BR102022007883A2 - DRYING PROCESS OF AGAVE SYRUP BY SPRAY DRYER, AGAVE POWDER AND ITS USE - Google Patents
DRYING PROCESS OF AGAVE SYRUP BY SPRAY DRYER, AGAVE POWDER AND ITS USE Download PDFInfo
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- BR102022007883A2 BR102022007883A2 BR102022007883-1A BR102022007883A BR102022007883A2 BR 102022007883 A2 BR102022007883 A2 BR 102022007883A2 BR 102022007883 A BR102022007883 A BR 102022007883A BR 102022007883 A2 BR102022007883 A2 BR 102022007883A2
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- Prior art keywords
- agave
- syrup
- weight
- drying
- spray dryer
- Prior art date
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- 244000193174 agave Species 0.000 title claims abstract description 34
- 238000001035 drying Methods 0.000 title claims abstract description 25
- 239000006188 syrup Substances 0.000 title claims abstract description 15
- 235000020357 syrup Nutrition 0.000 title claims abstract description 15
- 239000007921 spray Substances 0.000 title claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 18
- 239000000843 powder Substances 0.000 claims abstract description 13
- 239000000839 emulsion Substances 0.000 claims abstract description 10
- 230000008569 process Effects 0.000 claims abstract description 10
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 9
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 9
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000013305 food Nutrition 0.000 claims abstract description 7
- 230000001804 emulsifying effect Effects 0.000 claims abstract description 6
- 235000019909 Lorelite Nutrition 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 238000004945 emulsification Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 claims description 2
- 238000010981 drying operation Methods 0.000 claims description 2
- 238000009472 formulation Methods 0.000 claims description 2
- 239000004615 ingredient Substances 0.000 claims description 2
- 238000005063 solubilization Methods 0.000 claims description 2
- 230000007928 solubilization Effects 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 239000000047 product Substances 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 3
- 230000029087 digestion Effects 0.000 description 3
- 239000000428 dust Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 235000000346 sugar Nutrition 0.000 description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 238000000889 atomisation Methods 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 238000001694 spray drying Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 206010013911 Dysgeusia Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 208000006877 Insect Bites and Stings Diseases 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 206010052428 Wound Diseases 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- 230000008570 general process Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000000546 pharmaceutical excipient Substances 0.000 description 1
- 239000006041 probiotic Substances 0.000 description 1
- 235000018291 probiotics Nutrition 0.000 description 1
- 230000036186 satiety Effects 0.000 description 1
- 235000019627 satiety Nutrition 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 230000036559 skin health Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 150000008163 sugars Chemical group 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 230000001131 transforming effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/16—Evaporating by spraying
- B01D1/18—Evaporating by spraying to obtain dry solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/40—Mixing liquids with liquids; Emulsifying
- B01F23/41—Emulsifying
Landscapes
- Medicinal Preparation (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
processo de secagem de xarope de agave por spray dryer, agave em pó e seu uso. o presente pedido de patente de patente de invenção refere-se a um processo de secagem de xarope de agave utilizando-se a técnica de spray dryer, assim como o agave em pó obtido por esse processo e o seu uso. o campo de aplicação do presente pedido de patente de invenção está relacionado com a indústria alimentícia. os objetivos do presente pedido de patente de invenção são os de dissolver o agave com água para reduzir a viscosidade da calda; emulsionar a maltodextrina com o agave, em proporção pré-definida, no mixer ou bomba emulsificadora; secar a emulsão no aparelho spray dryer, obtendose assim, o produto agave em pó.drying process of agave syrup by spray dryer, agave powder and its use. The present patent application relates to a process for drying agave syrup using the spray dryer technique, as well as the agave powder obtained by this process and its use. The field of application of this patent application is related to the food industry. The objectives of the present patent application are to dissolve the agave with water to reduce the viscosity of the syrup; emulsify the maltodextrin with the agave, in a pre-defined proportion, in the mixer or emulsifying pump; dry the emulsion in the spray dryer, thus obtaining the powdered agave product.
Description
[001] O presente pedido de patente de patente de invenção refere-se a um processo de secagem de xarope de Agave utilizando-se a técnica de Spray Dryer, assim como o Agave em pó e o seu uso.[001] The present patent application refers to an Agave syrup drying process using the Spray Dryer technique, as well as Agave powder and its use.
[002] O campo de aplicação do presente pedido de patente de invenção está relacionado com a Indústria Alimentícia.[002] The field of application of this invention patent application is related to the Food Industry.
