WO2022230886A1 - Tobacco sheet for non-combustion heating-type fragrance inhaler and method for manufacturing same, non-combustion heating-type fragrance inhaler, and non-combustion heating-type fragrance inhaling system - Google Patents

Tobacco sheet for non-combustion heating-type fragrance inhaler and method for manufacturing same, non-combustion heating-type fragrance inhaler, and non-combustion heating-type fragrance inhaling system Download PDF

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Publication number
WO2022230886A1
WO2022230886A1 PCT/JP2022/018913 JP2022018913W WO2022230886A1 WO 2022230886 A1 WO2022230886 A1 WO 2022230886A1 JP 2022018913 W JP2022018913 W JP 2022018913W WO 2022230886 A1 WO2022230886 A1 WO 2022230886A1
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WO
WIPO (PCT)
Prior art keywords
tobacco
sheet
flavor
combustion heating
mass
Prior art date
Application number
PCT/JP2022/018913
Other languages
French (fr)
Japanese (ja)
Inventor
明弘 小出
公隆 打井
大輔 南條
萌夏 永山
克典 村越
哲朗 澁谷
悠衣 中山
俊輔 横手
真樹 六川
創 西野
Original Assignee
日本たばこ産業株式会社
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 日本たばこ産業株式会社 filed Critical 日本たばこ産業株式会社
Priority to CN202280030532.2A priority Critical patent/CN117241683A/en
Priority to JP2023517562A priority patent/JPWO2022230886A1/ja
Priority to EP22795799.0A priority patent/EP4331389A1/en
Priority to KR1020237040043A priority patent/KR20240000551A/en
Publication of WO2022230886A1 publication Critical patent/WO2022230886A1/en
Priority to US18/493,162 priority patent/US20240049767A1/en

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/12Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
    • A24B15/14Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/32Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/36Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring
    • A24B15/40Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms
    • A24B15/403Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms having only oxygen as hetero atoms
    • A24B15/406Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a heterocyclic ring having only oxygen or sulfur as hetero atoms having only oxygen as hetero atoms in a five-membered ring
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00Cigars; Cigarettes
    • A24D1/20Cigarettes specially adapted for simulated smoking devices
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/20Devices using solid inhalable precursors
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40Constructional details, e.g. connection of cartridges and battery parts
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20Macromolecular organic compounds
    • D21H17/21Macromolecular organic compounds of natural origin; Derivatives thereof
    • D21H17/23Lignins

Definitions

  • the present invention relates to a tobacco sheet for a non-combustion heating flavor inhaler, a manufacturing method thereof, a non-combustion heating flavor inhaler, and a non-combustion heating flavor inhalation system.
  • a combustion-type flavor inhaler obtains flavor by burning tobacco fillings including leaf tobacco and tobacco sheets.
  • Patent Literature 1 discloses a tobacco sheet used in a combustion type flavor inhaler.
  • a non-combustion heating type flavor inhaler has been proposed that obtains flavor by heating a flavor source such as a tobacco sheet instead of burning it.
  • the heating temperature of the non-combustion heating type flavor inhaler is lower than the combustion temperature of the combustion type flavor inhaler, for example, about 400° C. or less.
  • an aerosol generating agent can be added to the flavor source in the non-combustion heating type flavor inhaler from the viewpoint of increasing the amount of smoke.
  • the aerosol-generating agent is vaporized by heating to generate an aerosol. Since the aerosol is supplied to the user together with flavor components such as tobacco components, the user can obtain sufficient flavor.
  • a non-combustion heating flavor inhaler can comprise, for example, a tobacco-containing segment filled with tobacco sheets or the like, a cooling segment, and a filter segment.
  • the axial length of the tobacco-containing segment of the non-combustion-heating flavor inhaler is generally shorter than the axial length of the tobacco-containing segment of the normal combustion-type flavor inhaler in relation to the heating heater. Therefore, in the non-combustion heating type flavor inhaler, a large amount of tobacco sheets are filled in the short tobacco-containing segments in order to secure the amount of aerosol generated during heating.
  • non-combustion heating type flavor inhalers usually use tobacco sheets with low swelling, that is, high density tobacco sheets.
  • the swelling property is a value indicating the volume of a tobacco sheet having a predetermined mass when notches are compressed under a constant pressure for a certain period of time.
  • the present inventors believe that if a tobacco sheet with low swelling (high density) is used, the total heat capacity of the tobacco-containing segment increases. It was found that the tobacco sheet filled in the tobacco-containing segment does not sufficiently contribute to the generation of aerosol depending on the heating method and the capacity of the heater. In order to solve this problem, it is conceivable to reduce the total heat capacity of the tobacco-containing segment.
  • the present inventors (1) reduce the specific heat of the tobacco raw material contained in the tobacco sheet, and (2) use a highly bulky (low-density) tobacco sheet. I considered using it. However, as for (1), it is difficult to reduce the specific heat of the tobacco raw material itself, so it was considered effective to reduce the total heat capacity of the tobacco-containing segment by (2). Therefore, it is desired to develop a highly bulky (low density) tobacco sheet suitable for non-combustion heating type flavor inhalers.
  • An object of the present invention is to provide a highly bulky non-combustion heating flavor inhaler tobacco sheet, a non-combustion heating flavor inhaler including the tobacco sheet, and a non-combustion heating flavor inhalation system.
  • a tobacco sheet for a non-combustion heating type flavor inhaler comprising a tobacco raw material, the tobacco sheet having a wavy cross section in the thickness direction of the tobacco sheet.
  • Aspect 2 The tobacco sheet for non-combustion heated flavor inhalers according to aspect 1, further comprising fructans.
  • Aspect 3 The tobacco sheet for non-combustion heating flavor inhalers according to aspect 1 or 2, wherein the fructan is selected from the group consisting of inulin-type fructans, levan-type fructans, branched fructans, fructooligosaccharides, and mixtures thereof.
  • Aspect 4 further comprising a saturated fatty acid additive, said additive is selected from the group consisting of saturated fatty acids having a molar mass of 200-350 g/mol, esters of said saturated fatty acids, and combinations thereof; The content is 0.01 to 3% by weight based on the dry matter content of the sheet.
  • a tobacco sheet for a non-combustion heating type flavor inhaler according to any one of aspects 1 to 3.
  • Aspect 5 The tobacco sheet for a non-combustion heating type flavor inhaler according to aspect 4, wherein the saturated fatty acid and the saturated fatty acid ester are each a single item.
  • Aspect 6 as a filling, A sheet according to any one of aspects 1 to 5; including paper and The total content of lignin and hemicellulose in the paper is 0.1 to 10% by mass, Tobacco-containing segment.
  • Aspect 7 as a filling, A sheet according to any one of aspects 1 to 5; a paper containing an aerosol-generating agent; Tobacco-containing segment.
  • Aspect 8 A tobacco-containing segment comprising the tobacco sheet for a non-combustion heating flavor inhaler according to any one of aspects 1 to 5;
  • Aspect 9 A non-combustion heated flavor inhaler according to aspect 8; a heating device for heating the tobacco-containing segment; A non-combustion heated flavor suction system.
  • a method for producing a tobacco sheet for a non-combustion heating type flavor inhaler comprising: preparing a mixture comprising a tobacco raw material, an aerosol-generating agent, a first shaping agent and a second shaping agent; rolling the mixture to form a rolled article; A step of pressing a rotary roll blade against the rolled product to cut it into strips while imparting a corrugated shape; optionally adding the fructan to the rolled product; How to prepare.
  • a method for producing a tobacco sheet for a non-combustion heating type flavor inhaler comprising: preparing a mixture comprising a tobacco raw material, an aerosol-generating agent, a first molding agent and a second molding agent, and a saturated fatty acid-based additive; rolling the mixture to form a rolled article; A step of pressing a rotary roll blade against the rolled product to cut it into strips while imparting a corrugated shape; How to prepare.
  • the present invention it is possible to provide a highly bulky non-combustion heating flavor inhaler tobacco sheet, a non-combustion heating flavor inhaler including the tobacco sheet, and a non-combustion heating flavor inhalation system.
  • FIG. 1 is a cross-sectional view in the thickness direction showing an example of a tobacco sheet according to this embodiment;
  • FIG. It is a sectional view showing an example of a non-combustion heating type flavor inhaler concerning this embodiment.
  • An example of the non-combustion heating flavor inhalation system according to the present embodiment in which (a) the state before the non-combustion heating flavor inhaler is inserted into the heating device, and (b) the non-combustion heating flavor inhaler is heated.
  • It is sectional drawing which shows the state which inserts into an apparatus and heats.
  • 1 is a diagram showing one aspect of a tobacco segment;
  • FIG. 1 is a diagram showing one aspect of a tobacco segment;
  • FIG. 1 is a diagram showing one aspect of a tobacco segment;
  • FIG. 1 is a diagram showing one aspect of a tobacco segment;
  • FIG. 1 is a diagram showing one aspect of a tobacco segment
  • FIG. 1 is a diagram showing one aspect of a tobacco segment
  • FIG. 1 is a graph showing the relationship between the content (% by mass) of inulin-type fructan or fructose and the sensory evaluation (flavor or flavor inhibition) in Reference Examples.
  • Fig. 2 is a graph showing the relationship between the content (% by mass) of inulin-type fructan or fructose and the persistence of inhibitory effect on flavor and taste inhibition in Reference Examples.
  • a tobacco sheet for a non-combustion heating type flavor inhaler (hereinafter also referred to as a "tobacco sheet") according to the present embodiment contains tobacco raw material, and has a wavy cross-section in the thickness direction of the tobacco sheet. Since the tobacco sheet according to the present embodiment has a corrugated cross-sectional shape in the thickness direction, it is bulky and has a high swelling property. Therefore, by using the tobacco sheet according to the present embodiment, the total heat capacity of the tobacco-containing segment can be reduced, and the tobacco sheet filled in the tobacco-containing segment can sufficiently contribute to aerosol generation.
  • the tobacco sheet according to the present embodiment preferably further contains an aerosol-generating agent and one or more molding agents. improve more.
  • the tobacco sheet according to this embodiment has a wavy cross section in the thickness direction. That is, when the tobacco sheet according to the present embodiment is cut in the thickness direction in one plane direction, the cross section has a corrugated shape.
  • the plane direction may be, for example, the longitudinal direction or the lateral direction of the tobacco sheet.
  • the “wavy shape” is not particularly limited as long as it has a shape that undulates vertically, and the crests of the waves may have a straight shape or a curved shape. Also, the waves may be regular or irregular.
  • Fig. 1 shows an example of the cross-sectional shape in the thickness direction of the tobacco sheet according to this embodiment.
  • the tobacco sheet 1 shown in FIG. 1 has waves 2 in a cross-section in the thickness direction.
  • the width w1 of the wave 2 is not particularly limited, it is preferably within the range of 0.1 to 10.0 mm.
  • the height w2 of the wave 2 is not particularly limited, but is preferably within the range of 0.1 to 5.0 mm.
  • the thickness w3 of the tobacco sheet 1 is preferably within the range of 100-1000 ⁇ m.
  • the waves 2 may have a sawtooth shape 3 .
  • the size of the tobacco sheet according to the present embodiment in the planar direction is not particularly limited, but may be, for example, length: 5.0 to 40.0 mm and width: 0.5 to 2.0 mm.
  • the tobacco raw material contained in the tobacco sheet according to the present embodiment is not particularly limited as long as it contains tobacco components, and examples thereof include tobacco powder and tobacco extract.
  • Tobacco powder includes, for example, leaf tobacco, core bones, residual stems, and the like. These may be used alone or in combination of two or more. By chopping these into a predetermined size, they can be used as tobacco powder.
  • the size of the tobacco powder it is preferable that the cumulative 90% particle size (D90) in the volume-based particle size distribution measured by the dry laser diffraction method is 200 ⁇ m or more from the viewpoint of further improving the swelling property.
  • the tobacco powder content in 100% by mass of the tobacco sheet is preferably 45 to 95% by mass, more preferably 50 to 93% by mass, and more preferably 60 to 85% by mass. % is more preferred.
  • the tobacco extract for example, leaf tobacco is crushed, mixed and stirred with a solvent such as water to extract a water-soluble component from the leaf tobacco, and the resulting water extract is dried under reduced pressure and concentrated. Tobacco extracts obtained may be mentioned.
  • the tobacco sheet according to this embodiment preferably further contains an aerosol-generating agent.
  • Aerosol-generating agents include, for example, glycerin, propylene glycol, 1,3-butanediol and the like. These may be used alone or in combination of two or more.
  • the ratio of the aerosol-generating agent contained in 100% by mass of the tobacco sheet is preferably 4 to 50% by mass.
  • the proportion of the aerosol-generating agent is 4% by mass or more, sufficient aerosol can be generated during heating from the viewpoint of quantity.
  • the proportion of the aerosol generating agent is 50% by mass or less, sufficient aerosol can be generated during heating from the viewpoint of heat capacity.
  • the proportion of the aerosol generating agent is more preferably 6 to 40% by mass, even more preferably 8 to 30% by mass, and particularly preferably 10 to 20% by mass.
  • the tobacco sheet according to the present embodiment preferably further contains a molding agent from the viewpoint of shape retention.
  • the tobacco sheet according to the present embodiment has the first molding agent and the second molding agent from the viewpoint of being able to sufficiently achieve both the retention performance of the aerosol generating agent and the retention performance of the corrugated shape of the tobacco sheet.
  • the first molding agent and the second molding agent may be of different types, or the types of molding agents may be the same but the forms may be different.
  • the first molding agent include polysaccharides, proteins, synthetic polymers and the like. Examples of polysaccharides include cellulose derivatives and naturally occurring polysaccharides.
  • Cellulose derivatives include, for example, cellulose ethers such as methylcellulose, ethylcellulose, hydroxyethylcellulose, hydroxymethylethylcellulose, hydroxypropylcellulose, hydroxypropylmethylcellulose, benzylcellulose, tritylcellulose, cyanoethylcellulose, carboxymethylcellulose, carboxyethylcellulose, aminoethylcellulose; Organic acid esters such as cellulose, cellulose formate, cellulose propionate, cellulose butyrate, cellulose benzoate, cellulose phthalate, and tosyl cellulose; and inorganic acid esters such as cellulose nitrate, cellulose sulfate, cellulose phosphate, and cellulose xanthate. be done.
  • cellulose ethers such as methylcellulose, ethylcellulose, hydroxyethylcellulose, hydroxymethylethylcellulose, hydroxypropylcellulose, hydroxypropylmethylcellulose, benzylcellulose, tritylcellulose
  • Naturally-derived polysaccharides include guar gum, tara gum, roasted bean gum, tamarind seed gum, pectin, arabic gum, tragacanth gum, karaya gum, gutti gum, arabinogalactan, amaseed gum, cascha gum, psyllium seed gum, and mugwort seed gum.
  • plant-derived polysaccharides agar, alginic acid, propylene glycol alginate, furcelleran, algae-derived polysaccharides such as fukuronori extract; xanthan gum, gellan gum, curdlan, pullulan, Agrobacterium succinoglycan, welan gum, macro Microorganism-derived polysaccharides such as homopsis gum and rhamzan gum; crustacean-derived polysaccharides such as chitin, chitosan, and glucosamine; and starches such as starch, sodium starch glycolate, pregelatinized starch, and dextrin.
  • proteins examples include grain proteins such as wheat gluten and rye gluten.
  • Synthetic polymers include, for example, polyphosphoric acid, sodium polyacrylate, polyvinylpyrrolidone, and the like.
  • the second molding agent although different from the first molding agent, the same polysaccharides, proteins, synthetic polymers, etc. as those of the first molding agent can be used.
  • the ratio of the first molding agent contained in 100% by mass of the tobacco sheet is preferably 0.1 to 15% by mass.
  • the ratio of the first molding agent is 0.1% by mass or more, the raw material mixture can be easily molded into a sheet. Further, since the ratio of the first molding agent is 15% by mass or less, it is possible to sufficiently use other raw materials for securing the functions required for the tobacco-containing segment of the non-combustion heating type flavor inhaler.
  • the proportion of the first molding agent is more preferably 0.1 to 12% by mass, even more preferably 0.1 to 10% by mass, particularly 0.1 to 7% by mass. preferable.
  • the ratio of the second molding agent contained in 100% by mass of the tobacco sheet is preferably 0.1 to 15% by mass.
