AT80805B - Process for separating water or aqueous Process for separating water or aqueous solutions from petroleum or other oil emulsions. en solutions from petroleum or other oil emulsions. - Google Patents
Process for separating water or aqueous Process for separating water or aqueous solutions from petroleum or other oil emulsions. en solutions from petroleum or other oil emulsions.Info
- Publication number
- AT80805B AT80805B AT80805DA AT80805B AT 80805 B AT80805 B AT 80805B AT 80805D A AT80805D A AT 80805DA AT 80805 B AT80805 B AT 80805B
- Authority
- AT
- Austria
- Prior art keywords
- petroleum
- oil emulsions
- separating water
- solutions
- aqueous
- Prior art date
Links
Landscapes
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Description
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Verfahren zur Abscheidung von Wasser oder wässerigen Lösungen aus Erdöl-oder anderen Ölemulsionen.
Die Schwierigkeiten der Abscheidung von Wasser aus Erdö'-oder anderen Ölemulsionen suchte man bis jetzt dadurch zu überwinden, dass man die Emulsionen längere Zeit erwärmte, wodurch jedoch in den meisten Fällen, sogar bei sehr langem Abstehen, nur eine unvollständige Abscheidung der wässerigen Phasen erreicht wurde.
Der Gegenstand der vorliegenden Erfindung beruht auf der Erkenntnis, dass erst bei höherer Temperatur, die nur bei Überdruck zu erzielen ist, eine solche Verminderung
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der wässerigen Phase ermöglicht.
Dieser Zustand verminderter Viskosität wird dadurch erreicht, dass die Emulsion in geschlossenen Gefässen auf die Temperaturen über ioo"C unter mindestens I Atm.
Überdruck erwärmt, einige Zeit in diesem Zustand unterhalten, hierauf abgekühlt wird, worauf die getrennten Phasen nacheinander abgelassen werden können.
Die Erwärmung kann entweder durch Erhitzen in der Blase oder dadurch erfolgen, dass Wasserdampf unter Überdruck in das Reaktionsgefäss eingeführt wird. Die zur Trennung erforderliche Zeit ist von der Beschaffenheit der Emulsion und von der Grösse der suspen- dierten Wassertei1chen abhängig. Die Zeit des Abscheidens kann man verkürzen, wenn bei verminderter Viskosität die Emulsion durchgerührt und hierauf der Inhalt des Behälters absetzen gelassen wird.
Ausführungsbeispiel : Eine frisch aus dem Schachte gewonnene Rohölemulsion wird durch vier Stunden bei 8 Atm. Überdruck ohne Rühren erwärmt. Nach dieser Zeit ist die Trennung der Rohölemulsion in 56"/,) Salzlösung und 440/0 Rohöl vollzogen. Ein Erwärmen auf 5-6 Atm. führt auch zum Ziele, erfordert aber zur Trennung unter Riihren eine Arbeitszeit von etwa 10 Stunden.
**WARNUNG** Ende DESC Feld kannt Anfang CLMS uberlappen**.
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Process for separating water or aqueous solutions from petroleum or other oil emulsions.
The difficulties of separating water from petroleum or other oil emulsions have hitherto been attempted by heating the emulsions for a longer period of time, which in most cases, even when standing for a very long time, only achieves incomplete separation of the aqueous phases has been.
The subject matter of the present invention is based on the knowledge that such a reduction is only achieved at a higher temperature, which can only be achieved at overpressure
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the aqueous phase allows.
This state of reduced viscosity is achieved by bringing the emulsion in closed vessels to temperatures above 100 "C below at least 1 atm.
Heated overpressure, maintained in this state for some time, then cooled, whereupon the separate phases can be drained off one after the other.
The heating can take place either by heating in the bubble or by introducing steam into the reaction vessel under excess pressure. The time required for separation depends on the nature of the emulsion and the size of the suspended water particles. The separation time can be shortened if the emulsion is stirred through at a reduced viscosity and the contents of the container are then allowed to settle.
Exemplary embodiment: A crude oil emulsion freshly obtained from the shaft is heated for four hours at 8 atm. Heated overpressure without stirring. After this time, the separation of the crude oil emulsion into 56% salt solution and 440/0 crude oil is complete. Heating to 5-6 atm. Also works, but requires a working time of about 10 hours for separation with stirring.
** WARNING ** End of DESC field may overlap beginning of CLMS **.
Claims (1)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AT80805T | 1917-02-17 |
Publications (1)
Publication Number | Publication Date |
---|---|
AT80805B true AT80805B (en) | 1920-06-25 |
Family
ID=3602336
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT80805D AT80805B (en) | 1917-02-17 | 1917-02-17 | Process for separating water or aqueous Process for separating water or aqueous solutions from petroleum or other oil emulsions. en solutions from petroleum or other oil emulsions. |
Country Status (1)
Country | Link |
---|---|
AT (1) | AT80805B (en) |
-
1917
- 1917-02-17 AT AT80805D patent/AT80805B/en active
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