BE1004829A6 - Method for extracting natural detergent and organic fertilising agent fromtea seed residue - Google Patents

Method for extracting natural detergent and organic fertilising agent fromtea seed residue Download PDF

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Publication number
BE1004829A6
BE1004829A6 BE9100090A BE9100090A BE1004829A6 BE 1004829 A6 BE1004829 A6 BE 1004829A6 BE 9100090 A BE9100090 A BE 9100090A BE 9100090 A BE9100090 A BE 9100090A BE 1004829 A6 BE1004829 A6 BE 1004829A6
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BE
Belgium
Prior art keywords
surfactant
saponin
seed residue
natural detergent
natural
Prior art date
Application number
BE9100090A
Other languages
French (fr)
Inventor
Tcheng Go-Long
Original Assignee
Ryhshine Ind Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ryhshine Ind Corp filed Critical Ryhshine Ind Corp
Priority to BE9100090A priority Critical patent/BE1004829A6/en
Application granted granted Critical
Publication of BE1004829A6 publication Critical patent/BE1004829A6/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/382Vegetable products, e.g. soya meal, wood flour, sawdust
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F5/00Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
    • C05F5/006Waste from chemical processing of material, e.g. diestillation, roasting, cooking
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/10Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
    • Y02A40/20Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Botany (AREA)
  • Environmental & Geological Engineering (AREA)
  • Processing Of Solid Wastes (AREA)
  • Fertilizers (AREA)

Abstract

The invention relates to a method for extracting a natural detergent and anorganic fertilisation agent or fertiliser from tea seed residue whichcomprises the grinding of the tea seed residue into a powder. After mixingwith water, the saponin and the surface-active substance of the solution aredistilled. After distillation and dehydration, a food grade alcohol is addedto the saponin and to the surface-active substance to form a neutraldetergent. The powdery sediment from the distillation process is dried toform crystallised grains to be used as a natural organic fertilisation agentor fertiliser.

Description

       

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  Procédé d'extraction d'un détergent naturel et d'un agent fertilisant organique de résidus de semences de thé Arrière-plan de l'invention
La présente invention concerne un procédé permettant d'extraire un détergent naturel et un agent fertilisant organique de résidus de semences de thé. 



   Le thé est une plante toujours verte, à fleurs blanches, appartenant à la famille du thé, qui pousse en Chine, en Inde, au Japon, etc ; ses feuilles séchées et préparées sont couramment employées pour préparer une boisson et on peut soumettre ces semences à une extraction en vue de produire une essence de semences de thé comestible. Après extraction de l'essence de semences de thé, il subsiste un résidu de saveur amère, qui contient des substances alcalines et de la saponine et qui n'est pas approprié à titre d'agent fertilisant général permettant d'améliorer la qualité de la croissance de plantes. Le résidu des semences de thé s'utilise à présent couramment comme pesticide pour tuer les insectes dans les pêcheries. 



  Résumé de l'invention
L'invention a pour principal objet d'extraire un détergent naturel et un agent fertilisant organique des résidus de semences ou graines de thé. Conformément à la présente invention, on broie les résidus de semences ou graines de thé en une poudre que l'on mélange à de l'eau pour obtenir une solution. On sépare ensuite la saponine et l'agent tensioactif ou surfactif de la solution par distillation. Après le processus de distillation-déshydratation, on ajoute un alcool de qualité comestible à la saponine et à l'agent tensioactif ou surfactif pour former un détergent condensé, neutre. On sèche le sédi- 

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 ment pulvérulent du processus de distillation pour former des grains cristallisés que l'on utilise comme agent de fertilisation ou engrais organique naturel. 



   On donne ci-dessous un schéma de préparation de l'agent de fertilisation ou engrais organique et du détergent naturel. 

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 EMI3.1 
 

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 EMI4.1 
 Description détaillée de la forme de réalisation préférée 
En se reportant au schéma qui précède, on voit que l'on broie le résidu des semences de thé jusqu'à obtenir une poudre (par exemple : 140 meshes) et on mélange ensuite la poudre à de l'eau dans un rapport pondéral de 1 : 1 et on soumet le mélange à un processus de distillation à une température qui varie de 110 à   150 C.   Au cours du processus de distillation, on peut séparer une base pour savon et une substance tensioactive ou surfactice de la solution. On distille alors la saponine et la substance tensioactive ou surfactive et on les déshydrate pour en augmenter la densité.

   Après la déshydratation, on ajoute une fraction appropriée (des plus avantageusement 0,003%) d'alcool de qualité alimentaire à la saponine et à la substance tensioactive ou surfactive en vue de protéger la protéine résiduelle d'une dégradation, comme aussi de former un détergent naturel qui possède une valeur de pH de 7,3 (solution aqueuse à 0,25% à   25 C).   



   Le sédiment pulvérulent qui subsiste après le processus de distillation à haute température est ensuite séché en grains cristallisés et s'utilise alors à titre d'agent de fertilisation ou engrais organique naturel. L'agent de fertilisation ou engrais organique naturel est très stable et ne se dégrade pas facilement et contient une proportion élevée d'azote (N), de pentoxyde de phosphore   (PO)   et d'oxyde de potassium   (K20).   



   Comme on l'a décrit plus haut, l'objet de la présente invention réside dans un détergent naturel extrait et un agent de fertilisation ou engrais organique extrait de résidus de semences de thé, de manière à tirer plein bénéfice des   résidus   des semences de thé.



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  Method for extracting a natural detergent and an organic fertilizer from tea seed residues Background of the invention
The present invention relates to a method for extracting a natural detergent and an organic fertilizer from tea seed residues.



   Tea is an evergreen plant, with white flowers, belonging to the tea family, which grows in China, India, Japan, etc; its dried and prepared leaves are commonly used to prepare a beverage and these seeds can be extracted to produce an edible tea seed essence. After extracting the essence from tea seeds, there remains a bitter flavor residue, which contains alkaline substances and saponin and which is not suitable as a general fertilizing agent making it possible to improve the quality of the plant growth. The residue from tea seeds is now widely used as a pesticide to kill insects in fisheries.



  Summary of the invention
The main object of the invention is to extract a natural detergent and an organic fertilizer from seed residues or tea seeds. According to the present invention, the seed residues or tea seeds are ground into a powder which is mixed with water to obtain a solution. The saponin and the surfactant or surfactant are then separated from the solution by distillation. After the distillation-dehydration process, edible grade alcohol is added to the saponin and the surfactant or surfactant to form a condensed, neutral detergent. The sediment is dried

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 powdery from the distillation process to form crystallized grains which are used as a fertilizer or natural organic fertilizer.



   A diagram of preparation of the fertilizer or organic fertilizer and the natural detergent is given below.

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 EMI3.1
 

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 EMI4.1
 Detailed description of the preferred embodiment
Referring to the above diagram, it can be seen that the residue of the tea seeds is ground until a powder is obtained (for example: 140 meshes) and the powder is then mixed with water in a weight ratio of 1: 1 and the mixture is subjected to a distillation process at a temperature which varies from 110 to 150 C. During the distillation process, a soap base and a surfactant or surfactant can be separated from the solution. The saponin and the surfactant or surfactant are then distilled and dehydrated to increase the density.

   After dehydration, an appropriate fraction (most preferably 0.003%) of food grade alcohol is added to the saponin and to the surfactant or surfactant to protect the residual protein from degradation, as well as to form a detergent natural which has a pH value of 7.3 (0.25% aqueous solution at 25 C).



   The powdery sediment which remains after the high temperature distillation process is then dried into crystallized grains and is then used as a fertilizer or natural organic fertilizer. The natural organic fertilizer or fertilizer is very stable and does not degrade easily and contains a high proportion of nitrogen (N), phosphorus pentoxide (PO) and potassium oxide (K20).



   As described above, the object of the present invention resides in a natural detergent extract and an organic fertilizer or fertilizer extracted from tea seed residues, so as to derive full benefit from the residues of tea seeds .


    

Claims (1)

Revendication 1. Procédé d'extraction d'un détergent naturel et d'un agent de fertilisation ou engrais organique de résidus de semences de thé, caractérisé en ce qu'il comprend une première étape de broyage des résidus des semences de thé en une poudre, une seconde étape de mélange de la poudre ainsi obtenue à de l'eau, une troisième étape de distillation de la saponine et d'une substance tensioactive ou surfactive de la solution ainsi obtenue, une quatrième étape de distillation et de déshydratation de la saponine et de la substance tensioactive ou surfactive, Claim 1. Method for extracting a natural detergent and an organic fertilizer or fertilizer from tea seed residues, characterized in that it comprises a first stage of grinding the residues of tea seeds into a powder , a second stage of mixing the powder thus obtained with water, a third stage of distillation of the saponin and of a surfactant or surface-active substance of the solution thus obtained, a fourth stage of distillation and dehydration of the saponin and surfactant or surfactant, une cinquième étape de mélange d'un alcool de qualité alimentaire à la saponine et à la substance tensioactive ou surfactive de manière à obtenir un détergent naturel et une sixième étape de séchage du sédiment pulvérulent pour obtenir des grains cristallins à utiliser comme agent de fertilisation ou engrais organique naturel.  a fifth step of mixing a food-grade alcohol with the saponin and the surfactant or surfactant so as to obtain a natural detergent and a sixth step of drying the powdery sediment to obtain crystalline grains to be used as fertilizer or natural organic fertilizer.
BE9100090A 1991-01-30 1991-01-30 Method for extracting natural detergent and organic fertilising agent fromtea seed residue BE1004829A6 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
BE9100090A BE1004829A6 (en) 1991-01-30 1991-01-30 Method for extracting natural detergent and organic fertilising agent fromtea seed residue

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
BE9100090A BE1004829A6 (en) 1991-01-30 1991-01-30 Method for extracting natural detergent and organic fertilising agent fromtea seed residue

Publications (1)

Publication Number Publication Date
BE1004829A6 true BE1004829A6 (en) 1993-02-02

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Family Applications (1)

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BE9100090A BE1004829A6 (en) 1991-01-30 1991-01-30 Method for extracting natural detergent and organic fertilising agent fromtea seed residue

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102674961A (en) * 2012-05-05 2012-09-19 管天球 Organic fertilizer produced from tea cakes
CN104086246A (en) * 2014-07-27 2014-10-08 安徽科技学院 Method for producing iron-rich organic fertilizer by utilizing waste tea residues
CN111304662A (en) * 2020-04-10 2020-06-19 湖南淳湘农林科技有限公司 Preparation method of tea seed cake cleaning agent
CN112608182A (en) * 2020-12-17 2021-04-06 江苏农林职业技术学院 Formula and preparation method of tea byproduct fermented fertilizer

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102674961A (en) * 2012-05-05 2012-09-19 管天球 Organic fertilizer produced from tea cakes
CN104086246A (en) * 2014-07-27 2014-10-08 安徽科技学院 Method for producing iron-rich organic fertilizer by utilizing waste tea residues
CN104086246B (en) * 2014-07-27 2016-05-04 安徽科技学院 A kind of method of utilizing discarded tea grounds to produce rich iron fertilizer
CN111304662A (en) * 2020-04-10 2020-06-19 湖南淳湘农林科技有限公司 Preparation method of tea seed cake cleaning agent
CN112608182A (en) * 2020-12-17 2021-04-06 江苏农林职业技术学院 Formula and preparation method of tea byproduct fermented fertilizer

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RE Patent lapsed

Owner name: RYHSHINE INDUSTRIAL CORP.

Effective date: 19940131