  • the ratio of the second molding agent is 0.1% by mass or more, the raw material mixture can be easily molded into a sheet. Further, since the ratio of the second molding agent is 15% by mass or less, it is possible to sufficiently use other raw materials for securing the functions required for the tobacco-containing segment of the non-combustion heating type flavor inhaler.
  • the proportion of the second molding agent is more preferably 0.1 to 12% by mass, even more preferably 0.1 to 10% by mass, particularly 0.1 to 7% by mass. preferable.
  • the first molding agent and the second molding agent are the same type of molding agent but different in form
  • the first molding agent may be powder and the second molding agent may be solution or slurry.
  • a molding agent is directly mixed as a powder as a first molding agent, and a molding agent is dispersed or swollen in a solvent such as water and mixed as a second molding agent. can be done.
  • a solvent such as water
  • the tobacco sheet according to this embodiment may further contain a reinforcing agent from the viewpoint of further improving physical properties.
  • a reinforcing agent include fibrous substances such as fibrous pulp and fibrous synthetic cellulose, and liquid substances such as pectin suspension having a surface coating function that forms a film when dried. These may be used alone or in combination of two or more.
  • the proportion of the reinforcing agent contained in 100% by mass of the tobacco sheet is preferably 4 to 40% by mass. Within this range, other raw materials can be sufficiently used to secure the functions required for the tobacco-containing segment of the non-combustion-heating flavor inhaler.
  • the ratio of the reinforcing agent is more preferably 4.5 to 35% by mass, more preferably 5 to 30% by mass.
  • the tobacco sheet according to this embodiment may further contain a humectant from the viewpoint of maintaining quality.
  • moisturizing agents include sugar alcohols such as sorbitol, erythritol, xylitol, maltitol, lactitol, mannitol, and reduced maltose starch syrup. These may be used alone or in combination of two or more.
  • the ratio of the humectant contained in 100% by mass of the tobacco sheet is preferably 1 to 15% by mass. Within this range, other raw materials can be sufficiently used to secure the functions required for the tobacco-containing segment of the non-combustion-heating flavor inhaler.
  • the ratio of the moisturizing agent is more preferably 2 to 12% by mass, even more preferably 3 to 10% by mass.
  • the tobacco sheet according to the present embodiment may contain, in addition to the tobacco raw material, the aerosol-generating agent, the molding agent (first and second molding agents), the reinforcing agent, and the moisturizing agent, if necessary, a flavoring agent and a flavoring agent.
  • Flavoring agents such as seasonings, coloring agents, humectants, preservatives, diluents such as inorganic substances, and the like can be included.
  • the tobacco sheet according to the present embodiment has a swelling property of 190 cc/100 g or more.
  • the swelling property is 190 cc/100 g or more, the total heat capacity of the tobacco-containing segment of the non-combustion heating type flavor inhaler can be sufficiently reduced, and the tobacco sheet filled in the tobacco-containing segment is generated by aerosol generation. be able to contribute.
  • the swelling property is more preferably 210 cc/100 g or more, more preferably 230 cc/100 g or more.
  • the upper limit of the swelling range is not particularly limited, it can be, for example, 800 cc/100 g or less.
  • the swelling property was evaluated by cutting a tobacco sheet into a size of 0.8 mm ⁇ 20 mm, leaving it in a conditioned room at 22° C. and 60% for 48 hours, and applying it to DD-60A (trade name, manufactured by Borgwald). It is a value measured by The measurement is carried out by placing 15 g of cut tobacco sheets in a cylindrical container with an inner diameter of 60 mm and compressing the container with a load of 3 kg for 30 seconds to obtain the volume.
  • the tobacco sheet according to the present embodiment is produced by, for example, preparing a mixture containing a tobacco raw material, an aerosol-generating agent, a first molding agent, and a second molding agent, and rolling the mixture to form a rolled product. and a step of pressing a rotary roll blade against the rolled product to cut it into strips and imparting a corrugated shape. Note that the process of imparting a wave shape is also called a rippling process.
  • the tobacco sheet according to this embodiment can be produced by the following method.
  • a sheet cut into strips by a rotary roll blade is given a wavy shape and sawtooth shape as shown in FIG.
  • the rolled product is not cut by a rotary roll blade, for example, by peeling off the rolled product on the rolling roller with a doctor knife, resistance is applied when peeled from the roll, and the wavy shape is also applied. and a sawtooth shape.
  • the surface of the pressure roller may be heated or cooled, and the number of revolutions of the pressure roller may be adjusted depending on the purpose. Furthermore, by adjusting the spacing between the rolling rollers, it is possible to obtain a tobacco sheet with a desired basis weight.
  • the non-combustion-heating flavor inhaler according to this embodiment includes a tobacco-containing segment including the tobacco sheet or the like according to this embodiment. Since the non-combustion-heating flavor inhaler according to the present embodiment includes the tobacco-containing segment filled with the highly bulky tobacco sheet or the like according to the present embodiment, the total heat capacity of the tobacco-containing segment should be sufficiently reduced. , allowing the tobacco sheet filled in the tobacco-containing segment to contribute more to aerosol generation.
  • the non-combustion heating type flavor inhaler 4 shown in FIG. It comprises a segment 7 and a filter segment 8 .
  • the non-combustion-heating flavor inhaler according to this embodiment may have segments other than the tobacco-containing segment, cooling segment, center hole segment, and filter segment.
  • the axial length of the non-combustion heating type flavor inhaler according to the present embodiment is not particularly limited, but is preferably 40 mm or more and 90 mm or less, more preferably 50 mm or more and 75 mm or less, 50 mm or more, It is more preferably 60 mm or less.
  • the circumference of the non-combustion heating flavor inhaler is preferably 16 mm or more and 25 mm or less, more preferably 20 mm or more and 24 mm or less, and even more preferably 21 mm or more and 23 mm or less.
  • the length of the tobacco-containing segment is 20 mm
  • the length of the cooling segment is 20 mm
  • the length of the center hole segment is 8 mm
  • the length of the filter segment is 7 mm.
  • the length of the filter segment can be selected within a range of 4 mm or more and 10 mm or less.
  • the ventilation resistance of the filter segments at that time is selected to be 15 mmH 2 O/seg or more and 60 mmH 2 O/seg or less per segment.
  • the tobacco sheet according to the present embodiment is filled in wrapping paper (hereinafter also referred to as wrapper).
  • wrapper The method of packing the tobacco sheet into the wrapping paper is not particularly limited.
  • the tobacco sheet may be wrapped in a wrapper, or the tobacco sheet may be packed in a cylindrical wrapper.
  • the shape of the tobacco sheet has a longitudinal direction such as a rectangular shape, the tobacco sheet may be packed so that the longitudinal direction is in an unspecified direction in the wrapper, and the tobacco-containing segment 5 may be packed in an axial direction or a longitudinal direction. They may be aligned and filled in a direction perpendicular to the axial direction.
  • the cooling segment 6 may be configured by a cylindrical member 10.
  • the tubular member 10 may be, for example, a paper tube formed by processing cardboard into a cylindrical shape.
  • the tubular member 10 and the mouthpiece lining paper 15, which will be described later, are provided with perforations 11 penetrating both. Due to the presence of the perforations 11 outside air is introduced into the cooling segment 6 during suction. As a result, the vaporized aerosol component generated by heating the tobacco-containing segment 5 comes into contact with the outside air, and its temperature decreases, liquefying to form an aerosol.
  • the diameter (spanning length) of the perforations 11 is not particularly limited, but may be, for example, 0.5 mm or more and 1.5 mm or less.
  • the number of perforations 11 is not particularly limited, and may be one or two or more. For example, a plurality of perforations 11 may be provided on the circumference of the cooling segment 6 .
  • the amount of outside air introduced from the perforations 11 is preferably 85% by volume or less, more preferably 80% by volume or less, relative to the total volume of the gas inhaled by the user.
  • the ratio of the amount of outside air is 85% by volume or less, it is possible to sufficiently suppress reduction in flavor due to dilution by outside air.
  • this is also called a ventilation ratio.
  • the lower limit of the ventilation ratio range is preferably 55% by volume or more, more preferably 60% by volume or more.
  • the cooling segment may also be a segment comprising a crumpled, pleated, gathered or folded sheet of suitable construction material.
  • the cross-sectional profile of such elements may exhibit randomly oriented channels.
  • the cooling segment may also include a bundle of longitudinally extending tubes.
  • Such cooling segments may be formed, for example, from pleated, gathered, or folded sheet material wrapped with wrapping paper.
  • the axial length of the cooling segment can be, for example, 7 mm or more and 28 mm or less, and can be, for example, 18 mm.
  • the cooling segment can be substantially circular in its axial cross-sectional shape, and its diameter can be, for example, 5 mm or more and 10 mm or less, and can be, for example, about 7 mm.
  • the center hole segment is composed of a filling layer having one or more hollow portions and an inner plug wrapper (inner wrapping paper) covering the filling layer.
  • the center hole segment 7 is composed of a second filling layer 12 having a hollow portion and a second inner plug wrapper 13 covering the second filling layer 12 .
  • the center hole segment 7 has the function of increasing the strength of the mouthpiece segment 9 .
  • the second filling layer 12 has an inner diameter of ⁇ 1.0 mm, for example, filled with cellulose acetate fibers at a high density and hardened by adding a plasticizer containing triacetin in an amount of 6% by mass or more and 20% by mass or less based on the mass of cellulose acetate.
  • the second packed layer 12 has a high packing density of fibers, air and aerosol flow only through the hollow portion and hardly flow inside the second packed layer 12 during suction. Since the second filling layer 12 inside the center hole segment 7 is a fiber filling layer, the feeling of touch from the outside during use hardly causes the user to feel uncomfortable. Note that the center hole segment 7 may not have the second inner plug wrapper 13 and may retain its shape by thermoforming.
  • the configuration of the filter segment 8 is not particularly limited, it may be composed of a single or a plurality of packed layers. The outer side of the packing layer may be wrapped with one or more wrapping papers.
  • the ventilation resistance per segment of the filter segment 8 can be appropriately changed depending on the amount of filler, the material, etc. with which the filter segment 8 is filled. For example, when the filler is cellulose acetate fiber, increasing the amount of cellulose acetate fiber with which the filter segment 8 is filled can increase the ventilation resistance. When the filler is cellulose acetate fiber, the packing density of the cellulose acetate fiber can be 0.13-0.18 g/cm 3 .
  • the airflow resistance is a value measured by an airflow resistance measuring instrument (trade name: SODIMAX, manufactured by SODIM).
  • the length of the circumference of the filter segment 8 is not particularly limited, it is preferably 16 to 25 mm, more preferably 20 to 24 mm, even more preferably 21 to 23 mm.
  • the axial length of the filter segment 8 can be selected from 4 to 10 mm, and is selected so that its ventilation resistance is from 15 to 60 mmH 2 O/seg.
  • the axial length of the filter segment 8 is preferably 5-9 mm, more preferably 6-8 mm.
  • the cross-sectional shape of the filter segment 8 is not particularly limited, but may be, for example, circular, elliptical, polygonal, or the like.
  • the filter segment 8 may be directly added with destructible capsules containing perfume, perfume beads, and perfume.
  • the center hole segment 7 and the filter segment 8 can be connected with an outer plug wrapper (outer wrapping paper) 14 .
  • the outer plug wrapper 14 can be, for example, a cylinder of paper.
  • the tobacco-containing segment 5 , cooling segment 6 , connected center hole segment 7 and filter segment 8 can be connected by mouthpiece lining paper 15 .
  • These connections can be made, for example, by applying glue such as vinyl acetate glue to the inner surface of the mouthpiece lining paper 15, inserting the three segments, and winding them.
  • these segments may be divided into multiple times and connected with multiple lining papers.
  • the non-combustion heating flavor inhalation system includes the non-combustion heating flavor inhaler according to this embodiment, and a heating device that heats the tobacco-containing segment of the non-combustion heating flavor inhaler.
  • the non-combustion-heating flavor inhalation system according to the present embodiment may have a configuration other than the non-combustion-heating flavor inhaler and the heating device according to the present embodiment.
  • the non-combustion heating flavor inhalation system shown in FIG. 3 includes a non-combustion heating flavor inhaler 4 according to this embodiment and a heating device 16 that heats the tobacco-containing segment of the non-combustion heating flavor inhaler 4 from the outside. Prepare.
  • FIG. 3(a) shows the state before the non-combustion heating flavor inhaler 4 is inserted into the heating device 16, and FIG. indicates the state of
  • the heating device 16 shown in FIG. 3 includes a body 17, a heater 18, a metal tube 19, a battery unit 20, and a control unit 21.
  • the body 17 has a cylindrical recess 22, and a heater 18 and a metal pipe are provided on the inner side surface of the recess 22 at positions corresponding to the tobacco-containing segments of the non-combustion heating flavor inhaler 4 inserted into the recess 22. 19 are arranged.
  • the heater 18 can be a heater based on electric resistance, and electric power is supplied from the battery unit 20 according to an instruction from the control unit 21 that performs temperature control, and the heater 18 is heated. The heat emitted from the heater 18 is transmitted to the tobacco-containing segment of the non-combustion heating flavor inhaler 4 through the metal pipe 19 with high thermal conductivity.
  • FIG. 3(b) there is a gap between the outer circumference of the non-combustion-heating flavor inhaler 4 and the inner circumference of the metal tube 19 because it is schematically illustrated.
  • the heating device 16 heats the tobacco-containing segment of the non-combustion-heating flavor inhaler 4 from the outside, but it may heat the tobacco-containing segment from the inside.
  • the heating temperature of the heating device is not particularly limited, it is preferably 400°C or lower, more preferably 150°C or higher and 400°C or lower, and even more preferably 200°C or higher and 350°C or lower.
  • the heating temperature indicates the temperature of the heater of the heating device.
  • non-combustion heating type flavor inhalers are required to reduce the sense of flavor inhibition (irritation) or discomfort.
  • the sense of inhibition of flavor and taste means irritation to the oral cavity and throat upon inhalation.
  • a tobacco sheet for a non-combustion heating type flavor inhaler with reduced sense of inhibition of flavor and taste or discomfort will be described.
  • the tobacco sheet for a non-combustion heating type flavor inhaler contains fructans.
  • the fructans are thermally decomposed to generate a persistent sweet aroma.
  • the persistent sweet aroma that is generated can continue from the early stage to the late stage of smoking behavior and suppress the feeling of inhibition of flavor and taste.
  • the above fructans are not particularly limited, but inulin-type fructans, levan-type fructans, branched fructans, fructooligosaccharides, or a combination of two or more of these can be used. Among these, inulin-type fructans are preferable from the viewpoint of cost reduction.
  • fructan of this embodiment has the following characteristics when it produces a sweet aroma through caramelization reaction.
  • Fructans are formed by binding multiple monosaccharides and have a larger molecular structure than monosaccharides and disaccharides. Therefore, when fructans undergo a caramelization reaction, they are decomposed into relatively small sugar molecules such as monosaccharides and disaccharides, and then these monosaccharides and disaccharides undergo a caramelization reaction to generate a sweet aroma. It is thought that it goes through a multi-stage decomposition process. On the other hand, when monosaccharides and disaccharides undergo a caramelization reaction, it is believed that these sugars undergo a caramelization reaction to directly generate a sweet aroma.
  • fructans are considered to be able to generate a sweet aroma at a slower rate due to the increased number of decomposition processes, and to generate a sweet aroma over a long period of time.
  • the inhibition of flavor and taste can be suppressed continuously from the early stage to the late stage of smoking behavior due to such characteristics related to the caramelization reaction of fructans.
  • the fructan content relative to 100% by mass of the tobacco sheet is not particularly limited, but is 0.1 to 5% by mass, 0.3 to 3.5% by mass, or 0.5 to 3% by mass. %.
  • the fructan content is preferably as high as possible.
  • the fructan content is 0.5 to 0.5. 3% by weight is preferred.
  • the tobacco raw material can further include tobacco leaves, aged tobacco leaves, processed tobacco leaves, tobacco fillers, non-tobacco materials, or a combination of two or more of these.
  • Tobacco leaves is a general term for harvested tobacco leaves before undergoing ripening, which will be described later.
  • One mode of aging includes curing.
  • aged tobacco leaves before being processed into various forms used in tobacco products are referred to as “aged tobacco leaves.” ”.
  • processed tobacco leaves processed into various forms used in tobacco products are referred to as “processed tobacco leaves”.
