AU744181B2 - Clear or translucent aqueous fabric softener compositions containing high electrolyte content and optional phase stabilizer - Google Patents

Clear or translucent aqueous fabric softener compositions containing high electrolyte content and optional phase stabilizer Download PDF

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Publication number
AU744181B2
AU744181B2 AU17984/99A AU1798499A AU744181B2 AU 744181 B2 AU744181 B2 AU 744181B2 AU 17984/99 A AU17984/99 A AU 17984/99A AU 1798499 A AU1798499 A AU 1798499A AU 744181 B2 AU744181 B2 AU 744181B2
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AU
Australia
Prior art keywords
alkyl
group
softener
composition
formula
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
AU17984/99A
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English (en)
Other versions
AU1798499A (en
Inventor
Ellen Schmidt Baker
Rebecca Gayl Baker
Marc Johan Declercq
Hugo Jean-Marie Demeyere
Dean Larry Duval
Gayle Marie Frankenbach
Ryan Matthew Heiden
Charles Albert Hensley
Brent Alan Kolb
Ruth Anne Murphy
Masae Nogami
Ronald Edward Pegoli
John Henry Shaw Jr.
Toan Trinh
Errol Hoffman Wahl
Michael R. Weaver
Ronghui Wu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Procter and Gamble Co
Original Assignee
Procter and Gamble Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Procter and Gamble Co filed Critical Procter and Gamble Co
Publication of AU1798499A publication Critical patent/AU1798499A/en
Application granted granted Critical
Publication of AU744181B2 publication Critical patent/AU744181B2/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/046Salts
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38Cationic compounds
    • C11D1/62Quaternary ammonium compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38Cationic compounds
    • C11D1/645Mixtures of compounds all of which are cationic
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/835Mixtures of non-ionic with cationic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/0005Other compounding ingredients characterised by their effect
    • C11D3/001Softening compositions
    • C11D3/0015Softening compositions liquid
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2041Dihydric alcohols
    • C11D3/2044Dihydric alcohols linear
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2041Dihydric alcohols
    • C11D3/2048Dihydric alcohols branched
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2093Esters; Carbonates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/34Organic compounds containing sulfur
    • C11D3/3418Toluene -, xylene -, cumene -, benzene - or naphthalene sulfonates or sulfates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/43Solvents
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/16Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
    • C22F1/18High-melting or refractory metals or alloys based thereon
    • C22F1/183High-melting or refractory metals or alloys based thereon of titanium or alloys based thereon
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/34Sputtering
    • C23C14/3407Cathode assembly for sputtering apparatus, e.g. Target
    • C23C14/3414Metallurgical or chemical aspects of target preparation, e.g. casting, powder metallurgy
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38Cationic compounds
    • C11D1/42Amino alcohols or amino ethers
    • C11D1/44Ethers of polyoxyalkylenes with amino alcohols; Condensation products of epoxyalkanes with amines
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38Cationic compounds
    • C11D1/52Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
    • C11D1/526Carboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 are polyalkoxylated
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38Cationic compounds
    • C11D1/58Heterocyclic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/72Ethers of polyoxyalkylene glycols
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/74Carboxylates or sulfonates esters of polyoxyalkylene glycols
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/75Amino oxides
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
AU17984/99A 1997-11-24 1998-11-24 Clear or translucent aqueous fabric softener compositions containing high electrolyte content and optional phase stabilizer Ceased AU744181B2 (en)

Applications Claiming Priority (13)

Application Number Priority Date Filing Date Title
US6642497P 1997-11-24 1997-11-24
US60/066424 1997-11-24
US7656498P 1998-03-02 1998-03-02
US60/076564 1998-03-02
US9845598P 1998-08-31 1998-08-31
US9854598P 1998-08-31 1998-08-31
US9851498P 1998-08-31 1998-08-31
US9845098P 1998-08-31 1998-08-31
US60/098455 1998-08-31
US60/098514 1998-08-31
US60/098545 1998-08-31
US60/098450 1998-08-31
PCT/US1998/025079 WO1999027050A1 (en) 1997-11-24 1998-11-24 Clear or translucent aqueous fabric softener compositions containing high electrolyte content and optional phase stabilizer

Publications (2)

Publication Number Publication Date
AU1798499A AU1798499A (en) 1999-06-15
AU744181B2 true AU744181B2 (en) 2002-02-14

Family

ID=27556957

Family Applications (1)

Application Number Title Priority Date Filing Date
AU17984/99A Ceased AU744181B2 (en) 1997-11-24 1998-11-24 Clear or translucent aqueous fabric softener compositions containing high electrolyte content and optional phase stabilizer

Country Status (14)

