en not_active Not-in-force
- 2013-02-11 BR BR112014019850-0A patent/BR112014019850B1/pt not_active IP Right Cessation
- 2013-02-11 AP AP2014007908A patent/AP3822A/en active
- 2013-02-11 EA EA201400885A patent/EA027414B1/ru unknown
- 2013-02-11 WO PCT/IB2013/051107 patent/WO2013118103A2/en active Application Filing
- 2013-02-11 AU AU2013217230A patent/AU2013217230B2/en not_active Ceased
- 2013-02-11 CA CA2864216A patent/CA2864216C/en not_active Expired - Fee Related
- 2013-02-11 US US14/377,542 patent/US20150000804A1/en not_active Abandoned
- 2013-02-11 PL PL13714699T patent/PL2812295T3/pl unknown
-
2014
- 2014-08-08 CL CL2014002115A patent/CL2014002115A1/es unknown
- 2014-09-02 ZA ZA2014/06433A patent/ZA201406433B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| PL2812295T3 (pl) | 2017-01-31 |
| ZA201406433B (en) | 2016-05-25 |
| AU2013217230A1 (en) | 2014-09-18 |
| EP2812295B1 (en) | 2016-06-22 |
| CA2864216A1 (en) | 2013-08-15 |
| BR112014019850A2 (enrdf_load_stackoverflow) | 2017-06-20 |
| US20150000804A1 (en) | 2015-01-01 |
| EP2812295A2 (en) | 2014-12-17 |
| CA2864216C (en) | 2020-06-02 |
| EA201400885A1 (ru) | 2015-05-29 |
| WO2013118103A3 (en) | 2013-11-07 |
| AU2013217230B2 (en) | 2017-05-04 |
| WO2013118103A2 (en) | 2013-08-15 |
| BR112014019850A8 (pt) | 2017-07-11 |
| AP3822A (en) | 2015-09-30 |
| AP2014007908A0 (en) | 2014-08-31 |
| EA027414B1 (ru) | 2017-07-31 |
| CL2014002115A1 (es) | 2015-03-06 |
| GB201202402D0 (en) | 2012-03-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B06F | Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette] | ||
| B06U | Preliminary requirement: requests with searches performed by other patent offices: procedure suspended [chapter 6.21 patent gazette] | ||
| B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 11/02/2013, OBSERVADAS AS CONDICOES LEGAIS. |
|
| B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE A 10A ANUIDADE. |
|
| B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2709 DE 06-12-2022 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |