AR106225A1 - Proceso y aparato para producir ácido acético - Google Patents

Proceso y aparato para producir ácido acético

Info

Publication number
AR106225A1
AR106225A1 ARP160103004A ARP160103004A AR106225A1 AR 106225 A1 AR106225 A1 AR 106225A1 AR P160103004 A ARP160103004 A AR P160103004A AR P160103004 A ARP160103004 A AR P160103004A AR 106225 A1 AR106225 A1 AR 106225A1
Authority
AR
Argentina
Prior art keywords
head
acetic acid
acetaldehyde
rich
separate
Prior art date
Application number
ARP160103004A
Other languages
English (en)
Inventor
Mizutani Yoshihisa
Miura Hiroyuki
Original Assignee
Daicel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daicel Corp filed Critical Daicel Corp
Publication of AR106225A1 publication Critical patent/AR106225A1/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/143Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/143Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/148Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40Extractive distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/08Acetic acid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/42Regulation; Control
    • B01D3/4211Regulation; Control of columns
    • B01D3/4294Feed stream

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Se provee un proceso para producir de manera estable y segura ácido acético, sin aumentar la presión interna de la columna de destilación; el proceso comprende (1) un paso de reacción de carbonilación para dejar que el metanol reaccione con monóxido de carbono; (2) un paso de evaporación instantánea para separar la mezcla de reacción en una fase volátil y una fase menos volátil; (3) un primer paso de destilación para separar la fase volátil en una primera cabeza y una corriente de ácido acético crudo rica en ácido acético; y (4) un paso de separación para separar por lo menos acetaldehído de la primera cabeza; el paso de separación (4) comprende (6) un segundo paso de destilación para destilar la primera cabeza, controlando al mismo tiempo la presión interna de la columna de destilación provista de una unidad de control de presión 68 para formar una segunda cabeza rica en acetaldehído y yoduro de metilo y una corriente de fondo o inferior, y (7) un paso de extracción para extraer acetaldehído de la segunda cabeza para formar un extracto rico en acetaldehído y un refinado rico en yoduro de metilo.
ARP160103004A 2015-09-30 2016-09-30 Proceso y aparato para producir ácido acético AR106225A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2015194762 2015-09-30

Publications (1)

Publication Number Publication Date
AR106225A1 true AR106225A1 (es) 2017-12-27

Family

ID=58424077

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP160103004A AR106225A1 (es) 2015-09-30 2016-09-30 Proceso y aparato para producir ácido acético

Country Status (8)

Country Link
US (2) US10428006B2 (es)
JP (1) JP6822969B2 (es)
KR (1) KR102601400B1 (es)
CN (1) CN108137462A (es)
AR (1) AR106225A1 (es)
SG (1) SG11201800858SA (es)
TW (1) TW201726594A (es)
WO (1) WO2017057142A1 (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10428004B2 (en) 2017-01-18 2019-10-01 Daicel Corporation Method for producing acetic acid
JP6693959B2 (ja) * 2017-01-18 2020-05-13 株式会社ダイセル 酢酸の製造方法
CN112368257B (zh) * 2018-07-02 2023-12-19 株式会社大赛璐 乙酸的制造方法
JP6546709B1 (ja) * 2018-07-02 2019-07-17 株式会社ダイセル 酢酸の製造方法
CN109232223A (zh) * 2018-11-02 2019-01-18 江苏索普(集团)有限公司 一种合成醋酸的工艺
US10807935B2 (en) 2018-11-02 2020-10-20 Celanese International Corporation Process for continuous acetic acid production
US20210189308A1 (en) * 2019-12-19 2021-06-24 Abv Technology, Inc. Process for separating a fermented malt beverage
GB202015833D0 (en) * 2020-10-06 2020-11-18 Bp Chem Int Ltd Separation process and apparatus
CN115253378A (zh) * 2022-07-27 2022-11-01 郑州天一萃取科技有限公司 多级离心萃取系统、用于多级萃取的离心萃取机

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3244385B2 (ja) * 1994-06-15 2002-01-07 ダイセル化学工業株式会社 高純度酢酸の製造方法
US5625095A (en) 1994-06-15 1997-04-29 Daicel Chemical Industries, Ltd. Process for producing high purity acetic acid
JP3673565B2 (ja) * 1995-07-17 2005-07-20 日揮株式会社 蒸留装置及び蒸留方法
US7223883B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
US7223886B2 (en) 2004-03-02 2007-05-29 Celanese International Corporation Removal of permanganate reducing compounds from methanol carbonylation process stream
US7855306B2 (en) * 2005-04-28 2010-12-21 Celanese International Corporation Process for the production of acetic acid
JP4725360B2 (ja) * 2006-02-27 2011-07-13 住友化学株式会社 蒸留システムおよび蒸留システムにおける蒸留塔の塔頂圧力を制御する方法
US7619113B2 (en) 2007-09-27 2009-11-17 Celanese International Corporation Method and apparatus for making acetic acid with improved purification
US7820855B2 (en) * 2008-04-29 2010-10-26 Celanese International Corporation Method and apparatus for carbonylating methanol with acetic acid enriched flash stream
US7790920B2 (en) * 2008-09-11 2010-09-07 Lyondell Chemical Technology, L.P. Preparation of acetic acid
CN101380522B (zh) * 2008-10-15 2012-07-04 天津大学 一种加压精馏的装置和方法
US7884237B2 (en) * 2008-11-07 2011-02-08 Celanese International Corp. Methanol carbonylation with improved aldehyde removal
US8586789B2 (en) 2009-03-30 2013-11-19 Lyondell Chemical Technology, L.P. Removing hydrocarbon impurities from acetic acid production intermediate
JP5582044B2 (ja) * 2010-05-12 2014-09-03 三菱化学株式会社 蒸留塔の圧力制御方法
CN103370300B (zh) * 2010-12-15 2016-07-06 株式会社大赛璐 乙酸的制备方法
TWI547477B (zh) 2012-03-14 2016-09-01 大賽璐股份有限公司 醋酸之製造方法
US8859810B2 (en) * 2012-08-21 2014-10-14 Celanese International Corporation Process for recovering permanganate reducing compounds from an acetic acid production process
KR102080091B1 (ko) * 2012-12-21 2020-02-24 주식회사 다이셀 아세트산의 제조 방법
CN219166062U (zh) 2020-11-27 2023-06-13 宋恩儆 用于哺乳靠垫的功能性外罩及功能性哺乳靠垫

Also Published As

Publication number Publication date
US20190367439A1 (en) 2019-12-05
US20180230077A1 (en) 2018-08-16
KR20180059484A (ko) 2018-06-04
US10894759B2 (en) 2021-01-19
WO2017057142A1 (ja) 2017-04-06
CN108137462A (zh) 2018-06-08
JP6822969B2 (ja) 2021-01-27
TW201726594A (zh) 2017-08-01
SG11201800858SA (en) 2018-04-27
US10428006B2 (en) 2019-10-01
KR102601400B1 (ko) 2023-11-14
JPWO2017057142A1 (ja) 2018-07-26

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