BE459399A - - Google Patents

Info

Publication number

BE459399A

BE459399A BE459399DA BE459399A BE 459399 A BE459399 A BE 459399A BE 459399D A BE459399D A BE 459399DA BE 459399 A BE459399 A BE 459399A

Authority

BE

Belgium

Prior art keywords

parts

tertiary

solution

alcohol

mercury

Prior art date

Links

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• 230000000855 fungicidal effect Effects 0.000 claims description 6
• 230000001034 aminogenic effect Effects 0.000 claims description 5
• 230000000844 anti-bacterial effect Effects 0.000 claims description 5
• 239000000417 fungicide Substances 0.000 claims description 5
• 239000002917 insecticide Substances 0.000 claims description 5
• 239000003899 bactericide agent Substances 0.000 claims description 4
• 239000003795 chemical substances by application Substances 0.000 claims description 4
• -1 alkyl mercury salts Chemical class 0.000 claims description 3
• 150000004679 hydroxides Chemical class 0.000 claims description 3
• 238000000034 method Methods 0.000 claims description 2
• 239000000243 solution Substances 0.000 description 19
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 12
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
• 150000002731 mercury compounds Chemical class 0.000 description 5
• VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 4
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
• 238000009835 boiling Methods 0.000 description 4
• 150000001875 compounds Chemical class 0.000 description 4
• 239000000706 filtrate Substances 0.000 description 4
• 239000000203 mixture Substances 0.000 description 4
• QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
• DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
• UREACWLAXSOUKG-UHFFFAOYSA-M ethylmercury(1+);bromide Chemical compound CC[Hg]Br UREACWLAXSOUKG-UHFFFAOYSA-M 0.000 description 3
• 238000010992 reflux Methods 0.000 description 3
• 150000003839 salts Chemical class 0.000 description 3
• 229910052708 sodium Inorganic materials 0.000 description 3
• 239000011734 sodium Substances 0.000 description 3
• DENMGZODXQRYAR-UHFFFAOYSA-N 2-(dimethylamino)ethanethiol Chemical compound CN(C)CCS DENMGZODXQRYAR-UHFFFAOYSA-N 0.000 description 2
• WPQZXRFFGSOHES-UHFFFAOYSA-M bromo(propyl)mercury Chemical compound CCC[Hg]Br WPQZXRFFGSOHES-UHFFFAOYSA-M 0.000 description 2
• 239000000645 desinfectant Substances 0.000 description 2
• 150000002019 disulfides Chemical class 0.000 description 2
• 239000000839 emulsion Substances 0.000 description 2
• NRVFDGZJTPCULU-UHFFFAOYSA-N meda Chemical compound Cl.CN(C)CCS NRVFDGZJTPCULU-UHFFFAOYSA-N 0.000 description 2
• 239000000155 melt Substances 0.000 description 2
• 239000000843 powder Substances 0.000 description 2
• 238000002360 preparation method Methods 0.000 description 2
• 238000001953 recrystallisation Methods 0.000 description 2
• QIVUCLWGARAQIO-OLIXTKCUSA-N (3s)-n-[(3s,5s,6r)-6-methyl-2-oxo-1-(2,2,2-trifluoroethyl)-5-(2,3,6-trifluorophenyl)piperidin-3-yl]-2-oxospiro[1h-pyrrolo[2,3-b]pyridine-3,6'-5,7-dihydrocyclopenta[b]pyridine]-3'-carboxamide Chemical compound C1([C@H]2[C@H](N(C(=O)[C@@H](NC(=O)C=3C=C4C[C@]5(CC4=NC=3)C3=CC=CN=C3NC5=O)C2)CC(F)(F)F)C)=C(F)C=CC(F)=C1F QIVUCLWGARAQIO-OLIXTKCUSA-N 0.000 description 1
• PBLNBZIONSLZBU-UHFFFAOYSA-N 1-bromododecane Chemical compound CCCCCCCCCCCCBr PBLNBZIONSLZBU-UHFFFAOYSA-N 0.000 description 1
