BR112012019239A2 - processo de extração - Google Patents
processo de extraçãoInfo
- Publication number
- BR112012019239A2 BR112012019239A2 BR112012019239A BR112012019239A BR112012019239A2 BR 112012019239 A2 BR112012019239 A2 BR 112012019239A2 BR 112012019239 A BR112012019239 A BR 112012019239A BR 112012019239 A BR112012019239 A BR 112012019239A BR 112012019239 A2 BR112012019239 A2 BR 112012019239A2
- Authority
- BR
- Brazil
- Prior art keywords
- extraction
- solution
- uranium
- iron
- extraction solution
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G43/00—Compounds of uranium
- C01G43/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/38—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds containing phosphorus
- C22B3/381—Phosphines, e.g. compounds with the formula PRnH3-n, with n = 0-3
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/40—Mixtures
- C22B3/408—Mixtures using a mixture of phosphorus-based acid derivatives of different types
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B60/00—Obtaining metals of atomic number 87 or higher, i.e. radioactive metals
- C22B60/02—Obtaining thorium, uranium, or other actinides
- C22B60/0204—Obtaining thorium, uranium, or other actinides obtaining uranium
- C22B60/0217—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes
- C22B60/0252—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries
- C22B60/026—Obtaining thorium, uranium, or other actinides obtaining uranium by wet processes treatment or purification of solutions or of liquors or of slurries liquid-liquid extraction with or without dissolution in organic solvents
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Geology (AREA)
- Metallurgy (AREA)
- Environmental & Geological Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Inorganic Chemistry (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Extraction Or Liquid Replacement (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
processo de extração. a presente invenção está correlacionada a um método para recuperação seletiva de urânio de uma solução de urânio aquosa acídica à base de sulfato, contendo ferro e outros metais, por meio de extração por solvente, em que o agente de extração usado na solução orgânica de extração é bis(2-etil-hrxil) fosfato e um óxido de trialquilfosfina ramificado líquido é o agente modificador. é típico do método que a concentração de urânio na solução de alimentação seja inferior a 50 mg/l e um agente redutor é introduzido dentro da solução aquosa e/ou de extração, para prevenir a oxidação permanente do ferro em ferro trivalente. no presente método, a maior parte da solução de extração é circulada em um circuito que consiste do estágio de estração e de um tanque de armazenamento e apenas uma pequena parte da solução de extração contendo urãnio é enviada para purificação e separação.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI20100033A FI122274B (fi) | 2010-02-02 | 2010-02-02 | Uuttoprosessi |
| FI20100033 | 2010-02-02 | ||
| PCT/FI2011/050060 WO2011095679A1 (en) | 2010-02-02 | 2011-01-27 | Extraction process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| BR112012019239A2 true BR112012019239A2 (pt) | 2017-06-13 |
| BR112012019239B1 BR112012019239B1 (pt) | 2018-02-14 |
Family
ID=41727581
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112012019239-6A BR112012019239B1 (pt) | 2010-02-02 | 2011-01-27 | Método para recuperação seletiva de Urânio |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US8926924B2 (pt) |
| EP (1) | EP2531626B1 (pt) |
| CN (1) | CN102741433B (pt) |
| AU (1) | AU2011212310B2 (pt) |
| BR (1) | BR112012019239B1 (pt) |
| CA (1) | CA2787572C (pt) |