  • tobacco in which matured tobacco leaves are chopped into a predetermined size
  • tobacco sheet obtained by molding a composition containing matured tobacco leaves pulverized to a predetermined particle size (hereinafter also referred to as "tobacco fine powder") into a sheet shape
  • tobacco fine powder a composition containing matured tobacco leaves pulverized to a predetermined particle size
  • Mention may also be made of "tobacco granules” obtained by molding into granular form.
  • tobacco powder is also one form of processed tobacco leaves.
  • Non-tobacco materials include plant roots (including scales (bulbs), tuberous roots (potatoes), bulbs, etc.), stems, tubers, skins (including stem bark, bark, etc.), leaves, flowers (petals, pistils, etc.). , stamens, etc.), seeds, or tree trunks and branches.
  • the manufacturing method of tobacco sheets containing fructans is not limited. In some embodiments of the present application, it can be manufactured by preparing the tobacco sheets described above and supplying fructans from the outside. Specifically, it is preferable to supply fructans to the rolled product.
  • the roll-formed article may be before or after being given the corrugated shape.
  • the tobacco sheet for a non-combustion heating type flavor inhaler contains a saturated fatty acid additive.
  • the tobacco sheet may contain materials derived from Orient species.
  • the content of the material derived from the Orient species is preferably 10% by mass or less with respect to the tobacco raw material.
  • the upper limit of the content is preferably 8% by mass or less, more preferably 5% by mass or less.
  • the lower limit is preferably 0.1% by mass or more, more preferably 2% by mass or more, and still more preferably 3% by mass or more.
  • the saturated fatty acid additive is selected from the group consisting of saturated fatty acids having a molar mass of 200-350 g/mol, esters of the saturated fatty acids, and combinations thereof.
  • the saturated fatty acid reduces discomfort during smoking.
  • Said esters of saturated fatty acids are obtained from alcohols and saturated fatty acids having a molar mass of 200 to 350 g/mol, so that the molar mass of the ester varies with the molar mass of the alcohol.
  • the molar mass of the ester is in one embodiment from 210 to 1300 g/mol.
  • Esters of saturated fatty acids generally have a lower vapor pressure than fatty acids, so that the effect of reducing discomfort during smoking is sustained throughout smoking.
  • the effect of reducing discomfort during smoking is also simply referred to as the effect of reducing discomfort.
  • the lower limit of the molar mass of the saturated fatty acid ester is preferably 240 g/mol or more, more preferably 270 g/mol or more.
  • the upper limit is preferably 1140 g/mol or less, 1112 g/mol or less, 300 g/mol or less, or 290 g/mol or less.
  • the content of the saturated fatty acid-based additive is 0.01 to 3% by mass based on the total dry matter mass of the tobacco raw material (assuming the dry matter content is 100% by mass). If the content is less than the lower limit, the effect of reducing discomfort is not sufficient, and if the content exceeds the upper limit, the offensive odor increases. From this point of view, the lower limit of the content is preferably 1% by mass or more, and the upper limit is preferably 2% by mass or less.
  • the amount of dry substance is the mass excluding the medium described later, preferably the mass of the residue when the composition is dried at 100° C. for 5 hours.
  • the number of carbon atoms in the fatty acid portion of the saturated fatty acid and the ester is preferably 12-20, more preferably 15-19. When the number of carbon atoms is within this range, the effect of reducing discomfort becomes more pronounced.
  • the water solubility of the saturated fatty acid in the saturated fatty acid additive is preferably 0.15 mg/g or less, more preferably 0.12 mg/g or less.
  • the lower limit is not limited and may be 0 mg/g, preferably 0.05 mg/g or more.
  • the saturated fatty acids include octanoic acid, decanoic acid, myristic acid, palmitic acid, stearic acid, and nonadecanoic acid. Among them, palmitic acid, stearic acid, or nonadecanic acid is preferable from the viewpoint of availability and expression of discomfort-reducing effect.
  • the saturated fatty acid may be a mixture, it is preferably a single product rather than a mixture.
  • the single product includes the case where the compound is a pure product, or the case where the compound contains impurities that are unavoidably contained.
  • the saturated fatty acids consist exclusively of palmitic acid. If the saturated fatty acid is a single product, the dispersibility of the saturated fatty acid in the molded article such as a sheet is improved when the tobacco composition of the present invention is formed into the molded article.
  • ester of saturated fatty acid examples include the aforementioned alkyl ester and sugar ester of saturated fatty acid.
  • the alkyl moiety is preferably derived from a linear, branched or cyclic alkyl group having 1 to 10 carbon atoms such as a methyl group.
  • sugar moiety is preferably derived from a disaccharide such as sucrose. Examples of preferred said esters include sucrose palmitate and methyl palmitate.
  • the saturated fatty acid moiety in the ester is preferably derived from a single saturated fatty acid for the reasons described above. Although the alcohol moiety in the ester does not have to be a single product, it is preferably a single product for the reason described above.
  • the ester also functions as an emulsifier.
  • the saturated fatty acid additive contains the saturated fatty acid and the ester.
  • the type of saturated fatty acid additive can be appropriately selected depending on the tobacco raw material used. Therefore, this aspect also has the advantage of being versatile.
  • a part or all of the saturated fatty acid additive is preferably powder.
  • the saturated fatty acid-based additive is a powder
  • the dispersibility of the saturated fatty acid-based additive is improved in the molded article such as a sheet, as will be described later.
  • its size is not limited, for example, D50 is preferably 30-120 ⁇ m, more preferably 50-100 ⁇ m.
  • the saturated fatty acid additive preferably has a higher degree of crystallinity than wax or natural oils and fats.
  • the tobacco sheet may contain liquid sugar.
  • Liquid sugar is liquid sugar.
  • the liquid sugar content is preferably 3 to 10% by mass, more preferably 5 to 8% by mass, based on the amount of dry matter in the tobacco composition.
  • tobacco sheets may contain natural plant fragrances.
  • the content of the natural plant flavor is preferably 0.5 to 3% by mass, more preferably 2 to 3% by mass, based on the amount of dry matter in the tobacco composition.
  • Natural botanical flavors that are known in the field of tobacco can be used, but licorice is preferred in the present invention.
  • Licorice is a sweetener derived from Spanish licorice, which belongs to the genus Glycyrrhiza of the legume family.
  • the amount of nicotine contained in the tobacco sheet in this aspect is not limited, but in one aspect it can be 2% by mass or more based on the amount of dry matter in the tobacco sheet. In general, when the amount of nicotine increases, discomfort during smoking tends to increase. becomes more pronounced. Although the upper limit of the amount of nicotine is not limited, it is practically 3% by mass or less.
  • the amount of nicotine can be 1.5% by mass or less.
  • the amount of nicotine is within the above range, a milder flavor and taste can be imparted.
  • the lower limit of the amount of nicotine is not limited, it is practically 0.1% by mass or more.
  • the nicotine contained in the tobacco sheet may be derived from the tobacco raw material, or may be derived from other components.
  • the tobacco sheet in this aspect can contain the aforementioned aerosol-generating agent.
  • the amount of aerosol-generating agent is preferably 12% by weight or less, more preferably 11% by weight or less, based on the dry matter weight of the tobacco sheet.
  • the lower limit is not limited, and may be 0% by mass, preferably 1% by mass or more. If the amount of the aerosol-generating agent exceeds the upper limit, the production of the sheet may become difficult, and if it is less than the lower limit, the smoke sensitivity may decrease.
  • a binder is an adhesive for binding fibers together.
  • Binders include thickening polysaccharides such as gums, modified celluloses, and modified starches.
  • the amount of the binder is appropriately adjusted depending on the application, and can be, for example, about 1 to 10% by mass based on the amount of dry matter of the tobacco sheet.
  • the tobacco sheet in this aspect is manufactured by any method.
  • a saturated fatty acid-based additive is mixed to obtain a mixture containing the additive, and the sheet can be produced by the method described above.
  • a powdery saturated fatty acid-based additive and mix so as to maintain the powdery state.
  • the tobacco sheet produced in this way has good dispersibility of the aerosol generating agent.
  • Good dispersibility means that the saturated fatty acid additive is uniformly dispersed.
  • the mixing step is preferably carried out below the melting point of the saturated fatty acid additive. For example, this step can be carried out at 10-50°C.
  • a mixture (also referred to as “slurry”) containing a saturated fatty acid-based additive is preferably produced by a method comprising the following steps.
  • the slurry is prepared while the saturated fatty acid-based additive remains powdery.
  • the dispersibility of the component (B) is improved when the molding is formed.
  • the size of the powder is as described above.
  • the fact that the saturated fatty acid additive maintains a powdery state means that part or all of it maintains a powdery state.
  • the medium includes water and hydrophilic organic solvents, but the most preferable medium for handling is water.
  • a material that is solid at room temperature is pulverized into powder, and these are mixed to obtain a powder mixture.
  • liquid or pasty materials such as medium are mixed at room temperature to obtain a liquid mixture.
  • the viscosity of the slurry at 25°C is preferably 100,000 to 200,000 (mPa ⁇ s) from the viewpoint of good dispersion of the powdery saturated fatty acid additive in the medium.
  • the viscosity was measured using a Brookfield viscometer (Brookfield DV-I prime). Measured at 1.0 rpm using LV4.
  • the tobacco-containing segment (hereinafter also simply referred to as "tobacco segment”) includes paper or paper containing an aerosol-generating agent.
  • FIG. 4A A schematic of a tobacco segment in this embodiment is shown in FIG. 4A.
  • the tobacco segment 20A comprises a tobacco filler 21 and a wrapper 22 surrounding it.
  • the tobacco filling 21 includes the tobacco sheet T and the paper P.
  • the tobacco sheet T has a strand shape obtained by cutting it
  • the paper P also has a strand shape.
  • the strand may be obtained by cutting a sheet in which the tobacco sheet T and the paper P are laminated. Note that the wavy shape of the tobacco sheet T is omitted in the drawings for explaining this embodiment.
  • FIG. 4B shows a mode in which the sheet-like tobacco filler 21 is spirally filled into the wrapper 22 .
  • the sheet-shaped tobacco filler 21 may be a sheet in which the tobacco sheet T and the paper P are laminated, or may be a sheet obtained by joining the side surfaces of the tobacco sheet T and the paper P together or in the vicinity of the side surfaces. good.
  • FIG. 4C shows a mode in which the sheet-like tobacco filler 21 is folded and filled into the wrapper 22.
  • the sheet-shaped tobacco filler 21 may be a sheet in which the tobacco sheet T and the paper P are laminated, or may be a sheet obtained by joining the side surfaces of the tobacco sheet T and the paper P together or in the vicinity of the side surfaces. good.
  • FIG. 4D shows a mode of filling the shredded tobacco filler 21 into the wrapper 22.
  • FIG. The drawing shows a manner in which chopped pieces of tobacco sheet T and chopped paper P are prepared and filled. The cut may be obtained by cutting a sheet obtained by stacking the tobacco sheet T and the paper P.
  • FIG. 4E shows a mode in which the sheet-like tobacco filler 21 is rolled up by being compressed in the vertical and horizontal directions and then filled into the wrapper 22 .
  • the sheet-shaped tobacco filler 21 may be a sheet in which the tobacco sheet T and the paper P are laminated, or may be a sheet obtained by joining the side surfaces of the tobacco sheet T and the paper P together or in the vicinity of the side surfaces. good.
  • the tobacco segment as an aspect 3-1, has a total content of tobacco sheet, lignin and hemicellulose of 0.1 to 10% by mass as a filler. Including some paper.
  • the filling is a filling for tobacco segments.
  • Lignin is a high-molecular phenolic compound contained in trees and the like.
  • Hemicellulose is an insoluble polysaccharide contained in cell walls. When the total amount is within this range, offensive odors (such as fiber odors) during smoking can be reduced. That is, in this aspect, the effect of diluting the flavor and taste without greatly impairing the original flavor and taste is exhibited.
  • the upper limit of the total content of lignin and hemicellulose is preferably 9.0% by mass or less.
  • Lignin and hemicellulose are measured by known methods, but in the present invention, they are preferably measured by the following methods.
  • step 1) for example, a Thermo ScientificTM DionexTM ASETTM high-speed solvent extraction system (model number: ASE-350) can be used.
  • Step 2) can be specifically implemented as follows. Put 50 mg of sample A in a screw bottle, add 8.5 ml of ultrapure water (ML-Q water) and 0.5 ml of pancreatin solution, and shake at 40° C. and 125 rpm for 16 hours.
  • the pancreatin solution is the supernatant obtained by adding 8 g of pancreatin to 100 ml of 0.1 M phosphate buffer of pH 6.4, stirring for 1 hour, and centrifuging at 8000 rpm for 30 minutes.
  • the sample liquid is then transferred to a 15 ml centrifuge tube using ML-Q water and centrifuged at 8000 rpm for 15 minutes to remove the supernatant. This wash is repeated three times.
  • Steps ii) and iii) can be specifically performed as follows. 100 mg of sample A is placed in a screw bottle, 4 ml of 72% sulfuric acid is added, the sample is completely immersed in sulfuric acid, and shaken at 30° C. and 200 rpm for 4 hours. Next, 157.2 ml of ultrapure water (ML-Q water) is added so that the concentration of sulfuric acid after dilution becomes 4%, transferred to an eggplant flask, and heated under reflux in an oil bath at 110° C. for 2 hours. After allowing to cool to room temperature, filter, dry with a rotary dryer, and weigh.
  • ML-Q water ultrapure water
  • the content of the paper used in this embodiment is preferably 5-70% by mass, more preferably 10-50% by mass, still more preferably 15-40% by mass, relative to the dry matter content of the tobacco sheet.
  • the flavor and taste can be diluted to an appropriate level without impairing the original flavor and taste.
  • Dry matter content is, in one embodiment, the weight of the residue after drying the tobacco sheet at 100° C. for 5 hours.
  • the paper used in this embodiment is not limited as long as the total content of lignin and hemicellulose is within the above range. . However, from the viewpoint of suppressing the generation of offensive odors, non-coated paper or lightly coated paper is preferred. Moreover, the paper used in this embodiment may or may not contain an aerosol generating agent, which will be described later. The amount may be in the range described in the 3-2 aspect, or may be in a range other than this.
  • the tobacco segment includes, as an aspect 3-2, a tobacco sheet and a paper containing an aerosol-generating agent as fillers.
  • An aerosol-generating agent is a material that is vaporized by heating and then cooled to form an aerosol or atomized to form an aerosol. Since paper containing an aerosol-generating agent is used in this embodiment, it is possible to dilute the flavor and taste without reducing the amount of smoke.
  • the aerosol generating agent those described above can be used.
  • the amount is preferably 3 to 20% by weight, more preferably 5 to 15% by weight, based on the dry matter content of said paper.
  • Aerosol-generating agents can be added to the paper, such as by impregnation or spraying.
  • the content of the paper to which the aerosol generating agent is added is preferably 5 to 75% by mass, more preferably 10 to 50% by mass, still more preferably 15 to 40% by mass, relative to the dry matter content of the tobacco sheet. .
  • the paper used in this aspect is not limited, and may be the paper described in the 3-1 aspect.
  • the density of the paper before adding the aerosol generating agent used in this embodiment may be within the range described in Embodiment 3-1, or may be within a range other than this.
  • the amount of lignin and hemicellulose contained in the paper used in this embodiment is not limited, and may be within the range described in Embodiment 3-1, or may be within a range other than this.
  • the shape of the paper is not limited as long as it is easily mixed with the tobacco sheet.
  • the paper is a sheet, cut, or strand.
  • the shapes of the paper and tobacco sheets are similar, and in the most preferred embodiment, shredded paper and shredded tobacco sheets are used.
  • the paper may be added with menthol and other fragrances that are commonly used in the relevant field.
  • Tobacco lamina (leaf tobacco) was dry pulverized with a Hosokawa Micron ACM machine to obtain tobacco powder.
  • the cumulative 90% particle diameter (D90) in the volume-based particle size distribution measured by the dry laser diffraction method is measured using a Mastersizer (trade name, manufactured by Spectris Co., Ltd., Malvern Panalytical Division). As a result, it was 200 ⁇ m.