Country Link
EP (1) EP1036147A1 (zh)
JP (3) JP3866035B2 (zh)
KR (1) KR20010032434A (zh)
CN (1) CN1297474A (zh)
AR (1) AR017667A1 (zh)
AU (1) AU744181B2 (zh)
BR (1) BR9815323A (zh)
CA (1) CA2310612A1 (zh)
CZ (1) CZ20001814A3 (zh)
ID (1) ID28312A (zh)
MX (1) MXPA00008622A (zh)
PE (1) PE132599A1 (zh)
TR (1) TR200001470T2 (zh)
WO (1) WO1999027050A1 (zh)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6884767B1 (en) 1999-07-06 2005-04-26 The Procter & Gamble Company Clear or translucent aqueous polyquaternary ammonium fabric softener compositions containing low solvent
AU5912700A (en) * 1999-07-06 2001-01-22 Procter & Gamble Company, The Clear or translucent aqueous polyquaternary ammonium fabric softener compositions containing low solvent
DE19937987A1 (de) * 1999-08-11 2001-02-15 Drom Fragrances Internat Kg Zubereitung, insbesondere für WC-Erfrischer
HUP0204338A2 (en) * 1999-09-02 2003-04-28 Colgate Palmolive Co Fabric care composition containing polycarboxylate polymer and compound derived from urea
JP4024438B2 (ja) * 1999-11-01 2007-12-19 花王株式会社 第4級アンモニウム塩組成物
DE60120567T2 (de) 2000-01-19 2007-06-06 Kao Corporation Weichmacherzusammensetzung für die textilausrüstung
ATE332955T1 (de) * 2000-05-24 2006-08-15 Procter & Gamble Gewebeweichmacherzusammensetzung mit geruchskontrollmittel
DE10029027A1 (de) * 2000-06-13 2001-12-20 Basf Ag Verwendung alkoxilierter Polyvinylamine zur Modifizierung von Oberflächen
GB0014891D0 (en) 2000-06-16 2000-08-09 Unilever Plc Fabric softening compositions
WO2002031094A2 (en) * 2000-10-06 2002-04-18 Dow Global Technologies Inc. Clear softening formulations including alkoxylated additives
US20020187911A1 (en) * 2001-03-05 2002-12-12 Goldschmist Chemical Company Viscosity and softening enhancement by low-solids rinse cycle fabric softeners based on quaternary ammonium compounds and amine ethoxylates
EP1239024B1 (en) 2001-03-08 2007-11-21 Kao Corporation Softener composition
US6770617B2 (en) 2001-04-11 2004-08-03 Kao Corporation Softener composition
DE10119923A1 (de) * 2001-04-23 2002-10-24 Henkel Kgaa Mehrphasiges Konditioniermittel
DE10120176A1 (de) * 2001-04-24 2002-11-07 Henkel Kgaa Klare Weichspüler
WO2002101773A1 (en) 2001-05-11 2002-12-19 Mitsubishi Chemical Corporation Electrolytic solution for electrolytic capacitor and electrolytic capacitor using it
JP2005500444A (ja) * 2001-08-16 2005-01-06 ザ プロクター アンド ギャンブル カンパニー アルキレンオキシド置換されたカチオン電荷増強剤を含む透明な布地コンディショナー
US7954190B2 (en) * 2003-06-19 2011-06-07 The Procter & Gamble Company Process for increasing liquid extraction from fabrics
JP4579055B2 (ja) * 2005-06-01 2010-11-10 花王株式会社 透明又は半透明の液体柔軟剤組成物
JP4980032B2 (ja) * 2006-11-13 2012-07-18 花王株式会社 繊維製品処理剤
WO2008072780A1 (ja) 2006-12-12 2008-06-19 Kao Corporation 液体柔軟剤組成物あるいは透明又は半透明の液体柔軟剤組成物
DE102007056936A1 (de) 2007-11-23 2009-05-28 Henkel Ag & Co. Kgaa Biozides Textilbehandlungsmittel
EP2847307B1 (en) * 2012-05-07 2016-04-06 Evonik Degussa GmbH Fabric softener active composition and method for making it
MX2017017029A (es) * 2015-06-30 2018-05-17 Gillette Co Llc Miembro lubricante para cartuchos de rasuradora.
EP3339409B1 (en) * 2016-12-22 2020-04-15 The Procter & Gamble Company Fabric softener composition having improved freeze thaw stability
US10676694B2 (en) * 2016-12-22 2020-06-09 The Procter & Gamble Company Fabric softener composition having improved detergent scavenger compatibility
EP3404086B1 (en) * 2017-05-18 2020-04-08 The Procter & Gamble Company Fabric softener composition
CN116507707A (zh) * 2020-11-18 2023-07-28 联合利华知识产权控股有限公司 织物调理剂

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63223098A (ja) * 1987-03-12 1988-09-16 ライオン株式会社 柔軟剤組成物
JPH10168496A (ja) * 1996-12-11 1998-06-23 Lion Corp 粒状ノニオン洗剤組成物及びその製造方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0687291B2 (en) * 1993-03-01 2005-08-24 The Procter & Gamble Company Concentrated biodegradable quaternary ammonium fabric softener compositions and compounds containing intermediate iodine value unsaturated fatty acid chains
US5525245A (en) * 1994-12-21 1996-06-11 Colgate-Palmolive Company Clear, concentrated liquid fabric softener compositions
EP0923631A2 (en) * 1996-08-30 1999-06-23 The Procter & Gamble Company Concentrated premix with reduced flammability for forming fabric softening composition
US5747108A (en) * 1997-03-19 1998-05-05 Colgate-Palmolive Co. Super-concentrated liquid rinse cycle fabric softening composition

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63223098A (ja) * 1987-03-12 1988-09-16 ライオン株式会社 柔軟剤組成物
JPH10168496A (ja) * 1996-12-11 1998-06-23 Lion Corp 粒状ノニオン洗剤組成物及びその製造方法

Also Published As

Publication number Publication date
PE132599A1 (es) 2000-01-20
JP2006200123A (ja) 2006-08-03
ID28312A (id) 2001-05-10
JP4402060B2 (ja) 2010-01-20
JP2001524616A (ja) 2001-12-04
JP4242393B2 (ja) 2009-03-25
WO1999027050A1 (en) 1999-06-03
KR20010032434A (ko) 2001-04-25
AR017667A1 (es) 2001-09-12
JP2006200122A (ja) 2006-08-03
MXPA00008622A (es) 2001-03-01
CN1297474A (zh) 2001-05-30
EP1036147A1 (en) 2000-09-20
TR200001470T2 (tr) 2001-03-21
CZ20001814A3 (cs) 2001-10-17
BR9815323A (pt) 2001-10-09
CA2310612A1 (en) 1999-06-03
AU1798499A (en) 1999-06-15
JP3866035B2 (ja) 2007-01-10

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