WO2023121463A1 - Atomic force microscope (afm) device and method of operating the same - Google Patents

Atomic force microscope (afm) device and method of operating the same Download PDF

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Publication number
WO2023121463A1
WO2023121463A1 PCT/NL2022/050755 NL2022050755W WO2023121463A1 WO 2023121463 A1 WO2023121463 A1 WO 2023121463A1 NL 2022050755 W NL2022050755 W NL 2022050755W WO 2023121463 A1 WO2023121463 A1 WO 2023121463A1
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WIPO (PCT)
Prior art keywords
sample
tip
information
scanning
probe
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PCT/NL2022/050755
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English (en)
French (fr)
Inventor
Jakob van de Laar
Hamed Sadeghian Marnani
Arseniy KALININ
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Nearfield Instruments BV
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Nearfield Instruments BV
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Priority to KR1020247023015A priority Critical patent/KR20240129180A/ko
Priority to US18/709,243 priority patent/US20250004010A1/en
Priority to JP2024532950A priority patent/JP2024546629A/ja
Publication of WO2023121463A1 publication Critical patent/WO2023121463A1/en
Anticipated expiration legal-status Critical
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01QSCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q10/00Scanning or positioning arrangements, i.e. arrangements for actively controlling the movement or position of the probe
    • G01Q10/04Fine scanning or positioning
    • G01Q10/06Circuits or algorithms therefor
    • G01Q10/065Feedback mechanisms, i.e. wherein the signal for driving the probe is modified by a signal coming from the probe itself
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01QSCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q10/00Scanning or positioning arrangements, i.e. arrangements for actively controlling the movement or position of the probe
    • G01Q10/04Fine scanning or positioning
    • G01Q10/06Circuits or algorithms therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01QSCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q30/00Auxiliary means serving to assist or improve the scanning probe techniques or apparatus, e.g. display or data processing devices
    • G01Q30/04Display or data processing devices
    • G01Q30/06Display or data processing devices for error compensation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01QSCANNING-PROBE TECHNIQUES OR APPARATUS; APPLICATIONS OF SCANNING-PROBE TECHNIQUES, e.g. SCANNING PROBE MICROSCOPY [SPM]
    • G01Q60/00Particular types of SPM [Scanning Probe Microscopy] or microscopes; Essential components thereof
    • G01Q60/24AFM [Atomic Force Microscopy] or apparatus therefor, e.g. AFM probes

Definitions

  • the present invention pertains to an Atomic Force Microscope (AFM) device.
  • AFM Atomic Force Microscope
  • the present invention further pertains to a method of operating an AFM device.
  • AFM-devices are widely used for example in the semiconductor industry to determine a surface topography of a (semi-finished) product.
  • An AFM-device comprises a scanning head with a tip that is scanned along the surface of a sample along a scanning trajectory. Therewith the operation of the AFM-device is determined by various imaging parameters, such as a force threshold, a baseline offset, an approach profile, a retract profile and a scanning speed.
  • Practical samples for examination in the semiconductor industry typically comprise 3D samples with narrow and high aspect-ratio features.
  • the surface topography as imaged by the AFM-device may deviate from the actual surface topography of the sample due to various causes.
  • a relatively high level of the contact force may cause the tip to slip off from the top of the narrow feature, so that it slides to a lower level.
  • the height value as indicated in the imaged surface topography for a lateral position x,y is less than the actual height of the sample at that lateral position.
  • it has been found that deviations can occur when the tip is present at the lateral position of a narrow and relatively deep recessed portion of the sample.
  • An example thereof is a feature having a characteristic lateral size that is moderately larger than the diameter of the tip, i.e. larger than one times the diameter of the tip, but smaller than ten times the diameter of the tip and a depth substantially larger than the width, e.g. more than two times the diameter.
  • the feature is for example a hole, of which the characteristic lateral size is its diameter, or a trench, of which the characteristic lateral size is its width. Deviations may occur in this case because the contact -force exerted by the tip is not sufficient to outweigh friction forces exerted on the tip by a wall of the recessed portion, so that the tip does not fully protrude into the recessed portion.
  • the height value as indicated in the imaged surface topography for a lateral position x,y is greater than the actual height of the sample at that lateral position. It is noted that these deviations generally are less if the stiffness of the tip -cantilever combination is relatively high.
  • the stiffness of the tip -cantilever combination is determined by the rotational stiffness of the cantilever and the flexural stiffness of the tip.
  • Other local device properties may also affect the image surface topography. For example a feature of a relatively hard material may appear to be positioned at a higher level in the imaged surface topography than a feature of a relatively soft material, even if both features actually are at the same level in the imaged surface of the 3D sample.
  • the method of operating an AFM device comprises:
  • the prior information about the sample comprises information about the sample obtained prior to said scanning.
  • the prior information about the sample obtained prior to said scanning may for example comprise information from a specification of the sample and/or information about the sample obtained during recipe creation.
  • the specification of the sample specifies the desired topography of the sample, as well as the properties of the materials used for the features thereof.
  • Information about the sample obtained during recipe creation may indicate that the actual topography tends to deviate in a certain way from the designed topography. Although the information obtained during recipe creation does not fully describe the actual topography, it helps to predict the way in which the actual topography deviates.
  • the information obtained during recipe creation may indicate that edges are on average less wide than originally was specified.
  • Prior information about the sample renders it possible to scan surface elements of the sample with optimal settings so that the output signal obtained with these settings more accurately indicates the actual height of the surface as a function of the lateral position.
  • the information about the sample obtained prior to said scanning may further comprise information obtained from a preceding device inspection method, for example information obtained from an electron microscopic image of the sample.
  • the force threshold is an upper limit to a force exerted by the tip on the sample.
  • a relatively high force threshold is selected if information from the region of the current scan position indicates that the current scan point is expected to be within a relatively deep and narrow recess or at a bottom close to a steep wall and a relatively low force threshold is selected if the information from the region indicates a relatively wide recess or wide flat area away from relatively steep and high edges/walls.
  • the information about the sample obtained prior to said scanning does not always exactly correspond to the actual topology of the sample
  • this information renders it possible to set the force threshold optimally for the purpose of more exactly determining the actual topology.
  • surface elements having a high level that are close to a low level are more accurately imaged with a relatively low force threshold setting.
  • the risk of a lateral sliding of the tip towards a lower level is mitigated.
  • This also reduces the risk of damage caused by the tip on the sample surface.
  • a relatively narrow and deep recess in the surface of the sample is more accurately imaged with a relatively high force threshold setting.
  • the force exerted on the tip can more easily overcome forces, e.g. due to friction, exerted thereon by the sidewalls of the recess.
  • the depth of the recess is more accurately indicated in the imaged surface topography.
  • the information about the sample may further comprise information obtained from a scanning according to a previous scan line in a direction substantially parallel to the current scan line.
  • the present invention in particular is suitable to a trigger based scanning embodiment.
  • the scanning comprises a scanning cycle for each scanning position with the following stages: a) with the tip approaching the sample at a lateral position of the sample surface, b) retracting the tip from the sample and c) displacing the tip towards a new lateral position.
  • Interaction data indicative for an interaction between the tip and the sample is obtained during said approaching and/or retracting,
  • Imaging parameters to be adapted thereof are an initial height from which the sample surface is approached and a velocity with which the sample is approached.
  • Retracting the sample is determined by a retract profile.
  • imaging parameters to be adapted thereof are a force threshold, and/or a displacement threshold and/or a retract distance and/or velocity.
  • retraction of the tip from the sample starts if the force exerted by the tip exceeds a pre-specified force threshold.
  • retraction starts if the measured depth exceeds a depth threshold.
  • retraction starts as soon as one of these conditions occurs, whichever is the first, or alternatively retraction starts once both conditions are satisfied.
  • Another imaging parameter relevant for the retraction stage is the retract distance.
  • the retract distance is increased for locations where the adhesion of the surface is determined to be relatively high.
  • the retract distance may be adapted on the fly. I.e. retraction may be interrupted, and the surface may be approached again if it is detected that ringing of the cantilever is reduced to a sufficient extent, even before retraction over the predetermined distance has been completed. Therewith measurement speed is improved.
  • the cantilever In operation the cantilever is flexed due to forces acting between the tip and the sample surface. Also due to electrostatic forces a flexure of the cantilever may occur even at larger distances from the sample. This causes a bias which may be compensated for by taking into account a baseline offset. If desired, the baseline offset may be updated each measurement cycle.
  • the baseline offset and the force threshold may both be adapted dependent on the prior information of the sample at the lateral position to be scanned and the force threshold is chosen relative to the baseline offset.
  • the prior information about the sample may comprise information from a specification of the sample. This may comprise device design data and/or recipe data. It may be assumed that under normal circumstances the topography of the sample to be measured is approximated by the topography as derived from prior information about the sample, for example from the specification of the sample and/or information obtained during recipe creation.
  • the prior information about the sample may comprise information obtained from a scanning according to a previous scan line in a direction substantially parallel to the current scan line. Provided that the current scan line and the previous scan line are close enough to each other, the topography of the current scan line is approximated by the topography of the previous scan line, so that again a substantial improvement is obtained as compared to the case that a uniform set of settings is used for imaging the entire sample.
  • subsequent scanlines are substantially parallel. I.e. in that case subsequent scanlines are at a mutual distance Ay.
  • scanning proceeds by a movement of the probe in a direction x along a scanline y, y+Ay, y+2Ay, ... etc.
  • stepwise increasing the coordinate y between subsequent scanlines it is possible to gradually increase y while scanning. Therewith a triangular scan path is followed.
  • imaging parameters are adapted during scanning based on prior information about the sample and from prior information obtained from a previous scan line. Therewith a still further improvement is achieved.
  • prior information about the sample is used in combination with information obtained while scanning. For example if it appears at a position x along a current scan-line y that the topography strongly deviates from that at position x along the previous scan-line y-Ay this deviation may be incorporated when preparing the adaptation of the settings for the subsequent position x+Ax along the current scan-line.
  • An embodiment further comprises supplying an acoustic signal to one or more of the probe, the tip or the sample and analyzing an output signal based on an interaction of the acoustic signal with the sample.
  • the output signal is indicative for subsurface characteristics of the sample.
  • the force exerted by the tip on the sample is proportional to deflection of the cantilever and the stiffness of the cantilever.
  • a vibration of the probe is induced to change an effective force exerted by the probe to the sample.
  • the vibration increases the stiffness of the cantilever and therewith also increases the effective force exerted to the sample.
  • FIG. 1 schematically shows a part of an exemplary improved AFM-device and a sample scanned therewith;
  • FIG. 2 shows aspects of a controller of a first embodiment of the improved AFM-device
  • FIG. 3 schematically illustrates two graphs of a Z-position signal for a Z- actuator and for a measured deflection signal from a probe tip in an embodiment of the present invention
  • FIG. 4 schematically illustrates four probe deflection situations associated with certain positions in FIG. 3;
  • FIG. 5 shows aspects of a controller of a second embodiment of the improved AFM-device
  • FIG. 6 shows aspects of a controller of a third embodiment of the improved AFM-device
  • FIG. 7 shows aspects of a controller of a fourth embodiment of the improved AFM-device.
  • FIG. 1 schematically shows a part of an exemplary improved AFM-device 1 and a sample 9 scanned therewith;
  • FIG. 2 shows aspects of a controller of a first embodiment of the improved AFM- device;
  • the AFM-device 1 comprises at least one scan head 10 for scanning a sample 9.
  • the scan head 10 includes a probe 11 that comprises a cantilever 12 and a probe tip 13 arranged on the cantilever.
  • the AFM-device 1 further comprises a first actuator 20 that cooperates with a substrate holder 95 in order to move the probe tip 13 and the sample 9 relative to each other in one or more directions x, y parallel to a surface 91 of the sample for scanning of the surface with the probe tip.
  • the first actuator cooperates with the scan head and in again other embodiments a respective first actuator is provided to cooperate with the scan head and the substrate holder for scanning of the surface 91.
  • the AFM-device 1 further comprises a cantilever deflection detector 30 that is configured to measure a motion/position of the probe tip 13 relative to the scan head 10 and sample during said scanning.
  • the detector 30 is further configured to providing an output signal Sout, that is indicative of the deflection of the cantilever due to the tip -sample interaction, and as such (in the static regime) of the applied force.
  • the sample topography is derived from the height of the AFM head minus the tip-head distance as indicated by the cantilever deflection.
  • a tip deformation sensor 15 is provided that provides a sense signal Stdf, indicative for a deformation of the tip 13 when contacting the surface 91 of the sample 9.
  • the AFM-device 1 still further comprises a controller 40, that is configured to receive and analyze the output signal Sout from the cantilever deflection detector 30, for imaging sample characteristics at and/or below the surface 91 of the sample 9.
  • the controller 40 further receives additional information for its analysis, such as position signals x, y indicating the lateral position of the probe tip as indicated by the control signal of the XY actuator 20 and/or by the displacement sensor 21, as well as the z-position of the probe as indicated by the control signal for the Z actuator 60 and/or by the displacement sensor 61.
  • the controller 40 also receives the sense signal Stdf, indicative for a deformation of the tip 13.
  • the controller 40 is configured to reduce a force threshold if the indicated deformation of the tip exceeds a predetermined limit. Alternatively and/or additionally it may be configured to process an output signal obtained by the device to compensate for deviations caused by the deformation of the tip 13.
