WO2023113699A3 - Multiphasic crystalline nanoparticles and methods of producing thereof - Google Patents

Multiphasic crystalline nanoparticles and methods of producing thereof Download PDF

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Publication number
WO2023113699A3
WO2023113699A3 PCT/SG2022/050915 SG2022050915W WO2023113699A3 WO 2023113699 A3 WO2023113699 A3 WO 2023113699A3 SG 2022050915 W SG2022050915 W SG 2022050915W WO 2023113699 A3 WO2023113699 A3 WO 2023113699A3
Authority
WO
WIPO (PCT)
Prior art keywords
multiphasic
mixture
present disclosure
producing
crystalline nanoparticle
Prior art date
Application number
PCT/SG2022/050915
Other languages
French (fr)
Other versions
WO2023113699A2 (en
Inventor
Kwan Wee Tan
Yun Li
Original Assignee
Nanyang Technological University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nanyang Technological University filed Critical Nanyang Technological University
Publication of WO2023113699A2 publication Critical patent/WO2023113699A2/en
Publication of WO2023113699A3 publication Critical patent/WO2023113699A3/en

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05Metallic powder characterised by the size or surface area of the particles
    • B22F1/054Nanosized particles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/16Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2998/00Supplementary information concerning processes or compositions relating to powder metallurgy
    • B22F2998/10Processes characterised by the sequence of their steps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites

Abstract

The present disclosure provides for a method of producing multiphasic crystalline nanoparticle(s), comprising: (a) preparing a mixture of at least two metal precursors and solvent; (b) applying the mixture to a substrate; and (c) subjecting the mixture to laser irradiation for a duration of about 0.1 ms to about 500 ms, at a power of about 0.1 W to about 20 W, wherein step (c) comprises laser irradiating a mixture which does not comprise pure metal. The present disclosure also provides for a multiphasic crystalline nanoparticle comprising at least four metals selected from the group consisting of Li, Be, Na, Mg, K, Ca, Rb, Sr, Ba, Fr, Ra, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Zr, Mo, Ru, Rh, Pd, Ag, Cd, W, Re, Os, Ir, Pt, Au, Hg, Nb, Ce, Al, Cs, Si, Ge, Sn, Pb and combinations thereof, and at least two phases/and or crystal structures selected from the group consisting of FCC, BCC, cubic rock salt, tetragonal, rutile tetragonal, hexagonal, orthorhombic, rhombohedral, monoclinic or triclinic crystal systems. The present disclosure further provides for a multiphasic crystalline nanoparticle disclosed herein, for use in inhibiting bacterial growth.
PCT/SG2022/050915 2021-12-16 2022-12-16 Multiphasic crystalline nanoparticles and methods of producing thereof WO2023113699A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
SG10202113963V 2021-12-16
SG10202113963V 2021-12-16

Publications (2)

Publication Number Publication Date
WO2023113699A2 WO2023113699A2 (en) 2023-06-22
WO2023113699A3 true WO2023113699A3 (en) 2023-09-14

Family

ID=86775366

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/SG2022/050915 WO2023113699A2 (en) 2021-12-16 2022-12-16 Multiphasic crystalline nanoparticles and methods of producing thereof

Country Status (1)

Country Link
WO (1) WO2023113699A2 (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20190161840A1 (en) * 2017-11-28 2019-05-30 University Of Maryland, College Park Thermal shock synthesis of multielement nanoparticles
TWI734605B (en) * 2020-09-04 2021-07-21 國立中央大學 High entropy nanomaterial and preparation method thereof
US20220121122A1 (en) * 2020-10-16 2022-04-21 Panasonic Factory Solutions Asia Pacific In-situ synthesis and deposition of high entropy alloy and multi metal oxide nano/micro particles by femtosecond laser direct writing

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20190161840A1 (en) * 2017-11-28 2019-05-30 University Of Maryland, College Park Thermal shock synthesis of multielement nanoparticles
TWI734605B (en) * 2020-09-04 2021-07-21 國立中央大學 High entropy nanomaterial and preparation method thereof
US20220121122A1 (en) * 2020-10-16 2022-04-21 Panasonic Factory Solutions Asia Pacific In-situ synthesis and deposition of high entropy alloy and multi metal oxide nano/micro particles by femtosecond laser direct writing

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
LI YUN, TAY YEE YAN, BUENCONSEJO PIO J. S., MANALASTAS WILLIAM, TU WEI HAN, LIM HONG KIT, SALIM TEDDY, THOMPSON MICHAEL O., MADHAV: "Laser Annealing‐Induced Phase Transformation Behaviors of High Entropy Metal Alloy, Oxide, and Nitride Nanoparticle Combinations", ADVANCED FUNCTIONAL MATERIALS, WILEY - V C H VERLAG GMBH & CO. KGAA, DE, vol. 33, no. 13, 1 March 2023 (2023-03-01), DE , XP093092252, ISSN: 1616-301X, DOI: 10.1002/adfm.202211279 *
SHAH RUPAL R., KAEWGUN SUJAREE, LEE BURTRAND I., TZENG TZUEN-RONG J.: "The Antibacterial Effects of Biphasic Brookite-Anatase Titanium Dioxide Nanoparticles on Multiple-Drug-Resistant Staphylococcus aureus", JOURNAL OF BIOMEDICAL NANOTECHNOLOGY, AMERICAN SCIENTIFIC PUBLISHERS, US, vol. 4, no. 3, 1 September 2008 (2008-09-01), US , pages 339 - 348, XP009548792, ISSN: 1550-7033, DOI: 10.1166/jbn.2008.324 *

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Publication number Publication date
WO2023113699A2 (en) 2023-06-22

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