  • a tobacco sheet was manufactured using the tobacco powder as a tobacco raw material. Specifically, 70 parts by mass of the tobacco raw material, 12 parts by mass of glycerin as an aerosol generating agent, 4 parts by mass of powdered carboxymethyl cellulose as a first molding agent, and water as a second molding agent. 1 part by mass of swollen carboxymethylcellulose, 5 parts by mass of fibrous pulp as a reinforcing agent, and 8 parts by mass of cocoa powder as a flavoring agent were mixed and kneaded in an extruder. The kneaded product was formed into a sheet by two pairs of metal rolls to obtain a rolled product.
  • a rotary roll blade for noodle making was pressed against the rolled product, and the product was cut into strips and given a corrugated shape. Further, it was cut into 20 mm lengths and dried to obtain tobacco sheets with a length of 20 mm and a width of 0.8 mm.
  • the thickness direction cross-section of the tobacco sheet had a cross-sectional shape as shown in FIG.
  • the swelling property of the obtained tobacco sheet was measured. Specifically, after leaving the tobacco sheet in a conditioned room at 22° C. and 60% for 48 hours, the swelling property was measured with DD-60A (trade name, manufactured by Borgwald). The measurement was carried out by placing 15 g of tobacco sheet in a cylindrical container with an inner diameter of 60 mm and compressing the container with a load of 3 kg for 30 seconds to obtain the volume. Table 1 shows the results. In addition, in Table 1, the swelling property is shown as an increase rate (%) of the swelling property with respect to the reference value of the swelling property value of Comparative Example 1 described later.
  • Example 1 A roll-formed product was produced in the same manner as in Example 1. After that, it was cut into strips with a plurality of ring-shaped rotary blades. Further, the tobacco sheet was cut to a length of 20 mm to obtain a tobacco sheet having a length of 20 mm and a width of 0.8 mm. The swelling property of the obtained tobacco sheet was measured in the same manner as in Example 1. Table 1 shows the results.
  • the tobacco sheet of Example 1 which is the tobacco sheet according to the present embodiment, has improved swelling properties compared to the tobacco sheet of Comparative Example 1, which is not provided with a corrugated shape.
  • fructan- or fructose-containing composition sheet for smoking
  • 90 g of inulin-type fructan Name Fuji FF 10 g was added and mixed to obtain an inulin-type fructan solution.
  • a smoking composition sheet (containing an inulin-type fructan) after addition is prepared by adding a solution of inulin-type fructan using a syringe so as to spread over the entire tobacco sheet.
  • Each sheet having an inulin-type fructan content of 0.5, 1.0, 2.0, 3.0, or 3.5% by mass was obtained.
  • fructose manufactured by Happo Shokusan Co., Ltd., product name: fructose
  • a solution of fructose was obtained by mixing.
  • the above 1. Prepare a similar tobacco sheet, and add a solution of fructose using a syringe so that it spreads throughout the tobacco sheet, so that the fructose for the entire smoking composition sheet (containing fructose) after addition
  • Each sheet with a content of 0.5, 1.0, 2.0, 3.0, or 3.5% by weight was obtained.
  • a wrapper was filled with the fructan-containing smoking composition sheet or fructose-containing composition sheet obtained as described above to form a smoking segment, and the non-combustion heating type flavor inhalation article shown in FIG. 2 was prepared.
  • the above inulin-type fructan is one type of fructan, and smoking composition sheets containing inulin-type fructans correspond to examples of the present application.
  • the fructose is one type of monosaccharide, and the smoking composition sheet containing fructose corresponds to the comparative example of the present application.
  • smoking composition sheets containing inulin-type fructans correspond to examples of the present application, while smoking composition sheets containing fructose correspond to comparative examples of the present application.
  • the value of the flavor is preferably 1.5 or more. Therefore, from the viewpoint of achieving both the flavor and the effect of suppressing the feeling of inhibition of the flavor, the content of the inulin-type fructan is 0.5 to 3% by mass. was found to be desirable.
  • fructose was found to have a low and insufficient effect of suppressing the sense of flavor and taste inhibition.
  • fructose a panelist commented that the feeling of inhibition of flavor and taste increases in the latter half of smoking (the effect of suppressing the feeling of inhibition of flavor and taste does not last long).
  • a comparative experiment was carried out on the persistence of inhibitory effects on flavor and taste inhibition sensations of type fructans and fructose.
  • the inulin-type fructan suppresses the sensation of flavor and taste inhibition at any content of 0.5 to 3.5% by mass, compared to the 2.0% by mass fructose for comparison. It was found to be excellent in the durability of the effect.
  • fructose at any content of 0.5 to 3.5% by mass, compared to the 2.0% by mass inulin-type fructan for comparison, inhibited flavor and taste. It was found that the persistence of the anti-sensitivity effect was inferior. Inulin-type fructans undergo a process of thermal decomposition before they develop a sweet flavor through a caramelization reaction, so it is thought that they slowly generate a sweet flavor over a long period of time.
  • fructose is thought to generate a sweet flavor in a short period of time through a caramelization reaction. Since the sweet flavor suppresses the sense of inhibition of flavor-smelling taste, it is considered that the difference in duration of the effect of suppressing the sense of inhibition of flavor-drinking taste is caused by the difference in the generation time of the sweet flavor. From the above results, it was confirmed that the inulin-type fructan is superior to fructose in the persistence of the inhibitory effect on flavor and taste inhibition.
  • the tobacco material of this example continuously suppresses the sense of flavor and taste inhibition from the early stage to the latter stage of smoking behavior (excellent persistence of the effect of suppressing the sense of flavor and taste inhibition).
  • Example 1b A paper-made tobacco sheet was prepared as the component (A).
  • the sheet contained tobacco material and 15% by weight of vegetable glycerin as an aerosol generator.
  • a saturated fatty acid shown in Table 1b was prepared as component (B) and sprayed onto the sheet.
  • the amount of component (B) added per dry matter amount of the tobacco composition (total of the paper-made tobacco sheet and component (B)) is as shown in Table 1b.
  • the amount of octanoic acid added was 1.0% by weight per dry matter of the tobacco composition.
  • a plurality of slits were provided and then rolled up to obtain a tobacco rod.
  • the longitudinal direction of the slit was made parallel to the longitudinal direction of the tobacco segment.
  • a non-combustion heating tobacco flavor inhalation article having the structure shown in FIG. 2 was manufactured.
  • the length of each segment was as follows. Tobacco segment: 12mm Center hole part: 8mm Paper tube: 20mm Acetate filter: 40mm Using a hollow cylindrical heater with an outer diameter of 3.2 mm and an inner diameter of 1.3 mm, the non-combustion heating tobacco flavor inhalation article was heated under the following conditions to carry out a smoking test.
  • a non-combustion heated tobacco flavor inhalation article was manufactured and evaluated by the following procedure. 1) Tobacco lamina was pulverized with a lab mill to obtain fine tobacco powder having a raw material particle size D90 of 100 ⁇ m. 2) Granular palmitic acid and sucrose palmitate were pulverized with a lab mill to obtain a powder. 3) The softwood pulp was crushed with a lab mill. 4) These powdered materials were placed in a Ken mixer and mixed by stirring. 5) Liquid or pasty materials such as water, glycerin, licorice, liquid sugar, binder, etc. were placed in a mixer (manufactured by Primix) and mixed for 30 minutes.
  • a predetermined amount of the shredded tobacco composition was rolled up with wrapping paper into a size of ⁇ 7 ⁇ 20 mm to produce a single roll.
  • a single roll was used as a tobacco rod to obtain a non-combustion heating tobacco flavor inhalation article shown in FIG. 13)
  • the non-combustion heated tobacco flavor inhalation article was inserted into a heating device (PloomS manufactured by Japan Tobacco Inc.), heated, and subjected to smoking evaluation. Sensory evaluation was performed by well-trained panelists. The evaluation results are shown in Table 2b.
  • the fiber odor was evaluated according to the following criteria. 1: None (standard) 2: very low 3: low 4: moderate 5: strong
  • the sample liquid was then transferred to a 15 ml centrifuge tube using ML-Q water and centrifuged at 8000 rpm for 15 minutes to remove the supernatant. This washing was repeated three times. After washing, 10 ml of a 5% sulfuric acid aqueous solution was added and hydrolysis was carried out at 100° C. for 2.5 hours. After the hydrolysis reaction was completed, the sample was allowed to cool to room temperature. The precipitate was then filtered off and the filtrate was collected in a 250 ml volumetric flask. After thoroughly washing the residue on the filter paper with ML-Q water, the volume was adjusted to 250 ml. This solution was used as a sample for hemicellulose measurement.
  • a tobacco sheet for a non-combustion heating type flavor inhaler containing a tobacco raw material, the tobacco sheet for a non-combustion heating type flavor inhaler having a corrugated cross-section in the thickness direction of the tobacco sheet.
  • the tobacco sheet for a non-combustion heating type flavor inhaler according to [1] wherein the tobacco sheet further contains an aerosol generating agent.
  • the aerosol generating agent is at least one selected from the group consisting of glycerin, propylene glycol and 1,3-butanediol.
  • the first molding agent is at least one selected from the group consisting of polysaccharides, proteins and synthetic polymers.
  • the second molding agent is at least one selected from the group consisting of polysaccharides, proteins and synthetic polymers, which is different from the first molding agent.
  • non-combustion heated flavor inhaler tobacco sheet [8] The non-combustion heating type flavor inhalation according to any one of [5] to [7], wherein the ratio of the first molding agent contained in 100% by mass of the tobacco sheet is 0.1 to 15% by mass. Dexterous cigarette sheet. [9] The non-combustion heating type flavor inhalation according to any one of [5] to [8], wherein the ratio of the second molding agent contained in 100% by mass of the tobacco sheet is 0.1 to 15% by mass. Dexterous cigarette sheet.
  • a non-combustion heating flavor inhaler comprising a tobacco-containing segment including the tobacco sheet for a non-combustion heating flavor inhaler according to any one of [1] to [9].
  • a method for manufacturing a tobacco sheet for a non-combustion heating type flavor inhaler according to any one of [1] to [9], preparing a mixture comprising a tobacco material, an aerosol-generating agent, a first shaping agent, and a second shaping agent; rolling the mixture to form a rolled article; A step of pressing a rotary roll blade against the rolled product to cut it into strips while imparting a corrugated shape; method including.
  • [1a] A tobacco material containing fructans.
  • [2a] The tobacco material according to [1a], wherein the fructan is selected from the group consisting of inulin-type fructans, levan-type fructans, branched fructans, fructooligosaccharides, and mixtures thereof.
  • [3a] The tobacco material according to [1a] or [2], wherein the fructan content relative to the entire tobacco material is 0.5 to 3% by mass.
  • [4a] The tobacco material according to any one of [1a] to [3a], further comprising tobacco sheets or tobacco shreds.
  • [5a] A heated smoking article comprising the tobacco material of any one of [1a] to [4a].
  • [1b] (A) a tobacco material; (B) a tobacco composition comprising a saturated fatty acid additive, said component (B) is selected from the group consisting of saturated fatty acids having a molar mass of 200 to 350 g/mol, esters of said saturated fatty acids, and combinations thereof; A tobacco composition containing 0.01 to 3% by weight of component (B) based on the amount of dry matter in the composition.
  • [2b] The composition according to [1b], wherein the saturated fatty acid and saturated fatty acid ester in component (B) are each a single item.
  • [3b] The composition according to [1b] or [2b], wherein the fatty acid moiety in the saturated fatty acid and the ester of component (B) has 12 to 20 carbon atoms.
  • [4b] The composition according to any one of [1b] to [3b], further comprising 1 to 10% by mass of liquid sugar based on the amount of dry matter in the composition.
  • [5b] The composition according to any one of [1b] to [4b], wherein component (A) contains 10% by mass or less of a material derived from oriental species.
  • component (A) contains 10% by mass or less of a material derived from oriental species.
  • [6b] The composition according to any one of [1b] to [5b], further comprising 0.5 to 3% by mass of a natural botanical fragrance based on the amount of dry matter in the composition.
  • [7b] The composition according to any one of [1b] to [6b], containing 2% by mass or more of nicotine based on the amount of dry matter in the composition.
  • [11b] A step of mixing the component (A), the component (B) partially or wholly powder, and a medium so as to keep the powder in a powder state to form a slurry;
  • [1c] As a filling, tobacco material; including paper and The total content of lignin and hemicellulose in the paper is 0.1 to 10% by mass, heating tobacco segment; [2c] as a filler, tobacco material; a paper containing an aerosol-generating agent; heating tobacco segment; [3c] The tobacco segment according to [1c], wherein the total content of lignin and hemicellulose is 9.0% by mass or less. [4c] The tobacco segment according to [1c] or [3c], wherein the content of the paper is 5-70% by mass relative to the dry matter content of the tobacco material. [5c] The content of the paper is 15-40% by mass relative to the dry matter content of the tobacco material. The tobacco segment according to [4c].
  • [6c] The tobacco segment according to any one of [1c] to [5c], wherein the paper has a density of 0.05 to 0.8 [g/cm 3 ].
  • [7c] The tobacco segment of [2c] or [6c], wherein the content of the paper is 5-75% by mass relative to the dry matter content of the tobacco material.
  • [8c] The tobacco segment of any of [1c] or [3c]-[6c], wherein said paper comprises an aerosol-generating agent.
  • a non-combustion heating flavor inhalation article comprising the tobacco segment according to any one of [1c] to [8c] above.
  • [10c] The method for producing a tobacco segment according to any one of [1c] to [8c], comprising mixing the paper with the tobacco material.

Abstract

Provided is a tobacco sheet for a non-combustion heating-type fragrance inhaler including a tobacco material, wherein a cross-section of the tobacco sheet in the thickness direction has a wavy shape.

Description

非燃焼加熱型香味吸引器用たばこシート及びその製造方法、非燃焼加熱型香味吸引器、並びに非燃焼加熱型香味吸引システムTOBACCO SHEET FOR NON-COMBUSTION HEATING FLAVOR INSPIRATION AND MANUFACTURING METHOD THEREOF, NON-COMBUSTION HEATING FLAVOR INSPIRATION, AND NON-COMBUSTION HEATING FLAVOR SUCTION SYSTEM
 本発明は、非燃焼加熱型香味吸引器用たばこシート及びその製造方法、非燃焼加熱型香味吸引器、並びに非燃焼加熱型香味吸引システムに関する。 The present invention relates to a tobacco sheet for a non-combustion heating flavor inhaler, a manufacturing method thereof, a non-combustion heating flavor inhaler, and a non-combustion heating flavor inhalation system.
 燃焼型香味吸引器(シガレット)では、葉たばこやたばこシートを含むたばこ充填物を燃焼して香味を得る。例えば特許文献1には、燃焼型香味吸引器に使用されるたばこシートが開示されている。該燃焼型香味吸引器の代替として、たばこシート等の香味源を燃焼する代わりに加熱して香味を得る非燃焼加熱型香味吸引器が提案されている。非燃焼加熱型香味吸引器の加熱温度は、燃焼型香味吸引器の燃焼温度より低く、例えば約400℃以下である。このように、非燃焼加熱型香味吸引器の加熱温度は低いため、煙量を増加させる観点から、非燃焼加熱型香味吸引器では香味源にエアロゾル発生剤を添加することができる。エアロゾル発生剤は加熱により気化し、エアロゾルを発生する。該エアロゾルはたばこ成分等の香味成分を伴い使用者に供給されるため、使用者は十分な香味を得ることができる。 A combustion-type flavor inhaler (cigarette) obtains flavor by burning tobacco fillings including leaf tobacco and tobacco sheets. For example, Patent Literature 1 discloses a tobacco sheet used in a combustion type flavor inhaler. As an alternative to the combustion type flavor inhaler, a non-combustion heating type flavor inhaler has been proposed that obtains flavor by heating a flavor source such as a tobacco sheet instead of burning it. The heating temperature of the non-combustion heating type flavor inhaler is lower than the combustion temperature of the combustion type flavor inhaler, for example, about 400° C. or less. Thus, since the heating temperature of the non-combustion heating type flavor inhaler is low, an aerosol generating agent can be added to the flavor source in the non-combustion heating type flavor inhaler from the viewpoint of increasing the amount of smoke. The aerosol-generating agent is vaporized by heating to generate an aerosol. Since the aerosol is supplied to the user together with flavor components such as tobacco components, the user can obtain sufficient flavor.