  • the AFM-device is configured to perform a scanning cycle for each scanning position with the following stages.
  • the tip 13 approaches the sample 9 according to an approach profile wherein it starts from a reference position z above the sample 9.
  • the approach profile specifies the reference position z, which is for example a predetermined z-value which is higher than any z-value at the surface 91 of the sample 9.
  • the reference position z is a relative position at a predetermined distance with reference to an expected z-value of the surface at the lateral coordinate x,y to be approached.
  • the approach profile further specifies the velocity with which the surface 91 is approached. This is for example a constant velocity.
  • the velocity is variable, for example starting with a relatively high velocity and stepwise or gradually reducing the velocity while approaching.
  • the tip 13 is retracted from the sample surface 91.
  • the transition from the first stage to the second stage may be determined by one or more of the following. According to one option the transition takes place if the tip or the probe has progressed a predetermined distance towards the sample. According to another option the transition takes place if a force exerted by the tip exceeds a threshold value. According to a still further option, retraction starts as soon as one of these conditions occurs, whichever is the first, or alternatively retraction starts once both conditions are satisfied.
  • Another imaging parameter relevant for the retraction stage is the velocity with which retraction occurs. Operation in the second stage is determined by a velocity with which retraction is performed. As in the approach profile, the velocity may be a constant value, or may change during retraction.
  • the tip is displaced towards a subsequent lateral position.
  • the magnitude of the lateral distance is an example of a further imaging parameter.
  • interaction data is obtained that is indicative for an interaction between the tip and the sample.
  • a tip-sample force curve is determined, which specifies the force between the tip and the sample as a function of the displacement of the tip towards and/or away from the sample.
  • the sample 9 shown in FIG. 1 has surface sections 9 IB, 9 IS and 9 IT at various levels.
  • the tip 13 is currently positioned at the edge of a shoulder section 9 IS with a bottom section 9 IB. Due to a downward force exerted at the tip 13 there is a risk that a deformation of the cantilever 12 and/or tip occurs that causes the tip 13 to slide towards the bottom section 9 IB, so that the cantilever deflection detector 30 indicates a lower z-value than that of the position x,y where the tip 13 was originally positioned. Although this phenomenon only occurs near the edge of a section with a lower level section, the measurement errors become significant for samples with surface features having a high aspect ratio.
  • the walls 91BW of the bottom section 9 IB near the tip 13 exert forces on the tip that may prevent the tip to sufficiently approach the bottom section 9 IB, so that the cantilever deflection detector 30 indicates a higher z-value than the actual z- value at the position x,y of the tip 13. Also this type of measurement error becomes more significant if the aspect ratio, i.e. a ratio between a depth of the bottom section 9 IB relative to a lateral dimension thereof increases.
  • the improved AFM-device 1 as disclosed herein mitigates these error sources in that the controller 40 is configured to automatically adapt one or more imaging parameters during scanning in accordance with information about sample properties at the lateral position of the sample currently being scanned.
  • the information about sample properties comprises one or more of information from a specification of the sample, a recipe for manufacturing the sample and information obtained from a scanning according to a previous scan line in a direction substantially parallel to the current scan line.
  • information obtained while scanning a trajectory may also be used to provide additional adaptations on the fly.
  • the imaging parameters are locally optimized for a proper z-measurement.
  • a relatively low force threshold is selected at x,y positions that are predicted to be a position on the surface having a relative high level close to an edge with a lower level surface.
  • a relatively high force threshold is selected at lateral (x, y) positions predicted to be part of a bottom section close to a wall.
  • a further example is an adaptation of a baseline offset in accordance with a predicted height at a lateral position.
  • a still further example is an adaptation of a retract profile in accordance with an estimated adhesion of the sample surface at the lateral position of the tip.
  • the AFM device may comprise an acoustic signal generator e.g. 51a, 51b, 51c to supply an acoustic signal to one or more of the probe 11, the tip 13 or the sample 9 and a signal analysis module 52 to analyze an output signal based on an interaction of the acoustic signal with the sample 9.
  • the output signal S ou t of the tip -deflection sensor is further indicative for subsurface characteristics of the sample.
  • both topographic information and subsurface information can be obtained, for example for the purpose of overlay and/or alignment analysis.
  • the AFM device may comprise a signal source, for example signal source 51a, for inducing a vibration in the probe 11 to increase an effective stiffness of the cantilever 12.
