AU2014101215A4 - dual beam spectrum calibration analyzer - Google Patents

dual beam spectrum calibration analyzer Download PDF

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Publication number
AU2014101215A4
AU2014101215A4 AU2014101215A AU2014101215A AU2014101215A4 AU 2014101215 A4 AU2014101215 A4 AU 2014101215A4 AU 2014101215 A AU2014101215 A AU 2014101215A AU 2014101215 A AU2014101215 A AU 2014101215A AU 2014101215 A4 AU2014101215 A4 AU 2014101215A4
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Australia
Prior art keywords
spectral separation
calibration
light source
separation device
absorption
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AU2014101215A
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Jiuzhou Yan
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CHENGDU ZHONGYUAN QIANYE TECHNOLOGY Co Ltd
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CHENGDU ZHONGYUAN QIANYE TECHNOLOGY CO Ltd
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Publication of AU2014101215A4 publication Critical patent/AU2014101215A4/en
Priority to GB201423240A priority patent/GB201423240D0/en
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  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

A dual beam spectrum calibration analyzer comprises: a light source device(1), a first spectral separation device(2), a second spectral separation device (3), a beam refraction device(4), a beam wavelength calibration device (5), a injector device(6), a beam absorption calibration device(7), a signal detection device(8), a signal analysis recording device(9); wherein beam refraction device(4) is connected with first spectral separation device(2) and second spectral separation device (3); beam wavelength calibration device (5) is located between beam refraction device(4) and injector device(6); the beam refraction device (4) is used to conduct intermittent absorption and shielding for specific beam that is generated by first spectral separation device(2) and second spectral separation device (3), the beam wavelength calibration device (5) is mainly used to implement wavelength calibration for the beam which is from the light source device(1) , to eliminate the error; the injector device (6) conduct the role of sample introduction and preliminary analysis with sample test; through standard calibration solution, the beam absorption calibration device(7) can implement absorption correction for the beam that pass through the injector device (6); then the signal detection device (8) carry out conversion and analysis of optical signal after beam attenuation, which has a better sensitivity with spectral changes, good linearity and low noise level; then signal analysis recording device (9) implement the preservation and recording of optical signals; wherein the light source device (1) utilize the combination light source of Nickel-hydrogen lamp and quartz low-pressure mercury lamp ,which have a series connection mode ; the first spectral separation device (2) comprise concave mirrors and the prisms, which have a combination of alternating permutations; the beam refraction device (4) contains the rotating six-sided prism. 1 /4 5 6 78 Figure 1