[003] De origem mexicana, o Agave é uma planta do tipo suculenta muito usada como adoçante e erva medicinal (para tratar problemas de digestão e possíveis lesões, por exemplo). Ela funciona como substituta saudável do açúcar refinado, pois contém um néctar docinho que pode ser usado em diferentes receitas. Os probióticos, para quem não sabe, são bactérias benéficas que contribuem para o funcionamento do intestino e facilitam a digestão. A boa notícia é que o agave, planta medicinal mexicana, é rico nessas substâncias e, por isso, é ótimo para manter a saúde do trato digestório. O agave é uma opção 100% natural e pode auxiliar na dieta de diabéticos do tipo 2. Ele é fonte de fibras, nutrientes que contribuem para a digestão, garantem saciedade e, ao mesmo tempo, ajudam a regular o colesterol e os níveis de açúcar no sangue. Por ter um alto teor de flavonoides (substâncias antioxidantes), o agave ajuda a fortalecer a imunidade, faz bem para a saúde da pele e atua como anti-inflamatório natural. Não é à toa que o néctar da planta é usado muitas vezes para tratar feridas, queimaduras e picadas de inseto - afinal, tem propriedades que amenizam dores e possíveis inflamações.[003] Of Mexican origin, Agave is a succulent plant widely used as a sweetener and medicinal herb (to treat digestion problems and possible injuries, for example). It works as a healthy substitute for refined sugar, as it contains a sweet nectar that can be used in different recipes. Probiotics, for those who don't know, are beneficial bacteria that contribute to the functioning of the intestine and facilitate digestion. The good news is that agave, a Mexican medicinal plant, is rich in these substances and, therefore, is great for maintaining the health of the digestive tract. Agave is a 100% natural option and can help in the diet of type 2 diabetics. It is a source of fiber, nutrients that contribute to digestion, ensure satiety and, at the same time, help regulate cholesterol and sugar levels in the blood. Because it has a high content of flavonoids (antioxidant substances), agave helps strengthen immunity, is good for skin health and acts as a natural anti-inflammatory. It's no surprise that the plant's nectar is often used to treat wounds, burns and insect bites - after all, it has properties that alleviate pain and possible inflammation.
[004] Por definição, o Spray Dryer é caracterizado pela transformação de um fluido (líquido) em um material com características sólidas, atomizando-o na forma de pequenas gotas em um meio de secagem quente. Essa técnica vem sendo utilizada há décadas, principalmente porque o funcionamento é simples. Inicialmente o fluido é pulverizado em uma câmara fechada de secagem, gerando milhões de microgotas individuais na ordem de 10 a 50 micrômetros. Nesse ambiente há a entrada de uma corrente de ar quente controlada, sendo forçada por ventiladores. Assim, o ar quente permite a secagem das microgotas de maneira eficiente, principalmente porque a área de contato com a corrente de ar é grande. Na técnica, o produto líquido irá secar suavemente e de forma instantânea sem choque térmico, transformando-se em pó extremamente fino e linear, garantindo maior padronização e qualidade final ao processo.[004] By definition, the Spray Dryer is characterized by the transformation of a fluid (liquid) into a material with solid characteristics, atomizing it in the form of small drops in a hot drying medium. This technique has been used for decades, mainly because it works so simply. Initially the fluid is sprayed into a closed drying chamber, generating millions of individual microdroplets on the order of 10 to 50 micrometers. In this environment, a controlled stream of hot air enters, being forced by fans. Thus, the hot air allows the microdroplets to dry efficiently, mainly because the contact area with the air current is large. In this technique, the liquid product will dry gently and instantly without thermal shock, transforming into an extremely fine and linear powder, ensuring greater standardization and final quality to the process.
[005] O documento US11033914B2 intitulado “Sistema de secagem por pulverização de leito fluidizado” refere-se a um sistema de secagem por pulverização de leito fluidizado para secagem de líquido em pó, incluindo uma câmara de secagem alongada, um conjunto de bico de pulverização na extremidade superior da câmara de secagem e uma câmara de coleta de pó na extremidade inferior da câmara de secagem. Uma entrada de gás de secagem é fornecida na câmara de coleta de pó e uma saída de gás de secagem é fornecida na extremidade superior da câmara de secagem. Uma pluralidade de elementos de filtro cilíndricos na extremidade superior da câmara de secagem está em comunicação com a saída de gás de exaustão para filtrar o pó carregado de gás de secagem do gás de secagem que sai da câmara de secagem.[005] Document US11033914B2 entitled “Fluidized Bed Spray Drying System” refers to a fluidized bed spray drying system for drying liquid to powder, including an elongated drying chamber, a spray nozzle assembly at the upper end of the drying chamber and a dust collection chamber at the lower end of the drying chamber. A drying gas inlet is provided in the dust collection chamber and a drying gas outlet is provided at the upper end of the drying chamber. A plurality of cylindrical filter elements at the upper end of the drying chamber are in communication with the exhaust gas outlet to filter drying gas-laden dust from the drying gas leaving the drying chamber.
