BE530340A - - Google Patents
Info
- Publication number
- BE530340A BE530340A BE530340DA BE530340A BE 530340 A BE530340 A BE 530340A BE 530340D A BE530340D A BE 530340DA BE 530340 A BE530340 A BE 530340A
- Authority
- BE
- Belgium
- Prior art keywords
- acetone
- zone
- fraction
- distillation
- pipe
- Prior art date
Links
- CSCPPACGZOOCGX-UHFFFAOYSA-N acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 154
- 238000004821 distillation Methods 0.000 claims description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 33
- 238000006243 chemical reaction Methods 0.000 claims description 25
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 21
- YQHLDYVWEZKEOX-UHFFFAOYSA-N Cumene hydroperoxide Chemical compound OOC(C)(C)C1=CC=CC=C1 YQHLDYVWEZKEOX-UHFFFAOYSA-N 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 19
- 238000000354 decomposition reaction Methods 0.000 claims description 11
- 238000010992 reflux Methods 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 10
- 239000003085 diluting agent Substances 0.000 claims description 9
- 230000001264 neutralization Effects 0.000 claims description 9
- 238000004508 fractional distillation Methods 0.000 claims description 8
- 150000003839 salts Chemical class 0.000 claims description 8
- 239000011780 sodium chloride Substances 0.000 claims description 8
- IKHGUXGNUITLKF-UHFFFAOYSA-N acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims 1
- 230000003472 neutralizing Effects 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 12
- 238000010494 dissociation reaction Methods 0.000 description 11
- 230000005593 dissociations Effects 0.000 description 11
- 239000000047 product Substances 0.000 description 11
- 230000014759 maintenance of location Effects 0.000 description 7
- 230000005591 charge neutralization Effects 0.000 description 6
- 238000006386 neutralization reaction Methods 0.000 description 6
- NPDODHDPVPPRDJ-UHFFFAOYSA-N permanganate Chemical compound [O-][Mn](=O)(=O)=O NPDODHDPVPPRDJ-UHFFFAOYSA-N 0.000 description 6
- 239000010410 layer Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- RWGFKTVRMDUZSP-UHFFFAOYSA-N Cumene Chemical compound CC(C)C1=CC=CC=C1 RWGFKTVRMDUZSP-UHFFFAOYSA-N 0.000 description 3
- 239000003377 acid catalyst Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000011541 reaction mixture Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- VZJVWSHVAAUDKD-UHFFFAOYSA-N Potassium permanganate Chemical compound [K+].[O-][Mn](=O)(=O)=O VZJVWSHVAAUDKD-UHFFFAOYSA-N 0.000 description 2
- KWOLFJPFCHCOCG-UHFFFAOYSA-N methylphenylketone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- NESLWCLHZZISNB-UHFFFAOYSA-M sodium phenolate Chemical compound [Na+].[O-]C1=CC=CC=C1 NESLWCLHZZISNB-UHFFFAOYSA-M 0.000 description 2
- 238000009834 vaporization Methods 0.000 description 2
- BDCFWIDZNLCTMF-UHFFFAOYSA-N 2-phenylpropan-2-ol Chemical compound CC(C)(O)C1=CC=CC=C1 BDCFWIDZNLCTMF-UHFFFAOYSA-N 0.000 description 1
- MLUCVPSAIODCQM-NSCUHMNNSA-N Crotonaldehyde Chemical compound C\C=C\C=O MLUCVPSAIODCQM-NSCUHMNNSA-N 0.000 description 1
- 241001292274 Eumenes Species 0.000 description 1
- FUSUHKVFWTUUBE-UHFFFAOYSA-N Methyl vinyl ketone Chemical compound CC(=O)C=C FUSUHKVFWTUUBE-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating Effects 0.000 description 1
- 238000007792 addition Methods 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- -1 hydrogen ions Chemical class 0.000 description 1
- MHAJPDPJQMAIIY-UHFFFAOYSA-N hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000012044 organic layer Substances 0.000 description 1
- 230000001590 oxidative Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000001603 reducing Effects 0.000 description 1
- 239000003638 reducing agent Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000001187 sodium carbonate Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/08—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by decomposition of hydroperoxides, e.g. cumene hydroperoxide
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/04—Saturated compounds containing keto groups bound to acyclic carbon atoms
- C07C49/08—Acetone
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Publications (1)
Publication Number | Publication Date |
---|---|
BE530340A true BE530340A (de) |
Family
ID=163021
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BE530340D BE530340A (de) |
Country Status (1)
Country | Link |
---|---|
BE (1) | BE530340A (de) |
-
0
- BE BE530340D patent/BE530340A/fr unknown
Similar Documents
Publication | Publication Date | Title |
---|---|---|
FR2462392A1 (fr) | Oxydation de matieres organiques dans des solutions aqueuses de sels | |
EP0578194B1 (de) | Verfahren zur Herstellung von Phenol und Methylethylketon | |
BE530340A (de) | ||
EP0121466B1 (de) | Verfahren für die Dekomposition eines Komplexes von Orthobenzoylbenzoesäure, Wasserstofffluorid und Bortrifluorid | |
EP1018500A2 (de) | Verfahren zur Isolierung von Glykolen | |
JP3552306B2 (ja) | プロピレンオキシドとスチレンモノマーの製造法 | |
FR2529196A1 (fr) | Purification de phenol | |
JPH02115136A (ja) | ジクロロヒドリンの連続的製造方法 | |
BE496062A (de) | ||
EP0296990B1 (de) | Verfahren zur Herstellung von hydroxyliertem Polybutadien | |
FR2546514A1 (fr) | Procede et systeme pour la production d'ethanol | |
BE571099A (de) | ||
FR2545082A1 (fr) | Procede de purification d'un compose de carbonyle fluore melange a du fluorure d'hydrogene | |
BE488522A (de) | ||
CH654558A5 (fr) | Procede pour la production d'oxyfluorure de niobium. | |
SU334691A1 (ru) | Способ получения низших алифатических меркаптанов | |
BE420769A (de) | ||
BE499365A (de) | ||
BE563303A (de) | ||
BE616319A (de) | ||
BE490442A (de) | ||
FR2554808A1 (en) | Treating mother liquor from hexa:bromo cyclododecane prodn. | |
BE491627A (de) | ||
BE634961A (de) | ||
FR2477532A1 (fr) | Procede continu de preparation de dichlorhydrines de glycerine et produits obtenus par ce procede |