| CL (1) | CL2012002137A1 (pt) |
| EA (1) | EA021530B1 (pt) |
| ES (1) | ES2621463T3 (pt) |
| FI (1) | FI122274B (pt) |
| MX (1) | MX2012008885A (pt) |
| PE (1) | PE20130468A1 (pt) |
| WO (1) | WO2011095679A1 (pt) |
| ZA (1) | ZA201205548B (pt) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EA024748B1 (ru) * | 2012-09-13 | 2016-10-31 | БиЭйчПи БИЛЛИТОН ОЛИМПИК ДЭМ КОРПОРЕЙШН РТИ ЛТД. | Способ экстракции урана |
| US9567237B2 (en) | 2012-11-16 | 2017-02-14 | Honeywell International Inc. | Separation and recovery of molybdenum values from uranium process distillate |
| CN103146938B (zh) * | 2013-03-28 | 2015-02-04 | 中国科学院长春应用化学研究所 | 一种铀的萃取分离方法 |
| CN103397184B (zh) * | 2013-07-31 | 2014-12-03 | 南昌航空大学 | 一种反萃取分离叔胺有机相中铀和铁的方法 |
| CN106834686B (zh) * | 2015-12-04 | 2018-07-27 | 核工业北京地质研究院 | 一种镓生产流程中的除铀工艺 |
| CN111549242A (zh) * | 2020-04-24 | 2020-08-18 | 核工业北京化工冶金研究院 | 一种碱渣浸出液的铀纯化方法 |
| CN111646503B (zh) * | 2020-07-09 | 2022-05-17 | 雅安市鑫辉矿业有限公司 | 一种钛产品制备工艺 |
| CN115948665A (zh) * | 2021-10-08 | 2023-04-11 | 中核矿业科技集团有限公司 | 一种高稳定性的铀纯化萃取方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2859094A (en) * | 1957-02-07 | 1958-11-04 | John M Schmitt | Uranium extraction process using synergistic reagents |
| US3214239A (en) | 1962-07-02 | 1965-10-26 | Kerr Mc Gee Oil Ind Inc | Recovery of metal values from aqueous solution by solvent extraction with an organo phosphorus extractant |
| US4002716A (en) | 1973-08-23 | 1977-01-11 | Westinghouse Electric Corporation | Sulfide precipitation method of separating uranium from group II and group III metal ions |
| CA1157278A (en) * | 1981-06-11 | 1983-11-22 | William A. Rickelton | Solvent extraction process for the recovery of uranium |
| US4432945A (en) | 1981-11-04 | 1984-02-21 | The United States Of America As Represented By The Department Of Energy | Removing oxygen from a solvent extractant in an uranium recovery process |
| US4816241A (en) | 1982-02-16 | 1989-03-28 | J. R. Simplot Co. | Gaseous reduction of phosphoric acid |
| US7192563B2 (en) * | 2003-03-31 | 2007-03-20 | Secretary, Department Of Atomic Energy, Government Of India | Process for recovery of high purity uranium from fertilizer grade weak phosphoric acid |
-
2010
- 2010-02-02 FI FI20100033A patent/FI122274B/fi not_active IP Right Cessation
-
2011
- 2011-01-27 EP EP11739438.7A patent/EP2531626B1/en active Active
- 2011-01-27 PE PE2012001100A patent/PE20130468A1/es active IP Right Grant
- 2011-01-27 MX MX2012008885A patent/MX2012008885A/es active IP Right Grant
- 2011-01-27 ES ES11739438.7T patent/ES2621463T3/es active Active
- 2011-01-27 EA EA201290647A patent/EA021530B1/ru not_active IP Right Cessation
- 2011-01-27 BR BR112012019239-6A patent/BR112012019239B1/pt not_active IP Right Cessation
- 2011-01-27 WO PCT/FI2011/050060 patent/WO2011095679A1/en active Application Filing
- 2011-01-27 CN CN201180008048.1A patent/CN102741433B/zh not_active Expired - Fee Related
- 2011-01-27 US US13/576,583 patent/US8926924B2/en not_active Expired - Fee Related
- 2011-01-27 AU AU2011212310A patent/AU2011212310B2/en active Active
- 2011-01-27 CA CA2787572A patent/CA2787572C/en active Active
-
2012
- 2012-07-23 ZA ZA2012/05548A patent/ZA201205548B/en unknown
- 2012-08-01 CL CL2012002137A patent/CL2012002137A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EA021530B1 (ru) | 2015-07-30 |
| EP2531626A4 (en) | 2014-11-19 |
| PE20130468A1 (es) | 2013-04-26 |
| EA201290647A1 (ru) | 2013-03-29 |
| CL2012002137A1 (es) | 2012-11-23 |
| AU2011212310A1 (en) | 2012-09-20 |
| AU2011212310B2 (en) | 2013-10-10 |
| US20120297929A1 (en) | 2012-11-29 |
| ES2621463T3 (es) | 2017-07-04 |
| CN102741433B (zh) | 2014-06-04 |
