AU767499B2 - Single-wall carbon nanotubes for hydrogen storage or superbundle formation - Google Patents
Single-wall carbon nanotubes for hydrogen storage or superbundle formation Download PDFInfo
- Publication number
- AU767499B2 AU767499B2 AU43139/01A AU4313901A AU767499B2 AU 767499 B2 AU767499 B2 AU 767499B2 AU 43139/01 A AU43139/01 A AU 43139/01A AU 4313901 A AU4313901 A AU 4313901A AU 767499 B2 AU767499 B2 AU 767499B2
- Authority
- AU
- Australia
- Prior art keywords
- swnt
- swnts
- hydrogen
- superbundle
- suspension
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 239000002109 single walled nanotube Substances 0.000 title claims description 70
- 229910052739 hydrogen Inorganic materials 0.000 title claims description 69
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title claims description 66
- 239000001257 hydrogen Substances 0.000 title claims description 66
- 238000003860 storage Methods 0.000 title claims description 9
- 230000015572 biosynthetic process Effects 0.000 title description 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 90
- 238000000034 method Methods 0.000 claims description 33
- 239000000463 material Substances 0.000 claims description 32
- 229910052751 metal Inorganic materials 0.000 claims description 11
- 239000002184 metal Substances 0.000 claims description 11
- 239000002904 solvent Substances 0.000 claims description 10
- 239000000725 suspension Substances 0.000 claims description 9
- 239000000758 substrate Substances 0.000 claims description 7
- 238000012545 processing Methods 0.000 claims description 6
- 238000005054 agglomeration Methods 0.000 claims description 5
- 230000002776 aggregation Effects 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- 238000007872 degassing Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000523 sample Substances 0.000 description 34
- 238000001179 sorption measurement Methods 0.000 description 25
- 238000003795 desorption Methods 0.000 description 19
- 238000007254 oxidation reaction Methods 0.000 description 18
- 238000010992 reflux Methods 0.000 description 18
- 239000002071 nanotube Substances 0.000 description 16
- 230000003647 oxidation Effects 0.000 description 16
- 229910002804 graphite Inorganic materials 0.000 description 13
- 239000010439 graphite Substances 0.000 description 13
- 238000001069 Raman spectroscopy Methods 0.000 description 12
- 238000000746 purification Methods 0.000 description 12
- 239000004071 soot Substances 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 238000001237 Raman spectrum Methods 0.000 description 11
- 229910052799 carbon Inorganic materials 0.000 description 11
- 230000005540 biological transmission Effects 0.000 description 10
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- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 7
- 238000003917 TEM image Methods 0.000 description 7
- 229910002091 carbon monoxide Inorganic materials 0.000 description 7
- 229910017604 nitric acid Inorganic materials 0.000 description 7
- 238000001228 spectrum Methods 0.000 description 7
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 6
- 238000002474 experimental method Methods 0.000 description 5
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- 230000002441 reversible effect Effects 0.000 description 5
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- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 4
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- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000003575 carbonaceous material Substances 0.000 description 3
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- 150000002739 metals Chemical class 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 238000004375 physisorption Methods 0.000 description 3
- 229910052697 platinum Inorganic materials 0.000 description 3
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- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000013019 agitation Methods 0.000 description 2
- 229910052786 argon Inorganic materials 0.000 description 2
- 239000002041 carbon nanotube Substances 0.000 description 2
- 229910021393 carbon nanotube Inorganic materials 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
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- 125000000524 functional group Chemical group 0.000 description 2
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- 229930195733 hydrocarbon Natural products 0.000 description 2
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- 238000004519 manufacturing process Methods 0.000 description 2
- 239000002082 metal nanoparticle Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229910052759 nickel Inorganic materials 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- -1 polytetrafluoroethylene Polymers 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
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- 239000013014 purified material Substances 0.000 description 2
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- 239000010453 quartz Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 238000004611 spectroscopical analysis Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 238000010306 acid treatment Methods 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 229910003481 amorphous carbon Inorganic materials 0.000 description 1
- 238000000137 annealing Methods 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000004323 axial length Effects 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
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- 239000013078 crystal Substances 0.000 description 1
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- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000009616 inductively coupled plasma Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000000223 laser vaporisation method Methods 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002121 nanofiber Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000002455 polarised Raman spectroscopy Methods 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
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- 229910052710 silicon Inorganic materials 0.000 description 1
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- 229910052709 silver Inorganic materials 0.000 description 1
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- 238000004528 spin coating Methods 0.000 description 1
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- 239000013077 target material Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000004627 transmission electron microscopy Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/0005—Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes
- C01B3/001—Reversible uptake of hydrogen by an appropriate medium, i.e. based on physical or chemical sorption phenomena or on reversible chemical reactions, e.g. for hydrogen storage purposes ; Reversible gettering of hydrogen; Reversible uptake of hydrogen by electrodes characterised by the uptaking medium; Treatment thereof
- C01B3/0021—Carbon, e.g. active carbon, carbon nanotubes, fullerenes; Treatment thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/158—Carbon nanotubes
- C01B32/168—After-treatment
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/158—Carbon nanotubes
- C01B32/168—After-treatment
- C01B32/174—Derivatisation; Solubilisation; Dispersion in solvents
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/32—Hydrogen storage
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US17707500P | 2000-01-19 | 2000-01-19 | |
US60/177075 | 2000-01-19 | ||
PCT/US2001/001698 WO2001053199A2 (fr) | 2000-01-19 | 2001-01-17 | Nanotubes de carbone a paroi simple pour stockage de l'hydrogene ou formation de superamas |
Publications (2)
Publication Number | Publication Date |
---|---|
AU4313901A AU4313901A (en) | 2001-07-31 |
AU767499B2 true AU767499B2 (en) | 2003-11-13 |
Family
ID=22647080
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AU43139/01A Ceased AU767499B2 (en) | 2000-01-19 | 2001-01-17 | Single-wall carbon nanotubes for hydrogen storage or superbundle formation |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP1248745A2 (fr) |
JP (1) | JP2003520178A (fr) |
AU (1) | AU767499B2 (fr) |
WO (1) | WO2001053199A2 (fr) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4972833B2 (ja) * | 2001-08-13 | 2012-07-11 | ソニー株式会社 | カーボンナノチューブの精製及び整列方法 |
WO2004113222A1 (fr) * | 2003-06-17 | 2004-12-29 | Future Camp Gmbh | Procede pour stocker de maniere reversible de l'hydrogene atomique sur/dans un micromateriau et/ou un nanomateriau carbone, et dispositif de stockage d'hydrogene |
TWI272245B (en) * | 2005-12-02 | 2007-02-01 | Hon Hai Prec Ind Co Ltd | A method for making carbon nanotube device |
US8246874B2 (en) | 2005-12-02 | 2012-08-21 | Tsinghua University | Method for making carbon nanotube-based device |
CN100500556C (zh) | 2005-12-16 | 2009-06-17 | 清华大学 | 碳纳米管丝及其制作方法 |
JP5330034B2 (ja) * | 2008-03-13 | 2013-10-30 | 国立大学法人東北大学 | カーボンナノチューブの評価方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH06228824A (ja) * | 1993-02-01 | 1994-08-16 | Nec Corp | カーボン・ナノチューブの精製法 |
JPH10120409A (ja) * | 1996-10-17 | 1998-05-12 | Toyo Tanso Kk | 単層ナノチューブの分離・精製方法及び金属内包ナノカプセルの分離・精製方法 |
WO1998039250A1 (fr) * | 1997-03-07 | 1998-09-11 | William Marsh Rice University | Fibres de carbone produites a partir de nanotubes en carbone a paroi simple |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3049019B2 (ja) * | 1998-09-11 | 2000-06-05 | 双葉電子工業株式会社 | 単層カーボンナノチューブの皮膜を形成する方法及びその方法により皮膜を形成された単層カーボンナノチューブ |
KR100364095B1 (ko) * | 1999-06-15 | 2002-12-12 | 일진나노텍 주식회사 | 탄소나노튜브의 대량 정제 방법 |
-
2001
- 2001-01-17 JP JP2001553214A patent/JP2003520178A/ja active Pending
- 2001-01-17 WO PCT/US2001/001698 patent/WO2001053199A2/fr not_active Application Discontinuation
- 2001-01-17 AU AU43139/01A patent/AU767499B2/en not_active Ceased
- 2001-01-17 EP EP01916071A patent/EP1248745A2/fr not_active Withdrawn
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH06228824A (ja) * | 1993-02-01 | 1994-08-16 | Nec Corp | カーボン・ナノチューブの精製法 |
JPH10120409A (ja) * | 1996-10-17 | 1998-05-12 | Toyo Tanso Kk | 単層ナノチューブの分離・精製方法及び金属内包ナノカプセルの分離・精製方法 |
WO1998039250A1 (fr) * | 1997-03-07 | 1998-09-11 | William Marsh Rice University | Fibres de carbone produites a partir de nanotubes en carbone a paroi simple |
Also Published As
Publication number | Publication date |
---|---|
AU4313901A (en) | 2001-07-31 |
JP2003520178A (ja) | 2003-07-02 |
WO2001053199A3 (fr) | 2002-01-17 |
WO2001053199A2 (fr) | 2001-07-26 |
EP1248745A2 (fr) | 2002-10-16 |
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Legal Events
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FGA | Letters patent sealed or granted (standard patent) |