AU2001289978A1 - A multistep process for recovering betaine, erythritol, inositol, sucrose, mannitol, glycerol and amino acids from process solution using a weakly acid cationexchange resin - Google Patents

A multistep process for recovering betaine, erythritol, inositol, sucrose, mannitol, glycerol and amino acids from process solution using a weakly acid cationexchange resin

Info

Publication number
AU2001289978A1
AU2001289978A1 AU2001289978A AU8997801A AU2001289978A1 AU 2001289978 A1 AU2001289978 A1 AU 2001289978A1 AU 2001289978 A AU2001289978 A AU 2001289978A AU 8997801 A AU8997801 A AU 8997801A AU 2001289978 A1 AU2001289978 A1 AU 2001289978A1
Authority
AU
Australia
Prior art keywords
glycerol
erythritol
inositol
mannitol
sucrose
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2001289978A
Inventor
Heikki Heikkila
Jarmo Kuisma
Jari Lewandowski
Nina Mayra
Hannu Paananen
Vili Ravanko
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Finnfeeds Finland Ltd
Original Assignee
Finnfeeds Finland Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Finnfeeds Finland Ltd filed Critical Finnfeeds Finland Ltd
Publication of AU2001289978A1 publication Critical patent/AU2001289978A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B35/00—Extraction of sucrose from molasses
    • C13B35/02—Extraction of sucrose from molasses by chemical means
    • C13B35/06—Extraction of sucrose from molasses by chemical means using ion exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/04—Processes using organic exchangers
    • B01J39/07—Processes using organic exchangers in the weakly acidic form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J39/00—Cation exchange; Use of material as cation exchangers; Treatment of material for improving the cation exchange properties
    • B01J39/26—Cation exchangers for chromatographic processes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/28—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from natural products
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B20/00—Purification of sugar juices
    • C13B20/14—Purification of sugar juices using ion-exchange materials
    • C13B20/144—Purification of sugar juices using ion-exchange materials using only cationic ion-exchange material
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
    • C13B30/02—Crystallisation; Crystallising apparatus
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K13/00—Sugars not otherwise provided for in this class
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Biochemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

The invention relates to a method comprising a multistep process for recovering betaine, erythritol, inositol, sucrose, mannitol, glycerol and amino acids from corresponding starting materials. The invention comprises the use of a weakly acid cation exchange resin in chromatographic column in the multistep process. The starting materials are especially beet molasses, betaine molasses, syrups, thick juices, raw juices, corn steep cane based solutions and glycerol.
AU2001289978A 2000-09-29 2001-09-28 A multistep process for recovering betaine, erythritol, inositol, sucrose, mannitol, glycerol and amino acids from process solution using a weakly acid cationexchange resin Abandoned AU2001289978A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FI20002150 2000-09-29
FI20002150A FI20002150A (en) 2000-09-29 2000-09-29 Procedure for recycling products from process solutions
PCT/FI2001/000849 WO2002027037A1 (en) 2000-09-29 2001-09-28 A multistep process for recovering betaine, erythritol, inositol, sucrose, mannitol, glycerol and amino acids from a process solution using a weakly acid cation exchange resin

Publications (1)

Publication Number Publication Date
AU2001289978A1 true AU2001289978A1 (en) 2002-04-08

Family

ID=8559194

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2001289978A Abandoned AU2001289978A1 (en) 2000-09-29 2001-09-28 A multistep process for recovering betaine, erythritol, inositol, sucrose, mannitol, glycerol and amino acids from process solution using a weakly acid cationexchange resin

Country Status (11)

Country Link
US (1) US6770757B2 (en)
EP (1) EP1328664B1 (en)
JP (1) JP4973970B2 (en)
AT (1) ATE329062T1 (en)
AU (1) AU2001289978A1 (en)
DE (1) DE60120449T2 (en)
DK (1) DK1328664T3 (en)
ES (1) ES2266257T3 (en)
FI (1) FI20002150A (en)
PT (1) PT1328664E (en)
WO (1) WO2002027037A1 (en)

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US6663780B2 (en) * 1993-01-26 2003-12-16 Danisco Finland Oy Method for the fractionation of molasses
US20060106226A1 (en) * 1998-02-26 2006-05-18 Aminopath Labs, Llc And A Patent License Agreement Isolation of amino acids and related isolates
BE1014613A3 (en) * 2002-02-11 2004-01-13 Amylum Europe Nv Process for the preparation of alkali and heat stable polyols.
FI20020592A (en) 2002-03-27 2003-09-28 Danisco Sweeteners Oy Method for separating sugars, sugar alcohols, carbohydrates and mixtures thereof from solutions containing them
FI20021251A0 (en) 2002-06-26 2002-06-26 Finnfeeds Finland Oy Method for the recovery of betaine
WO2004076021A1 (en) * 2003-02-25 2004-09-10 Finnfeeds Finland Oy A simulated moving bed system and process
US20050061744A1 (en) * 2003-07-16 2005-03-24 Kearney Michael M. Method for the recovery of acids from hydrometallurgy process solutions
US7077953B2 (en) * 2003-09-11 2006-07-18 Harris Group, Inc. Nanofilter system and method of use
EP1781116A4 (en) * 2004-06-04 2009-07-29 Horizon Science Pty Ltd Natural sweetener
US8021697B2 (en) 2005-06-03 2011-09-20 Horizon Science Pty. Ltd. Substances having body mass redistribution properties
US7544293B2 (en) 2005-09-26 2009-06-09 Semba Inc. Valve and process for interrupted continuous flow chromatography
US8864995B2 (en) * 2006-01-10 2014-10-21 Dupont Nutrition Biosciences Aps Method for separating betaine
US20070161784A1 (en) * 2006-01-11 2007-07-12 Aminopath Labs, Llc Methods and products of amino acid isolation
WO2007105790A1 (en) * 2006-03-15 2007-09-20 Kyowa Hakko Kogyo Co., Ltd. Method for purification of amino acid
GB2437516A (en) * 2006-04-26 2007-10-31 Bai Leng Method and apparatus for purifying glycerine using filter membranes and a deionisation means
CN101479292A (en) * 2006-06-28 2009-07-08 协和发酵生化株式会社 Method for purification of oligopeptide
US7790040B2 (en) 2006-08-30 2010-09-07 Semba Biosciences, Inc. Continuous isocratic affinity chromatography
US8807164B2 (en) * 2006-08-30 2014-08-19 Semba Biosciences, Inc. Valve module and methods for simulated moving bed chromatography
CN104323268A (en) * 2006-09-19 2015-02-04 视界科技有限公司 Extracts derived from sugar cane and a process for their manufacture
JP5028125B2 (en) * 2007-03-30 2012-09-19 株式会社日立ハイテクノロジーズ Amino acid analysis method and amino acid analysis system
JP5753101B2 (en) * 2009-02-25 2015-07-22 デュポン ニュートリション バイオサイエンシーズ エーピーエス Separation method
WO2012106761A1 (en) 2011-02-08 2012-08-16 Horizon Science Pty Ltd Sugar extracts
JP6215833B2 (en) * 2011-11-15 2017-10-18 ティエンセ スイケルラフィナデリーイェー ナームローゼ フェンノートシャップＴｉｅｎｓｅ Ｓｕｉｋｅｒｒａｆｆｉｎａｄｅｒｉｊ ｎ．ｖ． How to recover betaine from molasses
US20150201660A1 (en) 2012-08-28 2015-07-23 The Product Makers (Austrilia) Pty Ltd Extraction Method
AU2014306366B9 (en) 2013-08-16 2020-03-26 Poly Gain Pte Ltd Sugar cane derived extracts and methods of treatment
CN112114050B (en) * 2019-06-19 2022-12-02 北京华医神农医药科技有限公司 Quality detection method of cistanche oral liquid
RU2765487C1 (en) * 2020-10-01 2022-01-31 Федеральное государственное бюджетное образовательное учреждение высшего образования "Кубанский государственный технологический университет" (ФГБОУ ВО "КубГТУ") Method for obtaining betaine and sucrose out of molasses

Family Cites Families (15)

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Publication number Priority date Publication date Assignee Title
DE2362211C3 (en) * 1973-12-14 1978-05-11 Sueddeutsche Zucker Ag, 6800 Mannheim Process for processing molasses
US4358322A (en) 1976-05-27 1982-11-09 Uop Inc. Process for separating a ketose from an aldose by selective adsorption
US4359430A (en) * 1980-02-29 1982-11-16 Suomen Sokeri Osakeyhtio Betaine recovery process
US4333770A (en) 1980-09-08 1982-06-08 Uop Inc. Extraction of sucrose from molasses
US4405378A (en) 1981-02-17 1983-09-20 Uop Inc. Extraction of sucrose
US4405377A (en) 1982-02-10 1983-09-20 Uop Inc. Process for the separation of monosaccharides
FI86416C (en) 1988-06-09 1992-08-25 Suomen Sokeri Oy Procedure for extracting betaine from molasses
FI96225C (en) * 1993-01-26 1996-05-27 Cultor Oy Process for fractionation of molasses
JP3352859B2 (en) * 1995-10-18 2002-12-03 オルガノ株式会社 Desalting method of sucrose solution using ion exchange resin
JP3561351B2 (en) * 1995-11-02 2004-09-02 積水化学工業株式会社 Sugar analysis method
US6224776B1 (en) * 1996-05-24 2001-05-01 Cultor Corporation Method for fractionating a solution
FI102962B (en) 1996-06-24 1999-03-31 Xyrofin Oy Process for the preparation of xylitol
FI105048B (en) 1997-05-22 2000-05-31 Xyrofin Oy Process for the preparation of isomaltulose and other products
JP3599306B2 (en) * 1998-01-05 2004-12-08 オルガノ株式会社 Sucrose liquid purification method
CN1081191C (en) * 1999-03-22 2002-03-20 华东理工大学 Method for separating D-ribose from fermentation liquor

Also Published As

Publication number Publication date
JP4973970B2 (en) 2012-07-11
US6770757B2 (en) 2004-08-03
EP1328664A1 (en) 2003-07-23
DE60120449T2 (en) 2007-05-31
EP1328664B1 (en) 2006-06-07
DK1328664T3 (en) 2006-10-09
PT1328664E (en) 2006-09-29
US20020169311A1 (en) 2002-11-14
DE60120449D1 (en) 2006-07-20
ES2266257T3 (en) 2007-03-01
ATE329062T1 (en) 2006-06-15
WO2002027037A1 (en) 2002-04-04
JP2004509932A (en) 2004-04-02
FI20002150A (en) 2002-03-30
FI20002150A0 (en) 2000-09-29

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