BE538757A - - Google Patents
Info
- Publication number
- BE538757A BE538757A BE538757DA BE538757A BE 538757 A BE538757 A BE 538757A BE 538757D A BE538757D A BE 538757DA BE 538757 A BE538757 A BE 538757A
- Authority
- BE
- Belgium
- Prior art keywords
- lime
- glycerin
- precipitate
- oxidation
- oxidant
- Prior art date
Links
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 42
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 26
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 26
- 239000004571 lime Substances 0.000 claims description 26
- 239000002244 precipitate Substances 0.000 claims description 21
- 235000011187 glycerol Nutrition 0.000 claims description 19
- 235000000346 sugar Nutrition 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 12
- 230000003647 oxidation Effects 0.000 claims description 11
- 238000007254 oxidation reaction Methods 0.000 claims description 11
- 239000002253 acid Substances 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 7
- 238000006243 chemical reaction Methods 0.000 claims description 7
- 239000008103 glucose Substances 0.000 claims description 7
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 150000008163 sugars Chemical class 0.000 claims description 6
- 239000007800 oxidant agent Substances 0.000 claims description 5
- 230000001590 oxidative effect Effects 0.000 claims description 5
- 159000000007 calcium salts Chemical class 0.000 claims description 4
- 239000003153 chemical reaction reagent Substances 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 2
- 150000002972 pentoses Chemical class 0.000 claims description 2
- 230000009466 transformation Effects 0.000 claims 2
- 239000000376 reactant Substances 0.000 claims 1
- 238000000844 transformation Methods 0.000 claims 1
- 230000008030 elimination Effects 0.000 description 7
- 238000003379 elimination reaction Methods 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- WXOMTJVVIMOXJL-BOBFKVMVSA-A O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)OS(=O)(=O)OC[C@H]1O[C@@H](O[C@]2(COS(=O)(=O)O[Al](O)O)O[C@H](OS(=O)(=O)O[Al](O)O)[C@@H](OS(=O)(=O)O[Al](O)O)[C@@H]2OS(=O)(=O)O[Al](O)O)[C@H](OS(=O)(=O)O[Al](O)O)[C@@H](OS(=O)(=O)O[Al](O)O)[C@@H]1OS(=O)(=O)O[Al](O)O Chemical compound O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)O.O[Al](O)OS(=O)(=O)OC[C@H]1O[C@@H](O[C@]2(COS(=O)(=O)O[Al](O)O)O[C@H](OS(=O)(=O)O[Al](O)O)[C@@H](OS(=O)(=O)O[Al](O)O)[C@@H]2OS(=O)(=O)O[Al](O)O)[C@H](OS(=O)(=O)O[Al](O)O)[C@@H](OS(=O)(=O)O[Al](O)O)[C@@H]1OS(=O)(=O)O[Al](O)O WXOMTJVVIMOXJL-BOBFKVMVSA-A 0.000 description 5
- 150000001323 aldoses Chemical class 0.000 description 5
- 239000011575 calcium Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 4
- 229910052601 baryte Inorganic materials 0.000 description 4
- 239000010428 baryte Substances 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 3
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- VBIXEXWLHSRNKB-UHFFFAOYSA-N ammonium oxalate Chemical compound [NH4+].[NH4+].[O-]C(=O)C([O-])=O VBIXEXWLHSRNKB-UHFFFAOYSA-N 0.000 description 2
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 235000019253 formic acid Nutrition 0.000 description 2
- 229910017604 nitric acid Inorganic materials 0.000 description 2
- 150000003538 tetroses Chemical class 0.000 description 2
- 238000012795 verification Methods 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 description 1
- RGHNJXZEOKUKBD-SQOUGZDYSA-N Gluconic acid Natural products OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000000174 gluconic acid Substances 0.000 description 1
- 235000012208 gluconic acid Nutrition 0.000 description 1
- 235000012204 lemonade/lime carbonate Nutrition 0.000 description 1
- 235000020094 liqueur Nutrition 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000010517 secondary reaction Methods 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/18—Polyhydroxylic acyclic alcohols
- C07C31/22—Trihydroxylic alcohols, e.g. glycerol
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Saccharide Compounds (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BE538757A true BE538757A (ref) |
Family
ID=168675
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BE538757D BE538757A (ref) |
Country Status (1)
| Country | Link |
|---|---|
| BE (1) | BE538757A (ref) |
-
0
- BE BE538757D patent/BE538757A/fr unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0518765B1 (fr) | Procédé pour l'obtention de polyglycérols et d'esters de polyglycérols | |
| US8052953B2 (en) | Method for recovering sulfuric acid from concentrated acid hydrolysate of plant cellulose material | |
| JP2012144441A (ja) | イオン液体、イオン液体の精製方法、およびセルロース系バイオマスの処理方法 | |
| WO2023279276A1 (zh) | 三氯蔗糖-6-酯的提纯方法 | |
| JP7812451B2 (ja) | トウモロコシ穂軸を用いて良質なキシロースと高級キャラメル色素を同時生産するシステム及び方法 | |
| BE538757A (ref) | ||
| SU1701115A3 (ru) | Способ получени сахаров из целлюлозосодержащего материала | |
| CN101434535B (zh) | 一种天然阿魏酸的制备方法 | |
| Geerligs | Cane sugar and its manufacture | |
| CN106589032A (zh) | 一种甲睾酮母液的处理方法 | |
| JPH0785720B2 (ja) | 高能率オルガノソルブ糖化法 | |
| US2389173A (en) | Recovery of glycerol from fermented liquors | |
| WO1986000906A1 (fr) | Procede de synthese d'aldosides ou de polyaldosides d'alkyle, de cycloalkyle ou d'alcenyle | |
| US2806892A (en) | Recovering trimethylolethane by ethyl acetate extraction | |
| CN117024267A (zh) | 一种bhb-镁的制备工艺 | |
| Lachman | The Benzil Rearrangement. III | |
| FR2760016A1 (fr) | Procede de fabrication industrielle de diosmine a partir de l'hesperidine | |
| CN117416997A (zh) | 一种以羰基镍粉为原料生产镍盐溶液的方法 | |
| Spoehr | On the behavior of the ordinary hexoses towards hydrogen peroxide in the presence of alkaline hydroxides, as well as of various iron salts... | |
| BE407583A (ref) | ||
| WO2025065148A1 (zh) | 一种卤水碳酸锂制备电池级碳酸锂的方法 | |
| CN116903483A (zh) | 一种氨基酸表面活性剂及其制备方法和应用 | |
| CN119504418A (zh) | 一种生物发酵法生产的长碳链二元酸的提取精制方法 | |
| BE554670A (ref) | ||
| US674412A (en) | Compound of sulfonized mineral oils containing formaldehyde and process of making same. |