 非燃焼加熱型香味吸引器は、例えば、たばこシート等が充填されたたばこ含有セグメントと、冷却セグメントと、フィルターセグメントとを備えることができる。非燃焼加熱型香味吸引器のたばこ含有セグメントの軸方向の長さは、加熱ヒーターとの関係で、通常燃焼型香味吸引器のたばこ含有セグメントの軸方向の長さよりも短い。そのため、非燃焼加熱型香味吸引器では、加熱時のエアロゾル生成量を担保するために、短いたばこ含有セグメントの区間内に多量のたばこシートが充填されている。短い区間内に多量のたばこシートを充填するために、非燃焼加熱型香味吸引器では、通常膨嵩性の低い、すなわち高密度のたばこシートが使用されている。なお、膨嵩性とは、所定質量のたばこシートの刻みを一定圧力で一定時間圧縮したときの体積を示す値である。 A non-combustion heating flavor inhaler can comprise, for example, a tobacco-containing segment filled with tobacco sheets or the like, a cooling segment, and a filter segment. The axial length of the tobacco-containing segment of the non-combustion-heating flavor inhaler is generally shorter than the axial length of the tobacco-containing segment of the normal combustion-type flavor inhaler in relation to the heating heater. Therefore, in the non-combustion heating type flavor inhaler, a large amount of tobacco sheets are filled in the short tobacco-containing segments in order to secure the amount of aerosol generated during heating. In order to fill a large amount of tobacco sheets in a short section, non-combustion heating type flavor inhalers usually use tobacco sheets with low swelling, that is, high density tobacco sheets. In addition, the swelling property is a value indicating the volume of a tobacco sheet having a predetermined mass when notches are compressed under a constant pressure for a certain period of time.
特公昭60-45914号公報Japanese Patent Publication No. 60-45914
 しかし、本発明者等は、加熱方式やヒーターの加熱能力とエアロゾルの生成を考えた場合、膨嵩性の低い(高密度の)たばこシートを用いるとたばこ含有セグメントの総熱容量が高くなるため、加熱方法やヒーターの能力によっては、たばこ含有セグメントに充填されたたばこシートがエアロゾル生成に十分に寄与しないことを見出した。当該課題を解決するためには、たばこ含有セグメントの総熱容量を低減することが考えられる。 However, considering the heating method, the heating capacity of the heater, and the generation of aerosol, the present inventors believe that if a tobacco sheet with low swelling (high density) is used, the total heat capacity of the tobacco-containing segment increases. It was found that the tobacco sheet filled in the tobacco-containing segment does not sufficiently contribute to the generation of aerosol depending on the heating method and the capacity of the heater. In order to solve this problem, it is conceivable to reduce the total heat capacity of the tobacco-containing segment.
 本発明者等は、たばこ含有セグメントの総熱容量を低減するために、(1)たばこシートに含まれるたばこ原料の比熱を低減する、(2)膨嵩性の高い(低密度の)たばこシートを用いる、ことを検討した。しかし、(1)についてはたばこ原料自体の比熱の低減は困難であるため、(2)によりたばこ含有セグメントの総熱容量を低減することが有効と考えられた。そのため、非燃焼加熱型香味吸引器に好適に用いられる膨嵩性の高い(低密度の)たばこシートの開発が望まれる。 In order to reduce the total heat capacity of the tobacco-containing segment, the present inventors (1) reduce the specific heat of the tobacco raw material contained in the tobacco sheet, and (2) use a highly bulky (low-density) tobacco sheet. I considered using it. However, as for (1), it is difficult to reduce the specific heat of the tobacco raw material itself, so it was considered effective to reduce the total heat capacity of the tobacco-containing segment by (2). Therefore, it is desired to develop a highly bulky (low density) tobacco sheet suitable for non-combustion heating type flavor inhalers.
 本発明は、膨嵩性の高い非燃焼加熱型香味吸引器用たばこシート、該たばこシートを含む非燃焼加熱型香味吸引器、及び非燃焼加熱型香味吸引システムを提供することを目的とする。 An object of the present invention is to provide a highly bulky non-combustion heating flavor inhaler tobacco sheet, a non-combustion heating flavor inhaler including the tobacco sheet, and a non-combustion heating flavor inhalation system.
 本発明は以下の実施態様を含む。
態様1
 たばこ原料を含む非燃焼加熱型香味吸引器用たばこシートであって、前記たばこシートの厚み方向の断面が波型形状を有する、非燃焼加熱型香味吸引器用たばこシート。
態様2
 フルクタンをさらに含む、態様1に記載の非燃焼加熱型香味吸引器用たばこシート。
態様3
 前記フルクタンが、イヌリン型フルクタン、レバン型フルクタン、分岐型フルクタン、フラクトオリゴ糖、及びこれらの混合物からなる群から選択される、態様1または2に記載の非燃焼加熱型香味吸引器用たばこシート。
態様4
 飽和脂肪酸系添加剤をさらに含み、
 前記添加剤が、モル質量が200~350g/molである飽和脂肪酸、当該飽和脂肪酸のエステル、およびこれらの組合せからなる群より選択され、
 その含有量が、前記シートの乾物質量当たり、0.01~3質量%である、
態様1~3のいずれかに記載の非燃焼加熱型香味吸引器用たばこシート。
態様5
 前記飽和脂肪酸および飽和脂肪酸エステルは、それぞれ単品である、態様4に記載の非燃焼加熱型香味吸引器用たばこシート。
態様6
 充填物として、
 態様1~5のいずれかに記載のシートと、
 紙と、を含み、
 前記紙のリグニンおよびヘミセルロースの合計含有量が0.1~10質量%である、
 たばこ含有セグメント。
態様7
 充填物として、
 態様1~5のいずれかに記載のシートと、
 エアロゾル発生剤を含有する紙と、を含む、
 たばこ含有セグメント。
態様8
 態様1~5のいずれかに記載の非燃焼加熱型香味吸引器用たばこシートを含むたばこ含有セグメントあるいは
 態様6または7に記載のたばこ含有セグメント
を備える非燃焼加熱型香味吸引器。
態様9
 態様8に記載の非燃焼加熱型香味吸引器と、
 前記たばこ含有セグメントを加熱する加熱装置と、
を備える非燃焼加熱型香味吸引システム。
態様10
 態様1~3のいずれかに記載の非燃焼加熱型香味吸引器用たばこシートの製造方法であって、
 たばこ原料と、エアロゾル発生剤と、第一の成型剤及び第二の成型剤と、を含む混合物を調製する工程と、
 前記混合物を圧延して圧延成形品を形成する工程と、
 前記圧延成形品に回転式ロール刃を押し当てて短冊状に切断しつつ波型形状を付与する工程と、
 必要に応じて、前記圧延成形品に前記フルクタンを添加する工程と、
を備える方法。
態様11
 態様4または5に記載の非燃焼加熱型香味吸引器用たばこシートの製造方法であって、
 たばこ原料と、エアロゾル発生剤と、第一の成型剤及び第二の成型剤と、飽和脂肪酸系添加剤と、を含む混合物を調製する工程と、
 前記混合物を圧延して圧延成形品を形成する工程と、
 前記圧延成形品に回転式ロール刃を押し当てて短冊状に切断しつつ波型形状を付与する工程と、
を備える方法。
The present invention includes the following embodiments.
Aspect 1
A tobacco sheet for a non-combustion heating type flavor inhaler, comprising a tobacco raw material, the tobacco sheet having a wavy cross section in the thickness direction of the tobacco sheet.
Aspect 2
The tobacco sheet for non-combustion heated flavor inhalers according to aspect 1, further comprising fructans.
Aspect 3
The tobacco sheet for non-combustion heating flavor inhalers according to aspect 1 or 2, wherein the fructan is selected from the group consisting of inulin-type fructans, levan-type fructans, branched fructans, fructooligosaccharides, and mixtures thereof.
Aspect 4
further comprising a saturated fatty acid additive,
said additive is selected from the group consisting of saturated fatty acids having a molar mass of 200-350 g/mol, esters of said saturated fatty acids, and combinations thereof;
The content is 0.01 to 3% by weight based on the dry matter content of the sheet.
A tobacco sheet for a non-combustion heating type flavor inhaler according to any one of aspects 1 to 3.
Aspect 5
The tobacco sheet for a non-combustion heating type flavor inhaler according to aspect 4, wherein the saturated fatty acid and the saturated fatty acid ester are each a single item.
Aspect 6
as a filling,
A sheet according to any one of aspects 1 to 5;
including paper and
The total content of lignin and hemicellulose in the paper is 0.1 to 10% by mass,
Tobacco-containing segment.
Aspect 7
as a filling,
A sheet according to any one of aspects 1 to 5;
a paper containing an aerosol-generating agent;
Tobacco-containing segment.
Aspect 8
A tobacco-containing segment comprising the tobacco sheet for a non-combustion heating flavor inhaler according to any one of aspects 1 to 5;
Aspect 9
A non-combustion heated flavor inhaler according to aspect 8;
a heating device for heating the tobacco-containing segment;
A non-combustion heated flavor suction system.
Aspect 10
A method for producing a tobacco sheet for a non-combustion heating type flavor inhaler according to any one of aspects 1 to 3, comprising:
preparing a mixture comprising a tobacco raw material, an aerosol-generating agent, a first shaping agent and a second shaping agent;
rolling the mixture to form a rolled article;
A step of pressing a rotary roll blade against the rolled product to cut it into strips while imparting a corrugated shape;
optionally adding the fructan to the rolled product;
How to prepare.
Aspect 11
A method for producing a tobacco sheet for a non-combustion heating type flavor inhaler according to aspect 4 or 5, comprising:
preparing a mixture comprising a tobacco raw material, an aerosol-generating agent, a first molding agent and a second molding agent, and a saturated fatty acid-based additive;
rolling the mixture to form a rolled article;
A step of pressing a rotary roll blade against the rolled product to cut it into strips while imparting a corrugated shape;
How to prepare.
 本発明によれば、膨嵩性の高い非燃焼加熱型香味吸引器用たばこシート、該たばこシートを含む非燃焼加熱型香味吸引器、及び非燃焼加熱型香味吸引システムを提供することができる。 According to the present invention, it is possible to provide a highly bulky non-combustion heating flavor inhaler tobacco sheet, a non-combustion heating flavor inhaler including the tobacco sheet, and a non-combustion heating flavor inhalation system.
本実施形態に係るたばこシートの一例を示す厚み方向の断面図である。1 is a cross-sectional view in the thickness direction showing an example of a tobacco sheet according to this embodiment; FIG. 本実施形態に係る非燃焼加熱型香味吸引器の一例を示す断面図である。It is a sectional view showing an example of a non-combustion heating type flavor inhaler concerning this embodiment. 本実施形態に係る非燃焼加熱型香味吸引システムの一例であって、(a)非燃焼加熱型香味吸引器を加熱装置に挿入する前の状態、(b)非燃焼加熱型香味吸引器を加熱装置に挿入して加熱する状態、を示す断面図である。An example of the non-combustion heating flavor inhalation system according to the present embodiment, in which (a) the state before the non-combustion heating flavor inhaler is inserted into the heating device, and (b) the non-combustion heating flavor inhaler is heated. It is sectional drawing which shows the state which inserts into an apparatus and heats. たばこセグメントの一態様を示す図である。1 is a diagram showing one aspect of a tobacco segment; FIG. たばこセグメントの一態様を示す図である。1 is a diagram showing one aspect of a tobacco segment; FIG. たばこセグメントの一態様を示す図である。1 is a diagram showing one aspect of a tobacco segment; FIG. たばこセグメントの一態様を示す図である。1 is a diagram showing one aspect of a tobacco segment; FIG. たばこセグメントの一態様を示す図である。1 is a diagram showing one aspect of a tobacco segment; FIG. 参考例における、イヌリン型フルクタン又はフルクトースの含有量(質量%)と官能評価(香味又は香喫味阻害感)との関係を示すグラフである。1 is a graph showing the relationship between the content (% by mass) of inulin-type fructan or fructose and the sensory evaluation (flavor or flavor inhibition) in Reference Examples. 参考例における、イヌリン型フルクタン又はフルクトースの含有量(質量%)と香喫味阻害感抑制効果持続性との関係を示すグラフである。Fig. 2 is a graph showing the relationship between the content (% by mass) of inulin-type fructan or fructose and the persistence of inhibitory effect on flavor and taste inhibition in Reference Examples.
 [非燃焼加熱型香味吸引器用たばこシート]
 本実施形態に係る非燃焼加熱型香味吸引器用たばこシート(以下、「たばこシート」ともいう。)は、たばこ原料を含み、前記たばこシートの厚み方向の断面は波型形状を有する。本実施形態に係るたばこシートは厚み方向の断面形状が波型であるため、嵩高く、高い膨嵩性を有する。そのため、本実施形態に係るたばこシートを用いることでたばこ含有セグメントの総熱容量を低減することができ、たばこ含有セグメントに充填されたたばこシートをエアロゾル生成に十分に寄与させることができる。また、本実施形態に係るたばこシートはエアロゾル発生剤や一種又は二種以上の成型剤をさらに含むことが好ましく、これらの配合割合を所定の範囲内とすることで、たばこシートの膨嵩性がより向上する。
[Tobacco sheet for non-combustion heating type flavor inhaler]
A tobacco sheet for a non-combustion heating type flavor inhaler (hereinafter also referred to as a "tobacco sheet") according to the present embodiment contains tobacco raw material, and has a wavy cross-section in the thickness direction of the tobacco sheet. Since the tobacco sheet according to the present embodiment has a corrugated cross-sectional shape in the thickness direction, it is bulky and has a high swelling property. Therefore, by using the tobacco sheet according to the present embodiment, the total heat capacity of the tobacco-containing segment can be reduced, and the tobacco sheet filled in the tobacco-containing segment can sufficiently contribute to aerosol generation. In addition, the tobacco sheet according to the present embodiment preferably further contains an aerosol-generating agent and one or more molding agents. improve more.
 (たばこシートの形状)
 本実施形態に係るたばこシートは、厚み方向の断面が波型形状を有する。すなわち、本実施形態に係るたばこシートを平面方向のある一方向において厚み方向に切断した場合、その断面の形状が波型の形状を有する。前記平面方向のある一方向は、例えばたばこシートの長手方向であってもよく、短手方向であってもよい。ここで「波型」とは、上下にうねった形状であれば特に限定されず、波の山は直線的な形状であってもよく、曲線的な形状であってもよい。また、波は規則的であってもよく、不規則的であってもよい。
(Shape of cigarette sheet)
The tobacco sheet according to this embodiment has a wavy cross section in the thickness direction. That is, when the tobacco sheet according to the present embodiment is cut in the thickness direction in one plane direction, the cross section has a corrugated shape. The plane direction may be, for example, the longitudinal direction or the lateral direction of the tobacco sheet. Here, the “wavy shape” is not particularly limited as long as it has a shape that undulates vertically, and the crests of the waves may have a straight shape or a curved shape. Also, the waves may be regular or irregular.
 本実施形態に係るたばこシートの厚み方向の断面形状の一例を図1に示す。図1に示されるたばこシート1は、厚み方向の断面において波2を有する。波2の幅w1は特に限定されないが、0.1~10.0mmの範囲内であることが好ましい。また、波2の高さw2は特に限定されないが、0.1~5.0mmの範囲内であることが好ましい。たばこシート1の厚みw3は、100~1000μmの範囲内であることが好ましい。図1に示されるように、波2は鋸歯形状3を有していてもよい。波2が鋸歯形状3を有することにより、たばこシートの混合体において鋸歯形状の先端と先端が接することによりさらに空隙を形成させることができ、結果として膨嵩性をより向上させることができる。本実施形態に係るたばこシートの平面方向における大きさは特に限定されないが、例えば長さ:5.0~40.0mm、幅:0.5~2.0mmであることができる。 Fig. 1 shows an example of the cross-sectional shape in the thickness direction of the tobacco sheet according to this embodiment. The tobacco sheet 1 shown in FIG. 1 has waves 2 in a cross-section in the thickness direction. Although the width w1 of the wave 2 is not particularly limited, it is preferably within the range of 0.1 to 10.0 mm. Also, the height w2 of the wave 2 is not particularly limited, but is preferably within the range of 0.1 to 5.0 mm. The thickness w3 of the tobacco sheet 1 is preferably within the range of 100-1000 μm. As shown in FIG. 1, the waves 2 may have a sawtooth shape 3 . Since the wave 2 has the saw-tooth shape 3, it is possible to further form voids in the mixture of tobacco sheets by contacting the tips of the saw-tooth shapes, and as a result, the swelling property can be further improved. The size of the tobacco sheet according to the present embodiment in the planar direction is not particularly limited, but may be, for example, length: 5.0 to 40.0 mm and width: 0.5 to 2.0 mm.