| MX2012008885A (es) | 2012-08-31 |
| BR112012019239B1 (pt) | 2018-02-14 |
| FI20100033A0 (fi) | 2010-02-02 |
| EP2531626A1 (en) | 2012-12-12 |
| FI122274B (fi) | 2011-11-15 |
| EP2531626B1 (en) | 2017-03-08 |
| CA2787572C (en) | 2016-05-03 |
| CA2787572A1 (en) | 2011-08-11 |
| ZA201205548B (en) | 2013-04-24 |
| WO2011095679A1 (en) | 2011-08-11 |
| FI20100033A (fi) | 2011-08-03 |
| US8926924B2 (en) | 2015-01-06 |
| CN102741433A (zh) | 2012-10-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| BR112012019239A2 (pt) | processo de extração | |
| CL2017002632A1 (es) | Proceso para lixiviar sulfuros de metal con reactivos que presentan grupos funcionales tiocarbonilo | |
| PE20040819A1 (es) | Proceso para recuperar un metal precioso a partir de un material | |
| PE20160329A1 (es) | Procesos para recuperar metales de soluciones acuosas | |
| BR112017000461A2 (pt) | agente de lixiviação e método de lixiviação para lixiviar uma terra rara em um minério de terra rara com adsorção de íons | |
| UA103575C2 (ru) | Способ выделения золота экстракцией растворителем | |
| BR112012029311A2 (pt) | processo de extração do solvente para separar cobalto de níquel em uma solução aquosa | |
| CL2017001257A1 (es) | Proceso para extraer metales a partir de los concentrados de minerales sulfurados que los contienen aplicando reducción directa con regeneración y reciclaje del agente reductor hierro y del fundente carbonato de sodio | |
| BR112015018771A2 (pt) | processo, método e sistema para remoção de metais pesados a partir de fluidos | |
| CL2012003214A1 (es) | Metodo para tratar una solucion acida que contiene iones yoduro y iones hierro (ii), que comprende oxidar los iones hierro en dicha solucion a iones hierro (iii) mediante microorganismos oxidantes del hierro, donde la oxidacion se efectua en presencia de carbon activado; y metodo para la lixiviacion de cobre a partir de una mena de sulfuro de cobre. | |
| BR112012014567A8 (pt) | processo de extração líquido-líquido para a purificação do urânio oriundo da dissolução nitria de um concentrado de urânio natural | |
| PE20151819A1 (es) | Metodo para recuperar oro a partir de minerales de oro conteniendo pirita | |
| CN104289184A (zh) | 一种2,4,6-三氯苯酚吸附剂及其应用 | |
| MX2015002140A (es) | Metodo de lixividacion en vertedero. | |
| PE20130977A1 (es) | Proceso de lixiviacion para concentrados de cobre que contienen calcopirita | |
| CL2017001589A1 (es) | Método de lixiviación en pilas | |
| BR112015004500A2 (pt) | método de produção para ímã permanente de terra rara | |
| CO6231046A2 (es) | Metodo y aparato para remover arsenico de un material portador de arsenico | |
| PH12018500427A1 (en) | Scandium oxide manufacturing method | |
| CL2015002889A1 (es) | Método para recuperar oro a partir de mineral de sulfuro. | |
| MX2014015865A (es) | Fijacion quimica de contaminantes metalicos in situ. | |
| CL2015002364A1 (es) | Método para lixiviar oro desde un mineral de oro que contiene pirita. | |
| BR112016013645A8 (pt) | método e disposição de processo para separação de índio e arsênico entre si | |
| AR059262A1 (es) | Solucion acuosa que comprende cianuro metalico para el proceso de cianuro destinado a la extraccion de oro y plata, proceso para preparar dicha solucion y uso de la misma. | |
| WU et al. | Determination of sulfur dioxide residues in Chinese materia medica by inline dialysis-ion chromatography |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] | ||
| B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE A 12A ANUIDADE. |
|
| B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2707 DE 22-11-2022 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |