ATE129753T1 - METHOD FOR PICKLING AND PASSIVING STAINLESS STEEL WITHOUT USING NITRIC ACID. - Google Patents
METHOD FOR PICKLING AND PASSIVING STAINLESS STEEL WITHOUT USING NITRIC ACID.Info
- Publication number
- ATE129753T1 ATE129753T1 AT91113628T AT91113628T ATE129753T1 AT E129753 T1 ATE129753 T1 AT E129753T1 AT 91113628 T AT91113628 T AT 91113628T AT 91113628 T AT91113628 T AT 91113628T AT E129753 T1 ATE129753 T1 AT E129753T1
- Authority
- AT
- Austria
- Prior art keywords
- pickling
- stainless steel
- passiving
- nitric acid
- bath
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
- C23G1/02—Cleaning or pickling metallic material with solutions or molten salts with acid solutions
- C23G1/08—Iron or steel
- C23G1/086—Iron or steel solutions containing HF
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Detergent Compositions (AREA)
Abstract
A process for pickling and passivating stainless steel using a bath of the following initial composition: H2SO4 at least 150 g/l Fe<3><+> at least 15 g/l HF at least 40 g/l stabilized H2O2 1-20 g/l non-ionic surfactants and acid attack inhibitors 1 g/l, into which an air flow and an H2O2 quantity of between 0.3 and 1 g/l per hour, controlled to maintain the bath Redox potential at >/= 350 mV, are fed in continuously.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ITMI910879A IT1245594B (en) | 1991-03-29 | 1991-03-29 | PICKLING AND PASSIVATION PROCESS OF STAINLESS STEEL WITHOUT NITRIC ACID |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE129753T1 true ATE129753T1 (en) | 1995-11-15 |
Family
ID=11359360
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT91113628T ATE129753T1 (en) | 1991-03-29 | 1991-08-14 | METHOD FOR PICKLING AND PASSIVING STAINLESS STEEL WITHOUT USING NITRIC ACID. |
Country Status (9)
Country | Link |
---|---|
EP (1) | EP0505606B2 (en) |
JP (1) | JP2655770B2 (en) |
AT (1) | ATE129753T1 (en) |
DE (2) | DE505606T1 (en) |
DK (1) | DK0505606T3 (en) |
ES (1) | ES2082063T5 (en) |
FI (1) | FI101234B (en) |
GR (1) | GR3018681T3 (en) |
IT (1) | IT1245594B (en) |
Families Citing this family (25)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1255655B (en) * | 1992-08-06 | 1995-11-09 | STAINLESS STEEL PICKLING AND PASSIVATION PROCESS WITHOUT THE USE OF NITRIC ACID | |
IT1255855B (en) * | 1992-10-12 | 1995-11-17 | Cesare Pedrazzini | PICKLING AND PASSIVATION PROCESS FOR TITANIUM SHEETS IN TAPE, WITHOUT THE USE OF NITRIC ACID. |
DE4237021C1 (en) * | 1992-11-02 | 1994-02-10 | Poligrat Gmbh | Means for pickling the surface of chromium-nickel steels and chrome steels and use of the agent |
DE4417284C2 (en) * | 1993-05-24 | 1999-03-25 | Alfred Schmitz | Process for pickling workpieces from high-alloy materials |
ES2247593T3 (en) * | 1994-09-26 | 2006-03-01 | Steris, Inc. | STAINLESS STEEL ACID TREATMENT. |
IT1276954B1 (en) * | 1995-10-18 | 1997-11-03 | Novamax Itb S R L | PICKLING AND PASSIVATION PROCESS OF STAINLESS STEEL WITHOUT THE USE OF NITRIC ACID |
FR2745301B1 (en) * | 1996-02-27 | 1998-04-03 | Usinor Sacilor | PROCESS FOR STRIPPING A STEEL PART AND PARTICULARLY A STAINLESS STEEL SHEET STRIP |
FR2772050B1 (en) * | 1997-12-10 | 1999-12-31 | Imphy Sa | PROCESS FOR STRIPPING STEEL AND IN PARTICULAR STAINLESS STEEL |
DE19755350A1 (en) * | 1997-12-12 | 1999-06-17 | Henkel Kgaa | Process for pickling and passivating stainless steel |
EP0974682A1 (en) * | 1998-07-18 | 2000-01-26 | Henkel Kommanditgesellschaft auf Aktien | Method and apparatus for the chemical treatment of metalsurfaces |
IT1302202B1 (en) | 1998-09-11 | 2000-07-31 | Henkel Kgaa | ELECTROLYTIC PICKLING PROCESS WITH SOLUTIONS FREE FROM ACIDONITRICO. |
IT1303814B1 (en) * | 1998-12-02 | 2001-02-23 | Henkel Kgaa | APPARATUS AND METHOD TO CONTROL PERACCIAIO PICKLING PROCESSES. |
DE10157340A1 (en) * | 2001-11-22 | 2003-05-28 | Sms Demag Ag | Process for treating the surfaces of a metal strand used for pickling a steel strip comprises moving the strand through a closed treatment channel at a regulated speed while directing turbulent jets of a pickling liquid |
DE10160318A1 (en) | 2001-12-07 | 2003-06-18 | Henkel Kgaa | Process for pickling martensitic or ferritic stainless steel |
ES2350095T3 (en) | 2002-10-15 | 2011-01-18 | HENKEL AG & CO. KGAA | SOLUTION AND DECAPING PROCEDURE FOR STAINLESS STEEL. |
EP1793016A1 (en) * | 2005-12-01 | 2007-06-06 | Elpochem AG | Polishing and deburring composition for workpieces of carbon steel and method of chemical polishing and deburring |
KR100936348B1 (en) * | 2007-12-21 | 2010-01-12 | 주식회사 포스코 | High corrosion resistance surface treatment solution fostering material of low chromium stainless steel and passcivity treatment method of stainless steel by using the fostering material |
CN102337548B (en) * | 2011-09-14 | 2012-12-05 | 西部钛业有限责任公司 | Acid washing method of titanium and zirconium materials without acid-free fog |
GB2499000A (en) * | 2012-02-02 | 2013-08-07 | Henkel Ag & Co Kgaa | Aqueous acidic pickling solution with hydroxylamine accelerators |
GB2508827A (en) | 2012-12-11 | 2014-06-18 | Henkel Ag & Co Kgaa | Aqueous compositions and processes for passivating and brightening stainless steel surfaces |
DE102012024542A1 (en) * | 2012-12-14 | 2014-06-18 | Poligrat Gmbh | Thixotropic mordant |
JP6526406B2 (en) * | 2014-12-10 | 2019-06-05 | 株式会社Ihi | Method of passivating stainless steel parts and passivating solution for stainless steel parts |
CN108220937A (en) * | 2018-01-18 | 2018-06-29 | 浙江苏泊尔股份有限公司 | A kind of processing method of stainless steel work-piece high temperature resistance discoloration |
JP6592624B2 (en) * | 2019-01-15 | 2019-10-16 | 株式会社Ihi | Passivation treatment method for stainless steel parts and passivation treatment liquid for stainless steel parts |
US20220220619A1 (en) * | 2020-01-09 | 2022-07-14 | Primetals Technologies Japan, Ltd. | Method for pickling steel plate and pickling apparatus |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS549120A (en) * | 1977-06-24 | 1979-01-23 | Tokai Electro Chemical Co | Method of controlling acid cleaning liquid for stainless steel |
JPS5442850A (en) * | 1977-09-10 | 1979-04-05 | Kubota Ltd | Method of treating raw sewage |
JPS5551514A (en) * | 1978-10-12 | 1980-04-15 | Osaka Cement | Steel fiber mixing method and its device |
JPS568109A (en) * | 1979-07-03 | 1981-01-27 | Toshikazu Iwasaki | Reflecting telescope |
ATE121804T1 (en) * | 1985-01-22 | 1995-05-15 | Ugine Sa | METHOD FOR ACID PICKLING STEEL, PARTICULARLY STAINLESS STEEL. |
FR2587369B1 (en) * | 1985-09-19 | 1993-01-29 | Ugine Gueugnon Sa | PROCESS OF ACID STRIPPING OF STAINLESS STEEL PRODUCTS |
-
1991
- 1991-03-29 IT ITMI910879A patent/IT1245594B/en active IP Right Grant
- 1991-08-14 AT AT91113628T patent/ATE129753T1/en not_active IP Right Cessation
- 1991-08-14 DK DK91113628.1T patent/DK0505606T3/en active
- 1991-08-14 DE DE91113628T patent/DE505606T1/en active Pending
- 1991-08-14 ES ES91113628T patent/ES2082063T5/en not_active Expired - Lifetime
- 1991-08-14 DE DE69114265T patent/DE69114265T3/en not_active Expired - Lifetime
- 1991-08-14 EP EP91113628A patent/EP0505606B2/en not_active Expired - Lifetime
- 1991-10-04 JP JP3284206A patent/JP2655770B2/en not_active Expired - Lifetime
-
1992
- 1992-02-12 FI FI920580A patent/FI101234B/en not_active IP Right Cessation
-
1996
- 1996-01-17 GR GR960400082T patent/GR3018681T3/en unknown
Also Published As
Publication number | Publication date |
---|---|
EP0505606B1 (en) | 1995-11-02 |
DE505606T1 (en) | 1994-02-03 |
DE69114265T3 (en) | 2004-08-05 |
JPH04304391A (en) | 1992-10-27 |
ES2082063T5 (en) | 2003-11-01 |
FI101234B (en) | 1998-05-15 |
FI920580A (en) | 1992-09-30 |
ES2082063T3 (en) | 1996-03-16 |
EP0505606B2 (en) | 2003-02-26 |
FI920580A0 (en) | 1992-02-12 |
JP2655770B2 (en) | 1997-09-24 |
DE69114265D1 (en) | 1995-12-07 |
DK0505606T3 (en) | 1995-12-04 |
DE69114265T2 (en) | 1996-04-18 |
IT1245594B (en) | 1994-09-29 |
GR3018681T3 (en) | 1996-04-30 |
ITMI910879A1 (en) | 1992-09-29 |
ITMI910879A0 (en) | 1991-03-29 |
EP0505606A1 (en) | 1992-09-30 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
UEP | Publication of translation of european patent specification | ||
EEIH | Change in the person of patent owner | ||
EEIH | Change in the person of patent owner | ||
REN | Ceased due to non-payment of the annual fee |