 (たばこ原料)
 本実施形態に係るたばこシートに含まれるたばこ原料としては、たばこ成分が含まれるものであれば特に限定されないが、例えばたばこ粉末やたばこ抽出物が挙げられる。たばこ粉末としては、例えば葉たばこ、中骨、残幹等が挙げられる。これらは一種を用いてもよく、二種以上を併用してもよい。これらを所定の大きさに裁刻することで、たばこ粉末として使用することができる。たばこ粉末の大きさとしては、乾式レーザー回折法により測定される体積基準の粒度分布における累積90%粒子径(D90)が200μm以上であることが、更なる膨嵩性向上の観点から好ましい。たばこ原料がたばこ粉末である場合、たばこシート100質量%に含まれるたばこ粉末の割合は、45~95質量%であることが好ましく、50~93質量%であることがより好ましく、60~85質量%であることがさらに好ましい。たばこ抽出物としては、例えば葉たばこを粗砕し、これを水等の溶媒と混合・攪拌することで葉たばこから水溶性成分を抽出し、得られた水抽出物を減圧乾燥して濃縮することで得られるたばこ抽出物が挙げられる。
(tobacco raw material)
The tobacco raw material contained in the tobacco sheet according to the present embodiment is not particularly limited as long as it contains tobacco components, and examples thereof include tobacco powder and tobacco extract. Tobacco powder includes, for example, leaf tobacco, core bones, residual stems, and the like. These may be used alone or in combination of two or more. By chopping these into a predetermined size, they can be used as tobacco powder. Regarding the size of the tobacco powder, it is preferable that the cumulative 90% particle size (D90) in the volume-based particle size distribution measured by the dry laser diffraction method is 200 μm or more from the viewpoint of further improving the swelling property. When the tobacco raw material is tobacco powder, the tobacco powder content in 100% by mass of the tobacco sheet is preferably 45 to 95% by mass, more preferably 50 to 93% by mass, and more preferably 60 to 85% by mass. % is more preferred. As the tobacco extract, for example, leaf tobacco is crushed, mixed and stirred with a solvent such as water to extract a water-soluble component from the leaf tobacco, and the resulting water extract is dried under reduced pressure and concentrated. Tobacco extracts obtained may be mentioned.
 (エアロゾル発生剤)
 本実施形態に係るたばこシートは、加熱時の煙量増加の観点から、さらにエアロゾル発生剤を含むことが好ましい。エアロゾル発生剤としては、例えばグリセリン、プロピレングリコール、1,3-ブタンジオール等が挙げられる。これらは一種を用いてもよく、二種以上を併用してもよい。
(Aerosol generating agent)
From the viewpoint of increasing the amount of smoke when heated, the tobacco sheet according to this embodiment preferably further contains an aerosol-generating agent. Aerosol-generating agents include, for example, glycerin, propylene glycol, 1,3-butanediol and the like. These may be used alone or in combination of two or more.
 たばこシートにエアロゾル発生剤が含まれる場合、たばこシート100質量%に含まれるエアロゾル発生剤の割合は、4~50質量%であることが好ましい。前記エアロゾル発生剤の割合が4質量%以上であることにより、量の観点から加熱時に十分なエアロゾルを発生させることができる。また、前記エアロゾル発生剤の割合が50質量%以下であることにより、熱容量の観点から加熱時に十分なエアロゾルを発生させることができる。前記エアロゾル発生剤の割合は、6~40質量%であることがより好ましく、8~30質量%であることがさらに好ましく、10~20質量%であることが特に好ましい。 When the tobacco sheet contains an aerosol-generating agent, the ratio of the aerosol-generating agent contained in 100% by mass of the tobacco sheet is preferably 4 to 50% by mass. When the proportion of the aerosol-generating agent is 4% by mass or more, sufficient aerosol can be generated during heating from the viewpoint of quantity. In addition, since the proportion of the aerosol generating agent is 50% by mass or less, sufficient aerosol can be generated during heating from the viewpoint of heat capacity. The proportion of the aerosol generating agent is more preferably 6 to 40% by mass, even more preferably 8 to 30% by mass, and particularly preferably 10 to 20% by mass.
 (成型剤)
 本実施形態に係るたばこシートは、形状担保の観点から、さらに成型剤を含むことが好ましい。本実施形態に係るたばこシートは、特に、たばこシートのエアロゾル発生剤の保持性能と波型形状の維持性能とを十分に両立させることができる観点から、第一の成型剤及び第二の成型剤をさらに含むことが好ましい。ここで、第一の成型剤と第二の成型剤とは成型剤の種類が異なっていてもよく、成型剤の種類は同一で形態が異なっていてもよい。第一の成型剤としては、例えば多糖類、タンパク、合成ポリマー等が挙げられる。多糖類としては、例えばセルロース誘導体、天然由来の多糖類が挙げられる。
(molding agent)
The tobacco sheet according to the present embodiment preferably further contains a molding agent from the viewpoint of shape retention. In particular, the tobacco sheet according to the present embodiment has the first molding agent and the second molding agent from the viewpoint of being able to sufficiently achieve both the retention performance of the aerosol generating agent and the retention performance of the corrugated shape of the tobacco sheet. It is preferable to further include Here, the first molding agent and the second molding agent may be of different types, or the types of molding agents may be the same but the forms may be different. Examples of the first molding agent include polysaccharides, proteins, synthetic polymers and the like. Examples of polysaccharides include cellulose derivatives and naturally occurring polysaccharides.
 セルロース誘導体としては、例えば、メチルセルロース、エチルセルロース、ヒドロキシエチルセルロース、ヒドロキシメチルエチルセルロース、ヒドロキシプロピルセルロース、ヒドロキシプロピルメチルセルロース、ベンジルセルロース、トリチルセルロース、シアノエチルセルロース、カルボキシメチルセルロース、カルボキシエチルセルロース、アミノエチルセルロース等のセルロースエーテル類;酢酸セルロース、ギ酸セルロース、プロピオン酸セルロース、酪酸セルロース、安息香酸セルロース、フタル酸セルロース、トシルセルロース等の有機酸エステル;硝酸セルロース、硫酸セルロース、リン酸セルロース、セルロースキサントゲン酸塩等の無機酸エステル等が挙げられる。 Cellulose derivatives include, for example, cellulose ethers such as methylcellulose, ethylcellulose, hydroxyethylcellulose, hydroxymethylethylcellulose, hydroxypropylcellulose, hydroxypropylmethylcellulose, benzylcellulose, tritylcellulose, cyanoethylcellulose, carboxymethylcellulose, carboxyethylcellulose, aminoethylcellulose; Organic acid esters such as cellulose, cellulose formate, cellulose propionate, cellulose butyrate, cellulose benzoate, cellulose phthalate, and tosyl cellulose; and inorganic acid esters such as cellulose nitrate, cellulose sulfate, cellulose phosphate, and cellulose xanthate. be done.
 天然由来の多糖類としては、例えば、グアーガム、タラガム、ローストビーンガム、タマリンド種子ガム、ペクチン、アラビアガム、トラガントガム、カラヤガム、ガッティガム、アラビノガラクタン、アマシードガム、カッシャガム、サイリウムシードガム、サバクヨモギシードガム等の植物由来の多糖類;カラギーナン、寒天、アルギン酸、アルギン酸プロピレングリコールエステル、ファーセレラン、フクロノリ抽出物等の藻類由来の多糖類;キサンタンガム、ジェランガム、カードラン、プルラン、アグロバクテリウムスクシノグリカン、ウェランガム、マクロホモプシスガム、ラムザンガム等の微生物由来の多糖類;キチン、キトサン、グルコサミン等の甲殻類由来の多糖類;デンプン、デンプングリコール酸ナトリウム、α化デンプン、デキストリン等のデンプン等が挙げられる。 Examples of naturally-derived polysaccharides include guar gum, tara gum, roasted bean gum, tamarind seed gum, pectin, arabic gum, tragacanth gum, karaya gum, gutti gum, arabinogalactan, amaseed gum, cascha gum, psyllium seed gum, and mugwort seed gum. plant-derived polysaccharides; carrageenan, agar, alginic acid, propylene glycol alginate, furcelleran, algae-derived polysaccharides such as fukuronori extract; xanthan gum, gellan gum, curdlan, pullulan, Agrobacterium succinoglycan, welan gum, macro Microorganism-derived polysaccharides such as homopsis gum and rhamzan gum; crustacean-derived polysaccharides such as chitin, chitosan, and glucosamine; and starches such as starch, sodium starch glycolate, pregelatinized starch, and dextrin.
 タンパクとしては、例えば、小麦グルテン、ライ麦グルテン等の穀物タンパクが挙げられる。合成ポリマーとしては、例えば、ポリリン酸、ポリアクリル酸ナトリウム、ポリビニルピロリドン等が挙げられる。第二の成型剤としては、第一の成型剤とは異なるものの、第一の成型剤と同様の多糖類、タンパク、合成ポリマー等を用いることができる。 Examples of proteins include grain proteins such as wheat gluten and rye gluten. Synthetic polymers include, for example, polyphosphoric acid, sodium polyacrylate, polyvinylpyrrolidone, and the like. As the second molding agent, although different from the first molding agent, the same polysaccharides, proteins, synthetic polymers, etc. as those of the first molding agent can be used.
 たばこシートに第一の成型剤が含まれる場合、たばこシート100質量%に含まれる第一の成型剤の割合は、0.1~15質量%であることが好ましい。前記第一の成型剤の割合が0.1質量%以上であることにより、原料の混合体をシート状に容易に成型可能となる。また、前記第一の成型剤の割合が15質量%以下であることにより、非燃焼加熱型香味吸引器のたばこ含有セグメントに求められる機能を担保するための他原料を十分に用いることができる。前記第一の成型剤の割合は、0.1~12質量%であることがより好ましく、0.1~10質量%であることがさらに好ましく、0.1~7質量%であることが特に好ましい。 When the tobacco sheet contains the first molding agent, the ratio of the first molding agent contained in 100% by mass of the tobacco sheet is preferably 0.1 to 15% by mass. When the ratio of the first molding agent is 0.1% by mass or more, the raw material mixture can be easily molded into a sheet. Further, since the ratio of the first molding agent is 15% by mass or less, it is possible to sufficiently use other raw materials for securing the functions required for the tobacco-containing segment of the non-combustion heating type flavor inhaler. The proportion of the first molding agent is more preferably 0.1 to 12% by mass, even more preferably 0.1 to 10% by mass, particularly 0.1 to 7% by mass. preferable.
 たばこシートに第二の成型剤が含まれる場合、たばこシート100質量%に含まれる第二の成型剤の割合は、0.1~15質量%であることが好ましい。前記第二の成型剤の割合が0.1質量%以上であることにより、原料の混合体をシート状に容易に成型可能となる。また、前記第二の成型剤の割合が15質量%以下であることにより、非燃焼加熱型香味吸引器のたばこ含有セグメントに求められる機能を担保するための他原料を十分に用いることができる。前記第二の成型剤の割合は、0.1~12質量%であることがより好ましく、0.1~10質量%であることがさらに好ましく、0.1~7質量%であることが特に好ましい。 When the tobacco sheet contains the second molding agent, the ratio of the second molding agent contained in 100% by mass of the tobacco sheet is preferably 0.1 to 15% by mass. When the ratio of the second molding agent is 0.1% by mass or more, the raw material mixture can be easily molded into a sheet. Further, since the ratio of the second molding agent is 15% by mass or less, it is possible to sufficiently use other raw materials for securing the functions required for the tobacco-containing segment of the non-combustion heating type flavor inhaler. The proportion of the second molding agent is more preferably 0.1 to 12% by mass, even more preferably 0.1 to 10% by mass, particularly 0.1 to 7% by mass. preferable.
 また、第一の成型剤と第二の成型剤とが成型剤の種類が同一で形態が異なる場合、例えば第一の成型剤が粉末、第二の成型剤が溶液又はスラリー等であることができる。例えば、後述するたばこシートの製造方法において、第一の成型剤として成型剤を粉末として直接混合し、かつ、第二の成型剤として成型剤を水等の溶媒に分散又は膨潤させて混合することができる。このような方法でも、種類の異なる二つの成型剤を使用した場合と同様の効果が得られる。 Further, when the first molding agent and the second molding agent are the same type of molding agent but different in form, for example, the first molding agent may be powder and the second molding agent may be solution or slurry. can. For example, in the method of manufacturing a tobacco sheet described later, a molding agent is directly mixed as a powder as a first molding agent, and a molding agent is dispersed or swollen in a solvent such as water and mixed as a second molding agent. can be done. Such a method can also provide the same effect as when two molding agents of different types are used.
 (補強剤)
 本実施形態に係るたばこシートは、更なる物性向上の観点から、さらに補強剤を含むことができる。補強剤としては、例えばファイバー状パルプ、ファイバー状合成セルロース等の繊維状物質、ペクチン懸濁水など乾燥すると膜を形成する表面コーティング機能をもった液状物質等が挙げられる。これらは一種を用いてもよく、二種以上を併用してもよい。
(Reinforcing agent)
The tobacco sheet according to this embodiment may further contain a reinforcing agent from the viewpoint of further improving physical properties. Examples of the reinforcing agent include fibrous substances such as fibrous pulp and fibrous synthetic cellulose, and liquid substances such as pectin suspension having a surface coating function that forms a film when dried. These may be used alone or in combination of two or more.
 たばこシートに補強剤が含まれる場合、たばこシート100質量%に含まれる補強剤の割合は、4~40質量%であることが好ましい。本範囲内の場合、非燃焼加熱型香味吸引器のたばこ含有セグメントに求められる機能を担保するための他原料を十分に用いることができる。前記補強剤の割合は、4.5~35質量%であることがより好ましく、5~30質量%であることがさらに好ましい。 When the tobacco sheet contains a reinforcing agent, the proportion of the reinforcing agent contained in 100% by mass of the tobacco sheet is preferably 4 to 40% by mass. Within this range, other raw materials can be sufficiently used to secure the functions required for the tobacco-containing segment of the non-combustion-heating flavor inhaler. The ratio of the reinforcing agent is more preferably 4.5 to 35% by mass, more preferably 5 to 30% by mass.
 (保湿剤)
 本実施形態に係るたばこシートは、品質保持の観点から、さらに保湿剤を含むことができる。保湿剤としては、例えばソルビトール、エリスリトール、キシリトール、マルチトール、ラクチトール、マンニトール、還元麦芽糖水飴等の糖アルコール等が挙げられる。これらは一種を用いてもよく、二種以上を併用してもよい。
(moisturizer)
The tobacco sheet according to this embodiment may further contain a humectant from the viewpoint of maintaining quality. Examples of moisturizing agents include sugar alcohols such as sorbitol, erythritol, xylitol, maltitol, lactitol, mannitol, and reduced maltose starch syrup. These may be used alone or in combination of two or more.
 たばこシートに保湿剤が含まれる場合、たばこシート100質量%に含まれる保湿剤の割合は、1~15質量%であることが好ましい。本範囲内の場合、非燃焼加熱型香味吸引器のたばこ含有セグメントに求められる機能を担保するための他原料を十分に用いることができる。前記保湿剤の割合は、2~12質量%であることがより好ましく、3~10質量%であることがさらに好ましい。 When the tobacco sheet contains a humectant, the ratio of the humectant contained in 100% by mass of the tobacco sheet is preferably 1 to 15% by mass. Within this range, other raw materials can be sufficiently used to secure the functions required for the tobacco-containing segment of the non-combustion-heating flavor inhaler. The ratio of the moisturizing agent is more preferably 2 to 12% by mass, even more preferably 3 to 10% by mass.
 (その他の成分)
 本実施形態に係るたばこシートは、前記たばこ原料、前記エアロゾル発生剤、前記成型剤(第一及び第二の成型剤)、前記補強剤、前記保湿剤以外にも、必要に応じて香料、呈味料等の香味料、着色剤、湿潤剤、保存料、無機物質等の希釈剤等を含むことができる。
(other ingredients)
The tobacco sheet according to the present embodiment may contain, in addition to the tobacco raw material, the aerosol-generating agent, the molding agent (first and second molding agents), the reinforcing agent, and the moisturizing agent, if necessary, a flavoring agent and a flavoring agent. Flavoring agents such as seasonings, coloring agents, humectants, preservatives, diluents such as inorganic substances, and the like can be included.