  • the vibration increases the stiffness of the cantilever 12 and therewith also increases the effective force exerted to the sample. In the absence of an induced vibration, the stiffness of the cantilever is determined by the static spring constant of the cantilever. By imposing the vibration, the stiffness is increased.
  • the effective force exerted to the sample can be computed from the deflection of the cantilever and its effective stiffness as a function of the induced vibration for example using a computation module 53.
  • the AFM device comprises a tip deformation sensor 15 to provide a tip deformation signal Stdf, indicative for a deformation of the tip 13.
  • the controller 40 of AFM-device is configured to reduce the force threshold if the indicated deformation of the tip exceeds a predetermined limit.
  • the AFM-device may be configured to compensate a reconstructed image for this deformation. This optional feature may be provided as an alternative or in combination with other measures taken for control of settings of the AFM-device.
  • FIG. 2 shows a first embodiment of the improved AFM-device 1 in more detail.
  • the controller 40 comprises a signal analysis unit 41, an image memory 42 and a motion profile generator 45.
  • the probe/cantilever deflection detector 30 comprises an optical detection element 31, in this example a four quadrant optical detection element and a deflection signal processing unit 32.
  • the deflection signal processing unit 32 computes the probe deflection from the signal S31 issued by the optical detection element 31 and provides the signal to motion profile generator 45.
  • the motion profile generator 45 generates a control signal Cz to control z-actuator 60 and a control signal Oxy to control xy-actuator 20.
  • the motion profile generator 45 further provides an input signal to image memory 42 that indicates the z- value determined for each pixel with lateral coordinates x,y.
  • the coordinates x,y,z to be stored in the image memory 42 are the coordinates specified by the motion profile generator 45.
  • the z-value is defined as the vertical “tip position'' at the moment a certain pre-defined force threshold is reached. In practice deviations may occur between the specified coordinates and the actual coordinates.
  • typically position sensors 21, 61 see FIG. 1 are provided to sense the lateral position (x,y) of the sample 9 and the vertical position z of the probe 11. The sense signals from these sensors are provided as feedback signal to the motion profile generator 45.
  • the topography Z(x,y) of the surface 91 of the sample 9 can be retrieved from the image memory 42.
  • the signal processing unit 41 computes a force threshold setting Ft(x,y) for a lateral position x,y, based on topographic data z(x,y-Ay) from a previous scanline.
  • FIG. 3 illustrates schematic graphs of a probe deflection signal d51 and the Z-position actuator signal z41 in the embodiment of FIG. 2 during a non-resonant imaging mode.
  • the lower graph illustrates the Z-position actuator signal Cz driving the probe 11 to and from the surface 91 of the sample 9.
  • the horizontal axis is indicative of time t, and the level of axis a43 corresponds with the Z-level at which the probe tip 13 just contacts the surface 91. Extending the probe 11 further towards the surface 91 in the negative Z direction causes the reactive force of the surface 91 on to the probe tip 13 to increase.
  • the upper graph schematically illustrates the deflection signal d51 of the probe tip 13 over time.
  • the deflection signal d51 is represented by parameter d.
  • the Z position actuator signal z41 further drives the probe 11 (and probe tip 13) towards the surface 91.
  • the vertical lines t45, t46, t47, t48, t49 mark characteristic points in time that will be discussed below.
  • stage A is schematically illustrated in situation s60 showing the position of the probe tip 13 and the probe 11 in relaxed state above the surface 91.
  • the probe tip 13 is briefly attracted by the surface 91 as illustrated by the dip in deflection signal d51.
  • the Z-position signal d41 indicates that the probe 11 is further extended towards the surface 91 such as to increase the probe-sample interaction force.
  • the part z44 of the Z-position signal z41 illustrates this by showing a negative Z-position. Extension of the probe 11 towards the surface 91 is continued until at time point t46 the threshold level Ft(x,y) in the probe-sample interaction force is reached. Thereafter, between t46 and t47, the probe 11 is retracted again showing an increase in the Z-position signal z41.
  • Stage B in fact consists of a first and a second part, corresponding to a part before the maximum in the deflection signal d51 prior to point t46, and after the maximum between time points t46 and t47.
  • the situation in stage B is in FIG. 4 schematically illustrated by situation s61.
  • the positive probe-sample interaction force causes the probe cantilever 12 to bend backward thereby providing the positive deflection signal d51 between points t45 and t47 in FIG. 3.
  • the probe 11 is at the Z-position corresponding with the level of axis a43 where the probe-sample interaction force is zero.
  • the probe 11 is further retracted from the surface 91 until the probe tip 13 will be released.