• QAXLTZBBDSDRPW-UHFFFAOYSA-N 2-(diethylamino)ethanethiol;hydron;chloride Chemical compound Cl.CCN(CC)CCS QAXLTZBBDSDRPW-UHFFFAOYSA-N 0.000 description 1
• LJUWVUOZDFPLDY-UHFFFAOYSA-N 2-[2,2-bis(dimethylamino)ethyldisulfanyl]-1-N,1-N,1-N',1-N'-tetramethylethane-1,1-diamine hydrochloride Chemical compound Cl.CN(C)C(CSSCC(N(C)C)N(C)C)N(C)C LJUWVUOZDFPLDY-UHFFFAOYSA-N 0.000 description 1
• PQSBRHXGVPVYFJ-UHFFFAOYSA-N 4-(dimethylamino)benzenethiol Chemical compound CN(C)C1=CC=C(S)C=C1 PQSBRHXGVPVYFJ-UHFFFAOYSA-N 0.000 description 1
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
• NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical group C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 description 1
• 230000001476 alcoholic effect Effects 0.000 description 1
• 125000000217 alkyl group Chemical group 0.000 description 1
• 125000002947 alkylene group Chemical group 0.000 description 1
• XSDQTOBWRPYKKA-UHFFFAOYSA-N amiloride Chemical compound NC(=N)NC(=O)C1=NC(Cl)=C(N)N=C1N XSDQTOBWRPYKKA-UHFFFAOYSA-N 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• 125000003118 aryl group Chemical group 0.000 description 1
• 125000000732 arylene group Chemical group 0.000 description 1
• ONDJORBPBJVUQX-UHFFFAOYSA-N bromoethane;mercury Chemical compound [Hg].CCBr ONDJORBPBJVUQX-UHFFFAOYSA-N 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• 125000000753 cycloalkyl group Chemical group 0.000 description 1
• 238000004821 distillation Methods 0.000 description 1
• 239000003995 emulsifying agent Substances 0.000 description 1
• 125000005448 ethoxyethyl group Chemical group [H]C([H])([H])C([H])([H])OC([H])([H])C([H])([H])* 0.000 description 1
• 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
• IHXIVQZIZFYPEG-UHFFFAOYSA-M ethyl-dimethyl-(1-phenoxydodecyl)azanium bromide Chemical compound [Br-].CCCCCCCCCCCC([N+](C)(C)CC)OC1=CC=CC=C1 IHXIVQZIZFYPEG-UHFFFAOYSA-M 0.000 description 1
• ULCGBFPYDQUTHX-UHFFFAOYSA-M ethylmercury(1+);hydroxide Chemical compound [OH-].CC[Hg+] ULCGBFPYDQUTHX-UHFFFAOYSA-M 0.000 description 1
• 238000001914 filtration Methods 0.000 description 1
• 125000000623 heterocyclic group Chemical group 0.000 description 1
• 230000000749 insecticidal effect Effects 0.000 description 1
• 238000004519 manufacturing process Methods 0.000 description 1
• QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
• 229910052753 mercury Inorganic materials 0.000 description 1
• 229910052751 metal Inorganic materials 0.000 description 1
• 239000002184 metal Substances 0.000 description 1
• RUHVDRGWCIAFLG-UHFFFAOYSA-N n,n-dimethyl-2-phenoxyethanamine Chemical compound CN(C)CCOC1=CC=CC=C1 RUHVDRGWCIAFLG-UHFFFAOYSA-N 0.000 description 1
• 150000002894 organic compounds Chemical class 0.000 description 1
• 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
• 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 description 1
• XEBWQGVWTUSTLN-UHFFFAOYSA-M phenylmercury acetate Chemical compound CC(=O)O[Hg]C1=CC=CC=C1 XEBWQGVWTUSTLN-UHFFFAOYSA-M 0.000 description 1
• 239000000047 product Substances 0.000 description 1
• 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
• WGJDWRPHMYVQFO-UHFFFAOYSA-M propylmercury(1+) hydroxide Chemical compound [OH-].C(CC)[Hg+] WGJDWRPHMYVQFO-UHFFFAOYSA-M 0.000 description 1
• 230000001681 protective effect Effects 0.000 description 1
• 125000004076 pyridyl group Chemical group 0.000 description 1