Description

1 DUAL BEAM SPECTRUM CALIBRATION ANALYZER FIELD OF THE INVENTION [0001] The present invention relates to the field of spectral calibration analysis, particularly involving dual beam spectrum calibration analyzer. GENERALBACKGROUND [0002]Spectral analysis is mainly used for correcting the emission spectrum analysis of the transitions between energy levels and absorption spectra of molecules, including the pure rotational spectrum of the vibration rotation spectrum band and electronic spectral bands. Pure rotational spectra of molecules are produced by molecular rotational transitions between energy levels, having a distribution in the far infrared band; the main observation is usually about absorption spectroscopy. Vibration - rotation spectra is produced by transitions between the different vibrational levels and the rotational levels, which have some dense lines, distributed in the near-infrared band. [0003]An electronic spectrum is produced by transitions with different levels of vibration and different rotation between different electronic states, which can be divided into a number of bands; the emission spectrums have a distribution in the visible or ultraviolet wavelength and can be observed. [0004]However, due to the absence of dipole moment in the non-polar molecules, rotational spectrum and vibration - rotation spectrum band do not exist, only polar molecules have such a spectral band. Therefore, the existing analytical device also has limitations for non-polar molecule spectroscopy; so it is necessary to make reasonable technical solutions for these problems to be addressed.
2 SUMMARY [0005]In order to overcome the deficiencies of prior devices, the present invention adopts the technical solution as follows. [0006]A dual beam spectrum calibration analyzer comprises: a light source device(1), a first spectral separation device(2), a second spectral separation device (3), a beam refraction device(4), a beam wavelength calibration device (5), a injector device(6), a beam absorption calibration device(7), a signal detection device(8), a signal analysis recording device(9); wherein beam refraction device(4) is connected with first spectral separation device(2) and second spectral separation device (3); beam wavelength calibration device (5) is located between beam refraction device(4) and injector device(6); the beam refraction device (4) is used to conduct intermittent absorption and shielding for specific beam that is generated by first spectral separation device(2) and second spectral separation device (3), the beam wavelength calibration device (5) is mainly used to implement wavelength calibration for the beam which is from the light source device(1) , to eliminate the error; the injector device (6) conduct the role of sample introduction and preliminary analysis with sample test; through standard calibration solution, the beam absorption calibration device(7) can implement absorption correction for the beam that pass through the injector device (6); then the signal detection device (8) carry out conversion and analysis of optical signal after beam attenuation, which has a better sensitivity with spectral changes, good linearity and low noise level; then signal analysis recording device (9) implement the preservation and recording of optical signals; wherein the light source device (1) utilize the combination light source of Nickel-hydrogen lamp and quartz low-pressure mercury lamp ,which have a series connection mode ; the first spectral separation device (2) comprise concave mirrors and the prisms, which have a combination of alternating permutations; the beam refraction device (4) contains the rotating six-sided prism.
3 [0007]The second spectral separation device (3) contains lens and gratings, the lens are in the front, the gratings are in the back. [0008]The beam wavelength calibration device (5) contains europium glass lens and molybdenum glass lens, which are alternately arranged in series. [0009]The signal detection device (8) involves photoelectric converter, wherein the cathode material of the photoelectric converter is gadolinium nitrate and technetium chloride composite material. [0010]Wherein the light source device (1) is mainly used for generating a light beam meet the testing requirements, the first spectral separation device (2) is mainly used for screening and separation of the beam wavelength to obtain a light beam Li for a particular target wavelength, and the second spectral separation device (3) is mainly used for screening and separation of the beam wavelength to obtain a particular target wavelength of the light beam L2. [0011]Compared with the prior art, the present invention has the advantages that: (1) Having a better sensitivity to spectral changes, good linearity, low noise level; (2) Able to absorb and block specific beam intermittently, providing analysis and detection precisely; (3) Having better detection performance and adaptation range with pure rotational spectrum, vibration rotation spectrum and electron spectroscopy.