  • adhesive forces pull on the probe tip 13 to thereby exert a negative force on the probe tip 13 such that contact between the probe tip 13 and the sample surface 91 are maintained during retracting the probe. This part of the deflection signal is indicated by stage C.
  • stage C is illustrated by situation s62, showing the negative deflection of the probe tip 13 caused by adhesive forces between the surface 91 and probe tip 13.
  • the probe 11 has been retracted to such an extent that the balance between the adhesive forces and the forces exerted by the Z-actuator 60 can no longer be maintained.
  • the probe tip 13 is released from the surface 91 and starts vibrating at its Eigen frequency.
  • This stage D of the deflection signal d51 is called ringing and is schematically illustrated in FIG. 4 by situation s63. The ringing continues until it dies out and the probe as from time point t49 is in a relaxed state again corresponding to stage A, after which the next extension to the surface may commence.
  • the next extension already commences before the cantilever is in the relaxed state provided that the ringing amplitude has decreased below a predetermined threshold level.
  • the cantilever assumes the relaxed state before it has reached the surface.
  • the probe may move in a lateral direction relative to the sample 9 towards a next pixel to the image. This process repeats itself until all pixels have been imaged.
  • For each pixel x,y the value z(x,y) is registered so that a topographic image is obtained of the surface 91 of the sample 9.
  • the selection of the force threshold Ft(x,y) to be used by the motion profile generator 45 is determined by the signal processing unit 41.
  • the height profile z(x,y) of the surface is estimated from the position of the head and the deflection of the cantilever as discussed with reference to FIG. 3 and 4.
  • the motion profile generator retracts the probe if the deflection d indicates that the current force threshold Ft is exceeded.
  • the height profile estimated for a neighborhood for example z(x,y-Ay) is used as an indication of the height profile z(x,y) at the location x,y, and with this information an optimal force threshold Ft(x,y) is selected by the signal processing unit 41.
  • the selection of the optimal force threshold Ft(x,y) may be additionally or alternatively determined by prior knowledge of the sample, e.g. specified topography data and/or recipe creation data and/or analysis results obtained from a current scanline, i.e. from a neighborhood z(x-Ax, y)
  • the signal processing unit 41 determines the value for the force threshold Ft(x,y) on the basis of image data obtained for the previous scan line y-Ay having a corresponding x-coordinate or having an x coordinate in the region of the currently scanned coordinate x. In some embodiments not only the z-value is registered that is measured at the point in time that the force threshold is reached, but instead a complete force distance curve is registered specifying the relationship between the distance z and the applied force.
  • the force threshold Ft(x,y) for a position with lateral coordinates is selected from at least a relatively low threshold value Ftlow and a relatively high threshold value Fthigh dependent on z-values measured on a preceding scan-line (y-Ay) according to the following criterion.
  • the selection of the force threshold depends on a region having a width Ay defined by the distance to the preceding scanline and a length dx of a recently scanned portion of the current scanline as follows: zt)
  • a relatively high force threshold Ft(x,y) is selected for that position.
  • the relatively high force threshold Ft(x,y) facilitates a protruding of the tip to the bottom surface of such features. Hence, this selection improves measurement of features with a low z-value.
  • the force threshold Ft(x,y) is determined as: This implies, that if there is an indication, based on knowledge of a region of the current scan position (x,y) that a feature having a high z-value can be expected, a relatively low force threshold Ft(x,y) is selected for that position.
  • the relatively low force threshold Ft(x,y) aims to prevent that the tip slips of the feature with high z-value to a lower position. Hence, this selection improves measurement of features with a high z-value.
  • the width of the region may extend over several preceding scanlines.
  • the threshold force is adapted in accordance with material properties at a sample position x,y, based on prior information about the sample and/or information obtained from the sample during scanning a preceding or current scanline.
  • a relatively low threshold force is used if it is expected, based on prior information about the sample and/or information obtained from the sample during scanning, that the hardness of the surface at the location to be scanned is relatively low and a relatively high threshold force is used if it is expected that the hardness of the surface at the location to be scanned is relatively high.
  • the force threshold Ft(x,y) is determined by a selection from predetermined threshold values.
  • the force threshold is determined as a continuous function from prior information about the sample, for example using a polynomial function, for example an interpolation function e.g. a cubic interpolation function, to compute an interpolated threshold value for a location from a plurality of predetermined threshold values known at nearby locations.
  • a lookup table is used.