 (膨嵩性)
 本実施形態に係るたばこシートの膨嵩性は、190cc/100g以上であることが好ましい。該膨嵩性が190cc/100g以上であることにより、非燃焼加熱型香味吸引器のたばこ含有セグメントの総熱容量を十分に低減することができ、たばこ含有セグメントに充填されたたばこシートがエアロゾル生成により寄与できるようになる。該膨嵩性は210cc/100g以上であることがより好ましく、230cc/100g以上であることがさらに好ましい。該膨嵩性の範囲の上限は特に限定されないが、例えば800cc/100g以下であることができる。なお、該膨嵩性は、たばこシートを0.8mm×20mmのサイズに裁刻し、22℃、60%の調和室内で48時間存置した後、DD-60A(商品名、ボルグワルド社製)にて測定される値である。測定は、裁刻されたたばこシート15gを内径60mmの円筒形容器に入れ、3kg荷重で30秒圧縮した時の容積を求めることで行われる。
(Bulkiness)
It is preferable that the tobacco sheet according to the present embodiment has a swelling property of 190 cc/100 g or more. When the swelling property is 190 cc/100 g or more, the total heat capacity of the tobacco-containing segment of the non-combustion heating type flavor inhaler can be sufficiently reduced, and the tobacco sheet filled in the tobacco-containing segment is generated by aerosol generation. be able to contribute. The swelling property is more preferably 210 cc/100 g or more, more preferably 230 cc/100 g or more. Although the upper limit of the swelling range is not particularly limited, it can be, for example, 800 cc/100 g or less. The swelling property was evaluated by cutting a tobacco sheet into a size of 0.8 mm×20 mm, leaving it in a conditioned room at 22° C. and 60% for 48 hours, and applying it to DD-60A (trade name, manufactured by Borgwald). It is a value measured by The measurement is carried out by placing 15 g of cut tobacco sheets in a cylindrical container with an inner diameter of 60 mm and compressing the container with a load of 3 kg for 30 seconds to obtain the volume.
 [たばこシートの製造方法]
 本実施形態に係るたばこシートは、例えばたばこ原料、エアロゾル発生剤、第一の成型剤、及び第二の成型剤を含む混合物を調製する工程と、前記混合物を圧延して圧延成形品を形成する工程と、前記圧延成形品に回転式ロール刃を押し当てて短冊状に切断しつつ波型形状を付与する工程と、を含むことができる。なお、波型形状を付与する処理をリップリング処理ともいう。例えば、以下の方法により本実施形態に係るたばこシートを製造することができる。
[Manufacturing method of tobacco sheet]
The tobacco sheet according to the present embodiment is produced by, for example, preparing a mixture containing a tobacco raw material, an aerosol-generating agent, a first molding agent, and a second molding agent, and rolling the mixture to form a rolled product. and a step of pressing a rotary roll blade against the rolled product to cut it into strips and imparting a corrugated shape. Note that the process of imparting a wave shape is also called a rippling process. For example, the tobacco sheet according to this embodiment can be produced by the following method.
 (1)水、たばこ原料、エアロゾル発生剤、第一及び第二の成型剤、及び補強剤を混合して混合物を得る工程。
 (2)当該混合物を複数の圧延ローラーに投入して圧延し、圧延成形品を得る工程。
 (3)圧延成形品に対して回転式ロール刃を押し当て、短冊状に切断しつつ波型形状を付与する工程。
(1) A step of mixing water, a tobacco raw material, an aerosol-generating agent, first and second molding agents, and a reinforcing agent to obtain a mixture.
(2) A step of rolling the mixture into a plurality of rolling rollers to obtain a rolled product.
(3) A step of pressing a rotary roll blade against the rolled product to cut it into strips and imparting a corrugated shape.
 回転式ロール刃により短冊状に切断されたシートは、ロールから剥離される時に抵抗力が掛かることで、図1に示されるような波型形状及び鋸歯形状が付与される。なお、圧延成形品を回転式ロール刃により切断しない場合には、例えば圧延ローラー上の圧延成形品をドクターナイフで剥離することで、ロールから剥離される時に抵抗力が掛かり、同様に波型形状及び鋸歯形状を付与することができる。また、前記方法でたばこシートを製造する場合、目的に応じて、圧延ローラーの表面を加温又は冷却してもよく、圧延ローラーの回転数を調整してもよい。さらに、圧延ローラーの間隔を調整することで、所望の坪量のたばこシートを得ることができる。 A sheet cut into strips by a rotary roll blade is given a wavy shape and sawtooth shape as shown in FIG. In the case where the rolled product is not cut by a rotary roll blade, for example, by peeling off the rolled product on the rolling roller with a doctor knife, resistance is applied when peeled from the roll, and the wavy shape is also applied. and a sawtooth shape. In the case of producing a tobacco sheet by the above method, the surface of the pressure roller may be heated or cooled, and the number of revolutions of the pressure roller may be adjusted depending on the purpose. Furthermore, by adjusting the spacing between the rolling rollers, it is possible to obtain a tobacco sheet with a desired basis weight.
 [非燃焼加熱型香味吸引器]
 本実施形態に係る非燃焼加熱型香味吸引器は、本実施形態に係るたばこシート等を含むたばこ含有セグメントを備える。本実施形態に係る非燃焼加熱型香味吸引器は、本実施形態に係る膨嵩性の高いたばこシート等が充填されたたばこ含有セグメントを備えるため、たばこ含有セグメントの総熱容量を十分に低減することができ、たばこ含有セグメントに充填されたたばこシートがエアロゾル生成により寄与できるようになる。
[Non-combustion heating flavor inhaler]
The non-combustion-heating flavor inhaler according to this embodiment includes a tobacco-containing segment including the tobacco sheet or the like according to this embodiment. Since the non-combustion-heating flavor inhaler according to the present embodiment includes the tobacco-containing segment filled with the highly bulky tobacco sheet or the like according to the present embodiment, the total heat capacity of the tobacco-containing segment should be sufficiently reduced. , allowing the tobacco sheet filled in the tobacco-containing segment to contribute more to aerosol generation.
 本実施形態に係る非燃焼加熱型香味吸引器の一例を図2に示す。図2に示される非燃焼加熱型香味吸引器4は、本実施形態に係るたばこシート等が充填されたたばこ含有セグメント5と、周上に穿孔11を有する筒状の冷却セグメント6と、センターホールセグメント7と、フィルターセグメント8と、を備える。本実施形態に係る非燃焼加熱型香味吸引器は、たばこ含有セグメント、冷却セグメント、センターホールセグメント及びフィルターセグメント以外にも、他のセグメントを有していてもよい。 An example of the non-combustion heating type flavor inhaler according to this embodiment is shown in FIG. The non-combustion heating type flavor inhaler 4 shown in FIG. It comprises a segment 7 and a filter segment 8 . The non-combustion-heating flavor inhaler according to this embodiment may have segments other than the tobacco-containing segment, cooling segment, center hole segment, and filter segment.
 本実施形態に係る非燃焼加熱型香味吸引器の軸方向の長さは特に限定されないが、40mm以上、90mm以下であることが好ましく、50mm以上、75mm以下であることがより好ましく、50mm以上、60mm以下であることがさらに好ましい。また、非燃焼加熱型香味吸引器の周の長さは16mm以上、25mm以下であることが好ましく、20mm以上、24mm以下であることがより好ましく、21mm以上、23mm以下であることがさらに好ましい。例えば、たばこ含有セグメントの長さは20mm、冷却セグメントの長さは20mm、センターホールセグメントの長さは8mm、フィルターセグメントの長さは7mmである態様を挙げることができる。なお、フィルターセグメントの長さは4mm以上、10mm以下の範囲内で選択可能である。また、その際のフィルターセグメントの通気抵抗は、セグメント当たり15mmHO/seg以上、60mmHO/seg以下であるように選択される。これら個々のセグメント長さは、製造適性、要求品質等に応じて、適宜変更できる。さらには、センターホールセグメントを用いずに、冷却セグメントの下流側にフィルターセグメントのみを配置しても、非燃焼加熱型香味吸引器として機能させることができる。 The axial length of the non-combustion heating type flavor inhaler according to the present embodiment is not particularly limited, but is preferably 40 mm or more and 90 mm or less, more preferably 50 mm or more and 75 mm or less, 50 mm or more, It is more preferably 60 mm or less. The circumference of the non-combustion heating flavor inhaler is preferably 16 mm or more and 25 mm or less, more preferably 20 mm or more and 24 mm or less, and even more preferably 21 mm or more and 23 mm or less. For example, the length of the tobacco-containing segment is 20 mm, the length of the cooling segment is 20 mm, the length of the center hole segment is 8 mm, and the length of the filter segment is 7 mm. In addition, the length of the filter segment can be selected within a range of 4 mm or more and 10 mm or less. Also, the ventilation resistance of the filter segments at that time is selected to be 15 mmH 2 O/seg or more and 60 mmH 2 O/seg or less per segment. These individual segment lengths can be changed as appropriate according to manufacturability, required quality, and the like. Furthermore, even if only the filter segment is arranged on the downstream side of the cooling segment without using the center hole segment, it can be made to function as a non-combustion heating type flavor inhaler.
 (たばこ含有セグメント)
 たばこ含有セグメント5は、本実施形態に係るたばこシートが巻紙(以下、ラッパーともいう)内に充填されている。たばこシートを巻紙内に充填する方法は特に限定されないが、例えばたばこシートをラッパーで包んでもよく、筒状のラッパー内にたばこシートを充填してもよい。たばこシートの形状が矩形状のように長手方向を有する場合、たばこシートは該長手方向がラッパー内でそれぞれ不特定の方向となるように充填されていてもよく、たばこ含有セグメント5の軸方向又は該軸方向に対して垂直な方向となるように整列させて充填されていてもよい。
(segment containing tobacco)
In the tobacco-containing segment 5, the tobacco sheet according to the present embodiment is filled in wrapping paper (hereinafter also referred to as wrapper). The method of packing the tobacco sheet into the wrapping paper is not particularly limited. For example, the tobacco sheet may be wrapped in a wrapper, or the tobacco sheet may be packed in a cylindrical wrapper. When the shape of the tobacco sheet has a longitudinal direction such as a rectangular shape, the tobacco sheet may be packed so that the longitudinal direction is in an unspecified direction in the wrapper, and the tobacco-containing segment 5 may be packed in an axial direction or a longitudinal direction. They may be aligned and filled in a direction perpendicular to the axial direction.
 (冷却セグメント)
 図2に示されるように、冷却セグメント6は筒状部材10で構成される態様を挙げることができる。筒状部材10は例えば厚紙を円筒状に加工した紙管であってもよい。
(cooling segment)
As shown in FIG. 2, the cooling segment 6 may be configured by a cylindrical member 10. As shown in FIG. The tubular member 10 may be, for example, a paper tube formed by processing cardboard into a cylindrical shape.
 筒状部材10及び後述するマウスピースライニングペーパー15には、両者を貫通する穿孔11が設けられている。穿孔11の存在により、吸引時に外気が冷却セグメント6内に導入される。これにより、たばこ含有セグメント5が加熱されることで生成したエアロゾル気化成分が外気と接触し、その温度が低下するため液化し、エアロゾルが形成される。穿孔11の径(差し渡し長さ)は特に限定されないが、例えば0.5mm以上、1.5mm以下であってもよい。穿孔11の数は特に限定されず、1つでも2つ以上でもよい。例えば穿孔11は冷却セグメント6の周上に複数設けられていてもよい。 The tubular member 10 and the mouthpiece lining paper 15, which will be described later, are provided with perforations 11 penetrating both. Due to the presence of the perforations 11 outside air is introduced into the cooling segment 6 during suction. As a result, the vaporized aerosol component generated by heating the tobacco-containing segment 5 comes into contact with the outside air, and its temperature decreases, liquefying to form an aerosol. The diameter (spanning length) of the perforations 11 is not particularly limited, but may be, for example, 0.5 mm or more and 1.5 mm or less. The number of perforations 11 is not particularly limited, and may be one or two or more. For example, a plurality of perforations 11 may be provided on the circumference of the cooling segment 6 .
 穿孔11から導入される外気量は、使用者により吸引される気体全体の体積に対して85体積%以下が好ましく、80体積%以下がより好ましい。前記外気量の割合が85体積%以下であることにより、外気によって希釈されることによる香味の低減を十分に抑制することができる。なお、これを別の言い方ではベンチレーション割合ともいう。ベンチレーション割合の範囲の下限は、冷却性の観点から、55体積%以上が好ましく、60体積%以上がより好ましい。 The amount of outside air introduced from the perforations 11 is preferably 85% by volume or less, more preferably 80% by volume or less, relative to the total volume of the gas inhaled by the user. When the ratio of the amount of outside air is 85% by volume or less, it is possible to sufficiently suppress reduction in flavor due to dilution by outside air. In other words, this is also called a ventilation ratio. From the viewpoint of cooling performance, the lower limit of the ventilation ratio range is preferably 55% by volume or more, more preferably 60% by volume or more.
 また、冷却セグメントは、しわ付けされた、ひだ付けされた、ギャザー加工された、又は折り畳まれた適切な構成材料のシートを含むセグメントであってもよい。そのような要素の断面プロフィールは、ランダムに向いたチャネルを示す場合がある。また、冷却セグメントは、縦方向延在チューブの束を含んでいてもよい。このような冷却セグメントは、例えば、ひだ付け、ギャザー付け、又は折り畳まれたシート材料を巻紙で巻装して形成することができる。 The cooling segment may also be a segment comprising a crumpled, pleated, gathered or folded sheet of suitable construction material. The cross-sectional profile of such elements may exhibit randomly oriented channels. The cooling segment may also include a bundle of longitudinally extending tubes. Such cooling segments may be formed, for example, from pleated, gathered, or folded sheet material wrapped with wrapping paper.
 冷却セグメントの軸方向の長さは、例えば7mm以上、28mm以下であることができ、例えば18mmであることができる。また、冷却セグメントは、その軸方向断面形状として実質的に円形であることができ、その直径は例えば5mm以上、10mm以下であることができ、例えば約7mmであることができる。 The axial length of the cooling segment can be, for example, 7 mm or more and 28 mm or less, and can be, for example, 18 mm. Also, the cooling segment can be substantially circular in its axial cross-sectional shape, and its diameter can be, for example, 5 mm or more and 10 mm or less, and can be, for example, about 7 mm.
 (センターホールセグメント)
 センターホールセグメントは1つまたは複数の中空部を有する充填層と、該充填層を覆うインナープラグラッパー(内側巻紙)とで構成される。例えば、図2に示されるように、センターホールセグメント7は、中空部を有する第二の充填層12と、第二の充填層12を覆う第二のインナープラグラッパー13とで構成される。センターホールセグメント7は、マウスピースセグメント9の強度を高める機能を有する。第二の充填層12は、例えば酢酸セルロース繊維が高密度で充填されトリアセチンを含む可塑剤が酢酸セルロース質量に対して、6質量%以上、20質量%以下添加されて硬化された内径φ1.0mm以上、φ5.0mm以下のロッドとすることができる。第二の充填層12は繊維の充填密度が高いため、吸引時は、空気やエアロゾルは中空部のみを流れることになり、第二の充填層12内はほとんど流れない。センターホールセグメント7内部の第二の充填層12が繊維充填層であることから、使用時の外側からの触り心地は、使用者に違和感を生じさせることが少ない。なお、センターホールセグメント7が第二のインナープラグラッパー13を持たず、熱成型によってその形が保たれていてもよい。
(center hole segment)
The center hole segment is composed of a filling layer having one or more hollow portions and an inner plug wrapper (inner wrapping paper) covering the filling layer. For example, as shown in FIG. 2, the center hole segment 7 is composed of a second filling layer 12 having a hollow portion and a second inner plug wrapper 13 covering the second filling layer 12 . The center hole segment 7 has the function of increasing the strength of the mouthpiece segment 9 . The second filling layer 12 has an inner diameter of φ1.0 mm, for example, filled with cellulose acetate fibers at a high density and hardened by adding a plasticizer containing triacetin in an amount of 6% by mass or more and 20% by mass or less based on the mass of cellulose acetate. As described above, a rod having a diameter of 5.0 mm or less can be obtained. Since the second packed layer 12 has a high packing density of fibers, air and aerosol flow only through the hollow portion and hardly flow inside the second packed layer 12 during suction. Since the second filling layer 12 inside the center hole segment 7 is a fiber filling layer, the feeling of touch from the outside during use hardly causes the user to feel uncomfortable. Note that the center hole segment 7 may not have the second inner plug wrapper 13 and may retain its shape by thermoforming.
