AT47526B - Process for the preparation of blue vat dyes of the sulfine series. - Google Patents

Process for the preparation of blue vat dyes of the sulfine series.

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Publication number
AT47526B
AT47526B AT47526DA AT47526B AT 47526 B AT47526 B AT 47526B AT 47526D A AT47526D A AT 47526DA AT 47526 B AT47526 B AT 47526B
Authority
AT
Austria
Prior art keywords
preparation
vat dyes
sulfine
series
blue vat
Prior art date
Application number
Other languages
German (de)
Original Assignee
Cassella Leopold & Co Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cassella Leopold & Co Gmbh filed Critical Cassella Leopold & Co Gmbh
Application granted granted Critical
Publication of AT47526B publication Critical patent/AT47526B/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Description

  

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Claims (1)

PATENT-ANSPRUCH : Verfahren zur Darstellung in verdünnter Schwefelalkalilösung schwerlöslicher blauer Küpenfarbstoffe aus den durch Kondensation von Nitrosophenolen und Carbazol in Gegenwart von konzentrierter Schwefelsäure erhältlichen Produkten oder ihren Leukoverbindungen, dadurch gekennzeichnet, dass man entweder die beim Erhitzen dieser Körper mit Alkalipolysulfiden nach den üblichen Methoden gewonnenen Rohschmelzen zur Knt- fernung der in verdunnten Schwefelalkalien löslichen Anteile mit Schwefelnatriumlösung extrahiert, oder aber die Schwefelung dieser Körper mit einem Alhalipolybulfid von hohem Schwefelgehalt, am besten in Gegenwart eines geeigneten Verdünnungs- oder Lösungsmittels, durchführt. PATENT CLAIM: Process for the preparation of poorly soluble blue vat dyes in dilute alkaline sulfur solution from the products obtainable by condensation of nitrosophenols and carbazole in the presence of concentrated sulfuric acid or their leuco compounds, characterized in that either the crude melts obtained when these bodies are heated with alkali polysulphides by the usual methods for kneading Removal of the solubles in dilute alkaline sulfur extracts with sodium sulphide solution, or the sulphurisation of these bodies with an alhalipolybulphide with a high sulfur content, preferably in the presence of a suitable diluent or solvent.
AT47526D 1909-05-14 1910-04-08 Process for the preparation of blue vat dyes of the sulfine series. AT47526B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE47526X 1909-05-14

Publications (1)

Publication Number Publication Date
AT47526B true AT47526B (en) 1911-04-25

Family

ID=5625670

Family Applications (1)

Application Number Title Priority Date Filing Date
AT47526D AT47526B (en) 1909-05-14 1910-04-08 Process for the preparation of blue vat dyes of the sulfine series.

Country Status (1)

Country Link
AT (1) AT47526B (en)

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