  • the determination of the force threshold Ft by the signal processing unit 41 may be additionally based on recently obtained imaging data from the current scanline y. For example, the signal processing unit 41 may overrule the decision made on the basis of a previous scanline y-Ay if the z-value z(x-Ax, y) determined for lateral position with coordinates x-Ax, y substantially deviates from the z-value z(x, y-Ay) determined for lateral position with coordinates x, y-Ay.
  • the signal processing unit 41 may compute an average value of a threshold value FtAx(x,y) determined based on imaging data from the current scanline and a threshold value FtAy(x,y) determined based on imaging data from the previous scanline with the expression:
  • FIG. 5 shows an alternative embodiment.
  • the signal processing unit 41 uses topographic information zs(x,y) stored in a topography memory unit 43, available from a specification or recipe of the sample 9.
  • the motion profile generator 45 and/or displacement sensor 21 provide the lateral coordinates x,y of the currently scanned position to the signal processing unit 41, so that the signal processing unit 41 can retrieve the expected z-value for that position zs(x,y) and/or expected z-values of neighboring positions from the topography memory unit 43 in order to determine the force threshold Ft(x,y) to be used by motion profile generator 45 for that lateral position x,y in a manner analogous as described for the embodiment in FIG. 2.
  • the process of determining the force threshold Ft(x,y) involves estimating uncertainties in the values involved in determining the threshold.
  • a different weight may be assigned to independent estimates of the force threshold using various approaches. Estimates having a high uncertainty, i.e. a low reliability are assigned a lower weight than estimates having a low uncertainty.
  • the force threshold Ft(x,y) to be used by motion profile generator 45 can then be determined by a weighted average of the various force threshold estimates in accordance with the assigned weights.
  • a threshold can be estimated on the basis of prior knowledge and topographic information obtained from previous scanlines and/or from preceding positions on the current scanline.
  • the determination of the force threshold Ft by the signal processing unit 41 may be additionally based on recently obtained imaging data from the current scanline y, as described above for the embodiment of FIG. 2.
  • the signal processing unit 41 is configured to determine the force threshold Ft(x,y) for a position with lateral coordinates x,y to be scanned based on a combination of topographic information zs(x,y) from a specification or recipe of the sample 9 as described with reference to FIG. 5 and topographic information z(x,y-Ay) obtained from a previous scanning line y-Ay as described with reference to FIG. 2.
  • the signal processing unit 41 is further configured to additionally incorporate recently obtained image data from the same scanline to determine the force threshold Ft(x,y) for a position with lateral coordinates x,y.
  • the computation of the threshold force is determined by signal processing unit 41 on the basis of information from a single position near the current scan point.
  • the computation may be based on a region of the current scan point x,y, for example information from a region x-dx ⁇ x’ ⁇ x+dx of the preceding scan line or information from a region of the current scan point specified in design data or recipe data, for example, a region x-dx ⁇ x’ ⁇ x+dx, y-dy ⁇ y’ ⁇ y+dy.
  • the signal processing unit 41 selects a relatively high force threshold if the information from the region indicates that the current scan point is expected to be within a narrow trench and selects a relatively low force threshold if the information from the region indicates a wide trench or other relatively flat area.
  • the current scan point is considered to be in a flat area if within a configurable distance (e.g. 10 times a diameter of the tip) the difference between a maximum surface level and a minimum surface level is less than a configurable factor (e.g. 0.5) times the height of the tip.
  • a configurable distance e.g. 10 times a diameter of the tip
  • a configurable factor e.g. 0.5
  • the configurable distance can be selected relatively small and the configurable factor relatively high. If the stiffness of the tip -cantilever combination is relatively low, the configurable distance can be selected relatively large and the configurable factor relatively small.
  • the imaging parameter to be adapted by the signal processing unit 41 is the force threshold Ft as a function of the lateral coordinates x,y
  • the imaging parameter to be adapted is a baseline offset, an approach profile or a retract profile.
  • FIG. 6 shows an exemplary embodiment, wherein the controller 40 comprises an adhesion signal processing unit 47 that determines a control signal dr(x,y) indicative for a retract distance of the retract profile to be used by the motion profile generator 45, i.e. the distance over which the motion profile generator 45 causes the z-actuator 60 to retract the probe 11 away from the sample 9.
  • a deflection curve signal processing unit 46 receives deflection curve data dz(x,y) for each scanned position.
  • the deflection curve data dz(x,y) is indicative for the deflection d measured as a function of the translation of the probe z, in particular the data indicating the deflection of the probe during the time interval from t47 to t48.
  • the deflection curve signal processing unit 46 estimates a magnitude Adh(x,y) of the adhesive forces at lateral position x,y of the sample and store the value in a memory 44.
