AU2023213772A1 - Method for purifying sugars in pre-hydrolysis liquor of hardwood pulping - Google Patents
Method for purifying sugars in pre-hydrolysis liquor of hardwood pulping Download PDFInfo
- Publication number
- AU2023213772A1 AU2023213772A1 AU2023213772A AU2023213772A AU2023213772A1 AU 2023213772 A1 AU2023213772 A1 AU 2023213772A1 AU 2023213772 A AU2023213772 A AU 2023213772A AU 2023213772 A AU2023213772 A AU 2023213772A AU 2023213772 A1 AU2023213772 A1 AU 2023213772A1
- Authority
- AU
- Australia
- Prior art keywords
- hydrolysis liquor
- lignin
- hydrolysis
- liquor
- pulping
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000006460 hydrolysis reaction Methods 0.000 title claims description 77
- 230000007062 hydrolysis Effects 0.000 title claims description 76
- 238000000034 method Methods 0.000 title claims description 52
- 238000004537 pulping Methods 0.000 title claims description 28
- 235000000346 sugar Nutrition 0.000 title claims description 28
- 239000011121 hardwood Substances 0.000 title claims description 17
- 150000008163 sugars Chemical class 0.000 title claims description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 38
- SRBFZHDQGSBBOR-IOVATXLUSA-N D-xylopyranose Chemical compound O[C@@H]1COC(O)[C@H](O)[C@H]1O SRBFZHDQGSBBOR-IOVATXLUSA-N 0.000 claims description 32
- 102000004190 Enzymes Human genes 0.000 claims description 23
- 108090000790 Enzymes Proteins 0.000 claims description 23
- 108010059896 Manganese peroxidase Proteins 0.000 claims description 17
- PYMYPHUHKUWMLA-UHFFFAOYSA-N arabinose Natural products OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 claims description 16
- SRBFZHDQGSBBOR-UHFFFAOYSA-N beta-D-Pyranose-Lyxose Natural products OC1COC(O)C(O)C1O SRBFZHDQGSBBOR-UHFFFAOYSA-N 0.000 claims description 16
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 12
- 239000003463 adsorbent Substances 0.000 claims description 12
- 238000000926 separation method Methods 0.000 claims description 12
- 241000219000 Populus Species 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 10
- 238000000746 purification Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 9
- 240000007472 Leucaena leucocephala Species 0.000 claims description 7
- 235000010643 Leucaena leucocephala Nutrition 0.000 claims description 7
- 238000001179 sorption measurement Methods 0.000 claims description 7
- 229920001221 xylan Polymers 0.000 claims description 6
- 150000004823 xylans Chemical class 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 5
- 230000035484 reaction time Effects 0.000 claims description 5
- 244000166124 Eucalyptus globulus Species 0.000 claims description 3
- 239000003814 drug Substances 0.000 claims description 3
- 229940079593 drug Drugs 0.000 claims description 3
- 229910021536 Zeolite Inorganic materials 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 2
- 235000013373 food additive Nutrition 0.000 claims description 2
- 239000002778 food additive Substances 0.000 claims description 2
- 230000036541 health Effects 0.000 claims description 2
- 239000011347 resin Substances 0.000 claims description 2
- 229920005989 resin Polymers 0.000 claims description 2
- 239000010457 zeolite Substances 0.000 claims description 2
- 238000010907 mechanical stirring Methods 0.000 claims 1
- 239000002808 molecular sieve Substances 0.000 claims 1
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims 1
- 229920005610 lignin Polymers 0.000 description 49
- 238000006243 chemical reaction Methods 0.000 description 18
- 230000000694 effects Effects 0.000 description 11
- 239000011572 manganese Substances 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 8
- 239000002994 raw material Substances 0.000 description 8
- 108010029541 Laccase Proteins 0.000 description 7
- 238000006731 degradation reaction Methods 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 229920002488 Hemicellulose Polymers 0.000 description 5
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 5
- 102000003992 Peroxidases Human genes 0.000 description 5
- 230000015556 catabolic process Effects 0.000 description 5
- 239000000835 fiber Substances 0.000 description 5
- 229910052748 manganese Inorganic materials 0.000 description 5
- 108040007629 peroxidase activity proteins Proteins 0.000 description 5
- 238000006116 polymerization reaction Methods 0.000 description 5
- 238000011084 recovery Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 238000010335 hydrothermal treatment Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000002023 wood Substances 0.000 description 3
- 239000002028 Biomass Substances 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 108010001336 Horseradish Peroxidase Proteins 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000010170 biological method Methods 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 description 2
- 229910000357 manganese(II) sulfate Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- NOEGNKMFWQHSLB-UHFFFAOYSA-N 5-hydroxymethylfurfural Chemical compound OCC1=CC=C(C=O)O1 NOEGNKMFWQHSLB-UHFFFAOYSA-N 0.000 description 1