[006] O documento ES2895376T3 refere-se a um método e aparelho para produzir partículas secas. A presente invenção refere-se a um método de preparação de uma composição em pó seco. Mais especificamente, a presente invenção refere-se a um método para a produção de partículas secas contendo um agente ativo. O método de preparação de uma composição em pó seco, caracterizado pelo fato de que compreende: combinar um primeiro componente e um segundo componente em um misturador estático para formar uma mistura, em que o primeiro componente compreende um agente ativo dissolvido em um solvente aquoso e o segundo componente compreende um excipiente dissolvido em um solvente orgânico; atomize a combinação para produzir microgotículas; e secar as gotas para formar partículas secas.[006] Document ES2895376T3 refers to a method and apparatus for producing dry particles. The present invention relates to a method of preparing a dry powder composition. More specifically, the present invention relates to a method for producing dry particles containing an active agent. The method of preparing a dry powder composition, characterized in that it comprises: combining a first component and a second component in a static mixer to form a mixture, wherein the first component comprises an active agent dissolved in an aqueous solvent and the second component comprises an excipient dissolved in an organic solvent; atomize the combination to produce microdroplets; and dry the droplets to form dry particles.
[007] Sendo assim, os objetivos do presente pedido de patente de invenção são os de: - dissolver o Agave com água para reduzir a viscosidade da calda; - emulsionar a Maltodextrina com o Agave, em proporção pré-definida, no mixer ou bomba emulsificadora; - secar a emulsão no aparelho Spray Dryer, obtendo-se assim, o produto agave em pó.[007] Therefore, the objectives of the present patent application are to: - dissolve the Agave with water to reduce the viscosity of the syrup; - emulsify the Maltodextrin with the Agave, in a pre-defined proportion, in the mixer or emulsifying pump; - dry the emulsion in the Spray Dryer, thus obtaining the powdered agave product.
[008] Como vantagens da presente invenção, pode-se destacar: - Produto orgânico; - Produto mais saudável que açúcar convencional; - Deixa os alimentos doces sem deixar retrogosto (amargor); - Reduzi a concentração de glicose em alimentos.[008] As advantages of the present invention, the following can be highlighted: - Organic product; - Healthier product than conventional sugar; - Leaves food sweet without leaving an aftertaste (bitterness); - Reduced the concentration of glucose in food.
[009] O presente pedido de invenção tem suas figuras e sua invenção melhor explicadas a seguir: A Figura 1 apresenta o processo geral de secagem do xarope de agave por Spray Dryer. O processo consiste nas seguintes etapas: - Etapa 1. Dissolveu-se o Agave com água para reduzir a viscosidade da calda. O líquido viscoso, de odor característico, de coloração amarelo dourado, densidade 1,380 g/cm3 (à 25oC) e viscosidade cinética 670 cSt (à 25oC). - Etapa 2. Emulsionou-se a Maltodextrina Lorelite 5 (65% em peso) com o agave (35% em peso), em proporção pré-definida (65/35 em peso), no mixer ou bomba emulsificadora (A). As proporções utilizadas são: 600 g de água desmineralizada; 300 g de Maltodextrina Lorelite 5 (95%) e 200 g de xarope de agave (80%).[009] The present application has its figures and invention better explained below: Figure 1 shows the general process of drying agave syrup by Spray Dryer. The process consists of the following steps: - Step 1. The Agave was dissolved in water to reduce the viscosity of the syrup. The viscous liquid, with a characteristic odor, golden yellow in color, density 1,380 g/cm3 (at 25oC) and kinetic viscosity 670 cSt (at 25oC). - Step 2. Maltodextrin Lorelite 5 (65% by weight) was emulsified with agave (35% by weight), in a pre-defined proportion (65/35 by weight), in the mixer or emulsifying pump (A). The proportions used are: 600 g of demineralized water; 300 g of Lorelite 5 Maltodextrin (95%) and 200 g of agave syrup (80%).