  • the adhesion signal processing unit 47 retrieves the data obtained for the magnitude Adh(x,y-Ay) for the previous scan line x,y-Ay and based on the assumption that Adh(x,y) is approximately equal to Adh(x,y-Ay) computes an optimal retract distance for the retract profile.
  • the retract distance is set to a larger value than in the case a relatively low adhesion is expected.
  • the adhesion signal processing unit 47 performs the computation on the basis of information about the adhesion from a specification or recipe of the sample 9.
  • the adhesion signal processing unit 47 is configured to determine the retract distance of the retract profile for a position with lateral coordinates x,y to be scanned based on a combination of adhesion information from a specification or recipe of the sample 9 and information on adhesion obtained from a previous scan line y-Ay.
  • the adhesion signal processing unit 47 is further configured to additionally incorporate recently obtained adhesion information from the same scanline to determine the retract distance for a position with lateral coordinates x,y.
  • FIG. 7 shows a still further embodiment.
  • a deflection curve signal processing unit 48 receives deflection curve data dz(x,y) for each scanned position.
  • deflection curve signal processing unit 48 in this embodiment computes the force-distance data for lateral position (x,y) as determined in a time-interval wherein the force becomes positive after t45 until the point in time that the probe is retracted at t46.
  • the force distance data may comprise two or more distances z measured for respective forces.
  • the signal processing unit 41 has access to the force distance data and based thereon it determines which threshold force Ft(x,y) is to be selected for a lateral position x,y based on the two or more distances zl(x,y-Ay), z2(x,y-Ay) measured for respective forces stored for a lateral position having a coordinate x’ at or near the x,y-Ay.
  • the signal processing unit 41 additionally bases the computation of the threshold force Ft(x,y) on force distance data obtained from the current scan line, e.g. force distance data obtained from the previous scanned position x-Ax, y.
  • a setting of an imaging parameter may be determined on the basis of a combination of input data obtained from various sources, including two or more of a prior information about the sample obtained from design information, recipe information, information retrieved from imaging data of a previous scanline, information retrieved from recent imaging data of the current scanline, and the like.
  • a prior information about the sample obtained from design information including two or more of a prior information about the sample obtained from design information, recipe information, information retrieved from imaging data of a previous scanline, information retrieved from recent imaging data of the current scanline, and the like.
  • the prior information used for combining is consistent, this is an indication of their reliability.
  • a value of an input parameter used for predicting an imaging parameter to be set may be computed as the average value, e.g. a weighted average value, of the input data obtained from the various sources.
  • the setting of the imaging parameter may be computed on the basis of each of the input data obtained from the various sources, and the setting of that imaging parameter that is actually used may be computed as the average value, e.g. a weighted average value, of the settings computed on the basis of the various input data.
  • the setting of the input parameter is the most conservative one of the individually predicted settings based on each of the input data. For example, from multiple settings of the force threshold the one with the lowest value is selected to minimize risk of damage of the sample.
  • any reference signs shall not be construed as limiting the claim.
  • the term 'comprising' and ‘including’ when used in this description or the appended claims should not be construed in an exclusive or exhaustive sense but rather in an inclusive sense.
  • the expression ‘comprising’ as used herein does not exclude the presence of other elements or steps in addition to those listed in any claim.
  • the words ‘a’ and ‘an’ shall not be construed as limited to ‘only one’, but instead are used to mean ‘at least one’, and do not exclude a plurality.
  • Features that are not specifically or explicitly described or claimed may be additionally included in the structure of the invention within its scope.

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  • Radiology & Medical Imaging (AREA)
  • Length Measuring Devices With Unspecified Measuring Means (AREA)
PCT/NL2022/050755 2021-12-24 2022-12-23 Atomic force microscope (afm) device and method of operating the same Ceased WO2023121463A1 (en)

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KR1020247023015A KR20240129180A (ko) 2021-12-24 2022-12-23 원자힘 현미경(afm) 장치 및 그의 동작 방법
US18/709,243 US20250004010A1 (en) 2021-12-24 2022-12-23 Atomic force microscope (afm) device and method of operating the same
JP2024532950A JP2024546629A (ja) 2021-12-24 2022-12-23 原子間力顕微鏡(afm)装置及びその操作方法

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US20070018097A1 (en) * 2005-07-13 2007-01-25 Jeol Ltd. Scanning probe microscope and method of operating the same
US20170227577A1 (en) * 2013-12-07 2017-08-10 Bruker Nano, Inc. Force Measurement with Real-Time Baseline Determination
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