4 BRIEF DESCRIPTION OF THE DRAWING [0012]Figure 1 is a schematic diagram of the present invention; List of reference characters: 1 light source device, 2 first spectral separation device, 3 second spectral separation device, 4 beam refraction device, 5 beam wavelength calibration device, 6 injector device, 7 beam absorption calibration device, 8 signal detection device, 9 signal analysis recording device. DETAILED DESCRIPTION OF PREFERRED EMBODIMENTS Embodiment 1 [0013]As shown in Fig. 1, a dual beam spectrum calibration analyzer comprises: a light source device(1), a first spectral separation device(2), a second spectral separation device (3), a beam refraction device(4), a beam wavelength calibration device (5), a injector device(6), a beam absorption calibration device(7), a signal detection device(8), a signal analysis recording device(9); wherein beam refraction device(4) is connected with first spectral separation device(2) and second spectral separation device (3); beam wavelength calibration device (5) is located between beam refraction device(4) and injector device(6); the beam refraction device (4) is used to conduct intermittent absorption and shielding for specific beam that is generated by first spectral separation device(2) and second spectral separation device (3), the beam wavelength calibration device (5) is mainly used to implement wavelength calibration for the beam which is from the light source device(1) , to eliminate the error; the injector device (6) conduct the role of sample introduction 5 and preliminary analysis with sample test; through standard calibration solution, the beam absorption calibration device(7) can implement absorption correction for the beam that pass through the injector device (6); then the signal detection device (8) carry out conversion and analysis of optical signal after beam attenuation, which has a better sensitivity with spectral changes, good linearity and low noise level; then signal analysis recording device (9) implement the preservation and recording of optical signals; wherein the light source device (1) utilize the combination light source of Nickel-hydrogen lamp and quartz low-pressure mercury lamp ,which have a series connection mode ; the first spectral separation device (2) comprise concave mirrors and the prisms, which have a combination of alternating permutations; the beam refraction device (4) contains the rotating six-sided prism. [0014]In the present invention, the second spectral separation device (3) contains lens and gratings, the lens are in the front, the gratings are in the back. [0015]In the present invention, the beam wavelength calibration device (5) contains europium glass lens and molybdenum glass lens, which are alternately arranged in series. Embodiment 2 [0016]A dual beam spectrum calibration analyzer comprises: a light source device(1), a first spectral separation device(2), a second spectral separation device (3), a beam refraction device(4), a beam wavelength calibration device (5), a injector device(6), a beam absorption calibration device(7), a signal detection device(8), a signal analysis recording device(9); wherein beam refraction device(4) is connected with first spectral separation device(2) and second spectral separation device (3); beam wavelength calibration device (5) is located between beam refraction device(4) and injector device(6); the beam refraction device (4) is used to conduct intermittent absorption and shielding for specific beam that is generated by first spectral 6 separation device(2) and second spectral separation device (3), the beam wavelength calibration device (5) is mainly used to implement wavelength calibration for the beam which is from the light source device(1) , to eliminate the error; the injector device (6) conduct the role of sample introduction and preliminary analysis with sample test; through standard calibration solution, the beam absorption calibration device(7) can implement absorption correction for the beam that pass through the injector device (6); then the signal detection device (8) carry out conversion and analysis of optical signal after beam attenuation, which has a better sensitivity with spectral changes, good linearity and low noise level; then signal analysis recording device (9) implement the preservation and recording of optical signals; wherein the light source device (1) utilize the combination light source of Nickel-hydrogen lamp and quartz low-pressure mercury lamp ,which have a series connection mode ; the first spectral separation device (2) comprise concave mirrors and the prisms, which have a combination of alternating permutations; the beam refraction device (4) contains the rotating six-sided prism. [0017]In the present invention, signal detection device (8) involves photoelectric converter, wherein the cathode material of the photoelectric converter is gadolinium nitrate and technetium chloride composite material.

Claims (3)

  1. 2. The dual beam spectrum calibration analyzer according to claim 1, wherein second spectral separation device (3) contains lens and gratings, the lens are in the front, the gratings are in the back.
  2. 3. The dual beam spectrum calibration analyzer according to claim 1, wherein beam wavelength calibration device (5) contains europium glass lens and molybdenum glass lens, which are alternately arranged in series.
  3. 4. The dual beam spectrum calibration analyzer according to claim 1, wherein signal detection device (8) involves photoelectric converter, wherein the cathode material of the photoelectric converter is gadolinium nitrate and technetium chloride composite material.
AU2014101215A 2014-05-28 2014-10-03 dual beam spectrum calibration analyzer Ceased AU2014101215A4 (en)

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AU2014101215A AU2014101215A4 (en) 2014-10-03 2014-10-03 dual beam spectrum calibration analyzer
GB201423240A GB201423240D0 (en) 2014-05-28 2014-12-29 Double wavelength spectroscopy detection analyzer

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113692524A (en) * 2019-03-27 2021-11-23 ams传感器新加坡私人有限公司 Self-calibrating spectral sensor module

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113692524A (en) * 2019-03-27 2021-11-23 ams传感器新加坡私人有限公司 Self-calibrating spectral sensor module

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