[010] A preparação da emulsão se deu da seguinte forma: carregou-se a água e iniciou-se o sistema de agitação do equipamento no modo mistura (A). Adicionou-se inicialmente a Maltodextrina Lorelite 5 (65% em peso), aguardando sua solubilização completa. Em seguida, adicionou-se o xarope de agave (35% em peso), mantendo-se a agitação. Após a mistura completa, iniciou-se o processo de emulsificação, utilizando-se a potência do MIXER ou bomba emulsificadora com rotor em linha de reciclo.[010] The emulsion was prepared as follows: water was loaded and the equipment's agitation system began in mixing mode (A). Maltodextrin Lorelite 5 (65% by weight) was initially added, waiting for its complete solubilization. Then, agave syrup (35% by weight) was added, stirring continued. After complete mixing, the emulsification process began, using the power of the MIXER or emulsifying pump with in-line recycle rotor.
[011] Com a formulação ingrediente proposta, foi possível obter uma emulsão estável, suficiente para manter o processo de alimentação do atomizador homogêneo e tempo de preparações adequado para manter a operação contínua de secagem. O xarope de agave é uma composição de açúcares muito solúvel em água e essa característica facilita a limpeza e descontaminação dos equipamentos e acessórios utilizados nas preparações. - Etapa 3. Secagem da emulsão no aparelho Spray Dryer (B). Obtém-se o produto agave em pó. Características da emulsão: emulsão límpida, de coloração amarelo claro, com densidade de 1,130 g/cm3(à 25 oC) e viscosidade cinética 80 cSt (à 25oC). A temperatura do ar de entrada (TE) foi de 140 oC. A temperatura do ar de saída (TS) foi de 78 oC. A pressão do atomizador foi de 8,0 bar. A potência do exaustor foi de 100%. A vazão média da bomba de admissão foi de 20 a 25%. A quantidade de suspensão à secar foi de 960 g. O tempo de secagem foi de 1h 30 min.[011] With the proposed ingredient formulation, it was possible to obtain a stable emulsion, sufficient to maintain the homogeneous atomizer feeding process and adequate preparation time to maintain the continuous drying operation. Agave syrup is a composition of sugars that is very soluble in water and this characteristic facilitates the cleaning and decontamination of equipment and accessories used in preparations. - Step 3. Drying the emulsion in the Spray Dryer (B). The agave product is obtained in powder form. Emulsion characteristics: clear, light yellow emulsion, with a density of 1.130 g/cm3 (at 25 oC) and kinetic viscosity 80 cSt (at 25 oC). The inlet air temperature (TE) was 140 oC. The outlet air temperature (TS) was 78 oC. The atomizer pressure was 8.0 bar. The exhaust fan power was 100%. The average flow rate of the intake pump was 20 to 25%. The amount of suspension to be dried was 960 g. Drying time was 1h 30 min.
[012] Estabilizados os parâmetros de atomização e secagem, a secagem se procedeu de forma tranquila, onde se observou o produto em pó bastante fino em função do processo de atomização em disco rotativo.[012] Once the atomization and drying parameters were stabilized, drying proceeded smoothly, where the product was observed to be in very fine powder form due to the atomization process on a rotating disc.
[013] Como características relevantes da presente invenção, destacam-se a facilidade de uso por ser um produto em pó; além do menor custo de frete no transporte; menor uso de glicose em alimentos; a criação de uma nova tecnologia, além de agregar a mesma à indústria alimentícia.[013] Relevant characteristics of the present invention include ease of use as it is a powder product; in addition to lower shipping costs; lower use of glucose in food; the creation of a new technology, in addition to adding it to the food industry.
Claims (3)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BR102022007883-1A BR102022007883A2 (en) | 2022-04-26 | 2022-04-26 | DRYING PROCESS OF AGAVE SYRUP BY SPRAY DRYER, AGAVE POWDER AND ITS USE |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BR102022007883-1A BR102022007883A2 (en) | 2022-04-26 | 2022-04-26 | DRYING PROCESS OF AGAVE SYRUP BY SPRAY DRYER, AGAVE POWDER AND ITS USE |
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| Publication Number | Publication Date |
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| BR102022007883A2 true BR102022007883A2 (en) | 2023-10-31 |
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| BR102022007883-1A BR102022007883A2 (en) | 2022-04-26 | 2022-04-26 | DRYING PROCESS OF AGAVE SYRUP BY SPRAY DRYER, AGAVE POWDER AND ITS USE |
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| BR (1) | BR102022007883A2 (en) |
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