- 229920000875 Dissolving pulp Polymers 0.000 description 1
- 101710121765 Endo-1,4-beta-xylanase Proteins 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006065 biodegradation reaction Methods 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 239000007857 degradation product Substances 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 239000008394 flocculating agent Substances 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- RJGBSYZFOCAGQY-UHFFFAOYSA-N hydroxymethylfurfural Natural products COC1=CC=C(C=O)O1 RJGBSYZFOCAGQY-UHFFFAOYSA-N 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 238000000053 physical method Methods 0.000 description 1
- 229920002401 polyacrylamide Polymers 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000000811 xylitol Substances 0.000 description 1
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 1
- 229960002675 xylitol Drugs 0.000 description 1
- 235000010447 xylitol Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/02—Monosaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/70—Carbohydrates; Sugars; Derivatives thereof
- A61K31/7004—Monosaccharides having only carbon, hydrogen and oxygen atoms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/70—Carbohydrates; Sugars; Derivatives thereof
- A61K31/715—Polysaccharides, i.e. having more than five saccharide radicals attached to each other by glycosidic linkages; Derivatives thereof, e.g. ethers, esters
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/04—Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Molecular Biology (AREA)
- Biochemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Microbiology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Genetics & Genomics (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Mycology (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Paper (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210088371.4 | 2022-01-25 | ||
| CN202210088371.4A CN114410707B (zh) | 2022-01-25 | 2022-01-25 | 一种纯化阔叶木制浆预水解液中糖分的方法 |
| PCT/CN2023/072917 WO2023143310A1 (zh) | 2022-01-25 | 2023-01-18 | 一种纯化阔叶木制浆预水解液中糖分的方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AU2023213772A1 true AU2023213772A1 (en) | 2023-09-07 |
Family
ID=81277927
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2023213772A Pending AU2023213772A1 (en) | 2022-01-25 | 2023-01-18 | Method for purifying sugars in pre-hydrolysis liquor of hardwood pulping |
Country Status (3)
| Country | Link |
|---|---|
| CN (1) | CN114410707B (zh) |
| AU (1) | AU2023213772A1 (zh) |
| WO (1) | WO2023143310A1 (zh) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114410707B (zh) * | 2022-01-25 | 2023-08-15 | 齐鲁工业大学 | 一种纯化阔叶木制浆预水解液中糖分的方法 |
| CN117491536B (zh) * | 2023-12-29 | 2024-03-12 | 中国林业科学研究院林产化学工业研究所 | 一种prc-apmp工艺制浆废水的微生物毒性物质鉴定方法 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI104835B (fi) * | 1997-01-14 | 2000-04-14 | Neste Chemicals Oy | Ligniinipohjaiset sideaineet lastulevyvalmistusta varten |
| JP3839940B2 (ja) * | 1997-11-26 | 2006-11-01 | 株式会社エス・ディー・エス バイオテック | 含金属処理剤による木材の処理方法およびその方法により処理された木材 |
| CN103429749B (zh) * | 2010-12-10 | 2016-12-14 | 诺维信公司 | 用于从含木素纤维素材料产生发酵产物的方法 |
| US20140302567A1 (en) * | 2011-10-14 | 2014-10-09 | The University Of Georgia Research Foundation, Inc | Methods and compositions using lignolytic enzymes and mediators to reduce and reform lignin contents in lignocellulosic biomass |
| CN104448159B (zh) * | 2013-11-26 | 2017-01-04 | 柳州爱格富食品科技股份有限公司 | 含有腐殖酸的高吸水树脂的制备方法 |
| CN103740787B (zh) * | 2014-01-17 | 2016-05-11 | 山东大学 | 一种利用阔叶木溶解浆预水解废液酶法生产低聚木糖的方法 |
| CN104894079B (zh) * | 2015-05-27 | 2019-01-04 | 华中科技大学 | 木质素降解液及制备方法以及用其降解木质素的方法 |
| WO2018233559A1 (en) * | 2017-06-20 | 2018-12-27 | Novozymes A/S | PROCESS FOR INCREASING THE PERCENTAGE OF HYDROLYSAT XYLOSE |
| CN107936143B (zh) * | 2017-11-24 | 2021-03-23 | 齐鲁工业大学 | 一种植物纤维原料水解液生物处理去除木素的方法 |
| CN108411044B (zh) * | 2018-04-04 | 2021-04-30 | 齐鲁工业大学 | 一种桉木热水预水解液中木糖的超声波辅助纯化方法 |
| CN109162135A (zh) * | 2018-09-13 | 2019-01-08 | 山东太阳纸业股份有限公司 | 一种利用阔叶木材生产溶解浆与低聚木糖的方法 |
| CN110042133B (zh) * | 2019-04-22 | 2021-06-04 | 齐鲁工业大学 | 一种生物酶协同物理化学法纯化制备杨木低聚木糖的方法 |
| CN110280217A (zh) * | 2019-06-24 | 2019-09-27 | 齐鲁工业大学 | 一种木素吸附剂、其制备方法及其应用 |
| CN110256608B (zh) * | 2019-06-24 | 2021-04-20 | 齐鲁工业大学 | 辣根过氧化物酶处理除去植物纤维预水解液中木素的方法 |
| CN110699403A (zh) * | 2019-11-13 | 2020-01-17 | 齐鲁工业大学 | 一种提升阔叶木制浆预水解液中低聚木糖纯化效率的方法 |
| CN114410707B (zh) * | 2022-01-25 | 2023-08-15 | 齐鲁工业大学 | 一种纯化阔叶木制浆预水解液中糖分的方法 |
-
2022
- 2022-01-25 CN CN202210088371.4A patent/CN114410707B/zh active Active
-
2023
- 2023-01-18 WO PCT/CN2023/072917 patent/WO2023143310A1/zh active Application Filing
- 2023-01-18 AU AU2023213772A patent/AU2023213772A1/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| CN114410707B (zh) | 2023-08-15 |
| WO2023143310A1 (zh) | 2023-08-03 |
| CN114410707A (zh) | 2022-04-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| DA3 | Amendments made section 104 |
Free format text: THE NATURE OF THE AMENDMENT IS: AMEND THE INVENTION TITLE TO READ METHOD FOR PURIFYING SUGARS IN PRE-HYDROLYSIS LIQUOR OF HARDWOOD PULPING |