 (フィルターセグメント)
 フィルターセグメント8の構成は特に限定されないが、単数または複数の充填層から構成されてよい。充填層の外側は一枚または複数枚の巻紙で巻装されてよい。フィルターセグメント8のセグメント当たりの通気抵抗は、フィルターセグメント8に充填される充填物の量、材料等により適宜変更することができる。例えば、充填物が酢酸セルロース繊維である場合、フィルターセグメント8に充填される酢酸セルロース繊維の量を増加させれば、通気抵抗を増加させることができる。充填物が酢酸セルロース繊維である場合、酢酸セルロース繊維の充填密度は0.13~0.18g/cmであることができる。なお、通気抵抗は通気抵抗測定器(商品名:SODIMAX、SODIM製)により測定される値である。
(filter segment)
Although the configuration of the filter segment 8 is not particularly limited, it may be composed of a single or a plurality of packed layers. The outer side of the packing layer may be wrapped with one or more wrapping papers. The ventilation resistance per segment of the filter segment 8 can be appropriately changed depending on the amount of filler, the material, etc. with which the filter segment 8 is filled. For example, when the filler is cellulose acetate fiber, increasing the amount of cellulose acetate fiber with which the filter segment 8 is filled can increase the ventilation resistance. When the filler is cellulose acetate fiber, the packing density of the cellulose acetate fiber can be 0.13-0.18 g/cm 3 . The airflow resistance is a value measured by an airflow resistance measuring instrument (trade name: SODIMAX, manufactured by SODIM).
 フィルターセグメント8の周の長さは特に限定されないが、16~25mmであることが好ましく、20~24mmであることがより好ましく、21~23mmであることがさらに好ましい。フィルターセグメント8の軸方向の長さは4~10mmを選択可能であり、その通気抵抗が15~60mmHO/segとなるように選択される。フィルターセグメント8の軸方向の長さは5~9mmが好ましく、6~8mmがより好ましい。フィルターセグメント8の断面の形状は特に限定されないが、例えば円形、楕円形、多角形等であることができる。また、フィルターセグメント8には香料を含んだ破壊性カプセル、香料ビーズ、香料を直接添加していてもよい。 Although the length of the circumference of the filter segment 8 is not particularly limited, it is preferably 16 to 25 mm, more preferably 20 to 24 mm, even more preferably 21 to 23 mm. The axial length of the filter segment 8 can be selected from 4 to 10 mm, and is selected so that its ventilation resistance is from 15 to 60 mmH 2 O/seg. The axial length of the filter segment 8 is preferably 5-9 mm, more preferably 6-8 mm. The cross-sectional shape of the filter segment 8 is not particularly limited, but may be, for example, circular, elliptical, polygonal, or the like. In addition, the filter segment 8 may be directly added with destructible capsules containing perfume, perfume beads, and perfume.
 図2に示されるように、センターホールセグメント7と、フィルターセグメント8とはアウタープラグラッパー(外側巻紙)14で接続できる。アウタープラグラッパー14は、例えば円筒状の紙であることができる。また、たばこ含有セグメント5と、冷却セグメント6と、接続済みのセンターホールセグメント7及びフィルターセグメント8とは、マウスピースライニングペーパー15により接続できる。これらの接続は、例えばマウスピースライニングペーパー15の内側面に酢酸ビニル系糊等の糊を塗り、前記3つのセグメントを入れて巻くことで接続することができる。なお、これらのセグメントは複数のライニングペーパーで複数回に分けて接続されていてもよい。 As shown in FIG. 2 , the center hole segment 7 and the filter segment 8 can be connected with an outer plug wrapper (outer wrapping paper) 14 . The outer plug wrapper 14 can be, for example, a cylinder of paper. Further, the tobacco-containing segment 5 , cooling segment 6 , connected center hole segment 7 and filter segment 8 can be connected by mouthpiece lining paper 15 . These connections can be made, for example, by applying glue such as vinyl acetate glue to the inner surface of the mouthpiece lining paper 15, inserting the three segments, and winding them. In addition, these segments may be divided into multiple times and connected with multiple lining papers.
 [非燃焼加熱型香味吸引システム]
 本実施形態に係る非燃焼加熱型香味吸引システムは、本実施形態に係る非燃焼加熱型香味吸引器と、該非燃焼加熱型香味吸引器のたばこ含有セグメントを加熱する加熱装置と、を備える。本実施形態に係る非燃焼加熱型香味吸引システムは、本実施形態に係る非燃焼加熱型香味吸引器及び前記加熱装置以外に、他の構成を有していてもよい。
[Non-combustion heating type flavor suction system]
The non-combustion heating flavor inhalation system according to this embodiment includes the non-combustion heating flavor inhaler according to this embodiment, and a heating device that heats the tobacco-containing segment of the non-combustion heating flavor inhaler. The non-combustion-heating flavor inhalation system according to the present embodiment may have a configuration other than the non-combustion-heating flavor inhaler and the heating device according to the present embodiment.
 本実施形態に係る非燃焼加熱型香味吸引システムの一例を図3に示す。図3に示される非燃焼加熱型香味吸引システムは、本実施形態に係る非燃焼加熱型香味吸引器4と、非燃焼加熱型香味吸引器4のたばこ含有セグメントを外側から加熱する加熱装置16とを備える。 An example of the non-combustion heating type flavor suction system according to this embodiment is shown in FIG. The non-combustion heating flavor inhalation system shown in FIG. 3 includes a non-combustion heating flavor inhaler 4 according to this embodiment and a heating device 16 that heats the tobacco-containing segment of the non-combustion heating flavor inhaler 4 from the outside. Prepare.
 図3(a)は非燃焼加熱型香味吸引器4を加熱装置16に挿入する前の状態を示し、図3(b)は非燃焼加熱型香味吸引器4を加熱装置16に挿入して加熱する状態を示す。図3に示される加熱装置16は、ボディ17と、ヒーター18と、金属管19と、電池ユニット20と、制御ユニット21とを備える。ボディ17は筒状の凹部22を有し、凹部22の内側側面であって、凹部22に挿入される非燃焼加熱型香味吸引器4のたばこ含有セグメントと対応する位置に、ヒーター18及び金属管19が配置されている。ヒーター18は電気抵抗によるヒーターであることができ、温度制御を行う制御ユニット21からの指示により電池ユニット20より電力が供給され、ヒーター18の加熱が行われる。ヒーター18から発せられた熱は、熱伝導度の高い金属管19を通じて非燃焼加熱型香味吸引器4のたばこ含有セグメントへ伝えられる。 FIG. 3(a) shows the state before the non-combustion heating flavor inhaler 4 is inserted into the heating device 16, and FIG. indicates the state of The heating device 16 shown in FIG. 3 includes a body 17, a heater 18, a metal tube 19, a battery unit 20, and a control unit 21. The body 17 has a cylindrical recess 22, and a heater 18 and a metal pipe are provided on the inner side surface of the recess 22 at positions corresponding to the tobacco-containing segments of the non-combustion heating flavor inhaler 4 inserted into the recess 22. 19 are arranged. The heater 18 can be a heater based on electric resistance, and electric power is supplied from the battery unit 20 according to an instruction from the control unit 21 that performs temperature control, and the heater 18 is heated. The heat emitted from the heater 18 is transmitted to the tobacco-containing segment of the non-combustion heating flavor inhaler 4 through the metal pipe 19 with high thermal conductivity.
 図3(b)においては、模式的に図示しているため、非燃焼加熱型香味吸引器4の外周と金属管19の内周との間に隙間があるが、実際は、熱を効率的に伝達する目的で非燃焼加熱型香味吸引器4の外周と金属管19の内周との間に隙間は無い方が望ましい。なお、加熱装置16は非燃焼加熱型香味吸引器4のたばこ含有セグメントを外側から加熱するが、内側から加熱するものであってもよい。 In FIG. 3(b), there is a gap between the outer circumference of the non-combustion-heating flavor inhaler 4 and the inner circumference of the metal tube 19 because it is schematically illustrated. For the purpose of transmission, it is desirable that there is no gap between the outer circumference of the non-combustion heating flavor inhaler 4 and the inner circumference of the metal tube 19 . The heating device 16 heats the tobacco-containing segment of the non-combustion-heating flavor inhaler 4 from the outside, but it may heat the tobacco-containing segment from the inside.
 加熱装置による加熱温度は特に限定されないが、400℃以下であることが好ましく、150℃以上400℃以下であることがより好ましく、200℃以上350℃以下であることがさらに好ましい。なお、加熱温度とは加熱装置のヒーターの温度を示す。 Although the heating temperature of the heating device is not particularly limited, it is preferably 400°C or lower, more preferably 150°C or higher and 400°C or lower, and even more preferably 200°C or higher and 350°C or lower. The heating temperature indicates the temperature of the heater of the heating device.
 さらに非燃焼加熱型香味吸引器には、香喫味阻害感(刺激)または不快感の低減が求められている。香喫味阻害感とは、吸入時の口腔や喉への刺激を意味する。以下、香喫味阻害感または不快感を低減させた非燃焼加熱型香味吸引器用たばこシートについて説明する。 In addition, non-combustion heating type flavor inhalers are required to reduce the sense of flavor inhibition (irritation) or discomfort. The sense of inhibition of flavor and taste means irritation to the oral cavity and throat upon inhalation. Hereinafter, a tobacco sheet for a non-combustion heating type flavor inhaler with reduced sense of inhibition of flavor and taste or discomfort will be described.
[第1の態様]
 本態様において非燃焼加熱型香味吸引器用たばこシートは、フルクタンを含む。当該たばこシートを喫煙に供すると、フルクタンが熱分解して持続的に甘い香気を発生させる。発生した持続的な甘い香気は、喫煙行動の初期から後期まで継続して香喫味阻害感を抑制することができる。
[First aspect]
In this aspect, the tobacco sheet for a non-combustion heating type flavor inhaler contains fructans. When the tobacco sheet is smoked, the fructans are thermally decomposed to generate a persistent sweet aroma. The persistent sweet aroma that is generated can continue from the early stage to the late stage of smoking behavior and suppress the feeling of inhibition of flavor and taste.
 上記フルクタンとしては、特に限定されないが、イヌリン型フルクタン、レバン型フルクタン、分岐型フルクタン、フラクトオリゴ糖、又はこれらのうちの2種以上の組み合わせを使用することができる。これらの中でも、コスト抑制の観点より、イヌリン型フルクタンが好ましい。 The above fructans are not particularly limited, but inulin-type fructans, levan-type fructans, branched fructans, fructooligosaccharides, or a combination of two or more of these can be used. Among these, inulin-type fructans are preferable from the viewpoint of cost reduction.
 理論に拘束されないが、本態様のフルクタンがカラメル化反応により甘い香気を発生させる際には以下のような特徴があると推定される。
 フルクタンは、複数の単糖類が結合して形成されており、かつ単糖類及び二糖類より大きな分子構造を有する。そのため、フルクタンがカラメル化反応を起こす際には、単糖類、二糖類などの比較的小さい分子の糖に分解した後、これらの単糖類や二糖類がカラメル化反応を起こして甘い香気を発生させるという多段階の分解工程を経ると考えられる。一方、単糖類や二糖類がカラメル化反応を起こす際には、それらの糖がカラメル化反応を起こして甘い香気を直接発生させると考えられる。したがって、フルクタンは、単糖類や二糖類に比べて、分解工程が多い分だけ遅い速度で甘い香気を発生させ、かつ長時間にわたって甘い香気を発生させることができると考えられる。本態様においては、このようなフルクタンのカラメル化反応に関する特徴により、喫煙行動の初期から後期まで継続して香喫味阻害感を抑制することができると考えられる。
Although not bound by theory, it is presumed that the fructan of this embodiment has the following characteristics when it produces a sweet aroma through caramelization reaction.
Fructans are formed by binding multiple monosaccharides and have a larger molecular structure than monosaccharides and disaccharides. Therefore, when fructans undergo a caramelization reaction, they are decomposed into relatively small sugar molecules such as monosaccharides and disaccharides, and then these monosaccharides and disaccharides undergo a caramelization reaction to generate a sweet aroma. It is thought that it goes through a multi-stage decomposition process. On the other hand, when monosaccharides and disaccharides undergo a caramelization reaction, it is believed that these sugars undergo a caramelization reaction to directly generate a sweet aroma. Therefore, compared to monosaccharides and disaccharides, fructans are considered to be able to generate a sweet aroma at a slower rate due to the increased number of decomposition processes, and to generate a sweet aroma over a long period of time. In this embodiment, it is thought that the inhibition of flavor and taste can be suppressed continuously from the early stage to the late stage of smoking behavior due to such characteristics related to the caramelization reaction of fructans.
 いくつかの実施形態において、前記たばこシート100質量%に対するフルクタンの含有量は、特に限定されないが、0.1~5質量%、0.3~3.5質量%、又は0.5~3質量%とすることができる。香喫阻害感を抑制する観点や香喫阻害感抑制の持続性の観点からは、フルクタンの含有量は多い方が好ましい。一方、フルクタンの含有量が多すぎると香味が低減してしまう場合もあるため、香喫阻害感の抑制及びその持続性と香味とを両立する観点からは、フルクタンの含有量は0.5~3質量%が好ましい。 In some embodiments, the fructan content relative to 100% by mass of the tobacco sheet is not particularly limited, but is 0.1 to 5% by mass, 0.3 to 3.5% by mass, or 0.5 to 3% by mass. %. From the viewpoint of suppressing the feeling of inhibition of smoking and the persistence of suppression of the inhibition of smoking, the fructan content is preferably as high as possible. On the other hand, if the fructan content is too high, the flavor may be reduced. Therefore, from the viewpoint of suppressing the feeling of inhibition of smoking flavor and maintaining the flavor and flavor, the fructan content is 0.5 to 0.5. 3% by weight is preferred.
 本態様において、たばこ原料は、たばこ葉、熟成済たばこ葉、加工済たばこ葉、たばこ充填物、非たばこ材、又はこれらのうちの2種以上の組み合わせを更に含むことができる。 In this aspect, the tobacco raw material can further include tobacco leaves, aged tobacco leaves, processed tobacco leaves, tobacco fillers, non-tobacco materials, or a combination of two or more of these.
 <たばこ葉、熟成済たばこ葉、及び加工済たばこ葉>
 「たばこ葉」とは、収穫されたたばこの葉が、後述する熟成を経る前のものの総称である。なお、熟成の一態様にはキュアリングが含まれる。これに対して、熟成を経たたばこ葉であって、たばこ製品で利用される種々の形態(後述するたばこ刻や、たばこシート、たばこ顆粒等)に加工される前のものを「熟成済たばこ葉」と称する。さらに、熟成済たばこ葉を、たばこ製品で利用される種々の形態に加工したものを「加工済たばこ葉」と称する。
<Tobacco leaves, aged tobacco leaves, and processed tobacco leaves>
“Tobacco leaves” is a general term for harvested tobacco leaves before undergoing ripening, which will be described later. One mode of aging includes curing. On the other hand, aged tobacco leaves before being processed into various forms used in tobacco products (such as cut tobacco, tobacco sheets, tobacco granules, etc.) are referred to as "aged tobacco leaves." ”. Furthermore, the aged tobacco leaves processed into various forms used in tobacco products are referred to as "processed tobacco leaves".
 たばこ製品で利用される加工済たばこ葉の形態としては、例えば、熟成済たばこ葉を所定の大きさに刻んだ「たばこ刻」を挙げることができる。また、熟成済たばこ葉を所定の粒径となるように粉砕したもの(以下、「たばこ細粉」ともいう。)を含む組成物を、シート形状に成形して得られる「たばこシート」や、顆粒形状に成形して得られる「たばこ顆粒」を挙げることもできる。なお、前記「たばこ細粉」も加工済たばこ葉の一形態である。 As a form of processed tobacco leaves used in tobacco products, for example, "cut tobacco" in which matured tobacco leaves are chopped into a predetermined size can be mentioned. Also, a "tobacco sheet" obtained by molding a composition containing matured tobacco leaves pulverized to a predetermined particle size (hereinafter also referred to as "tobacco fine powder") into a sheet shape, Mention may also be made of "tobacco granules" obtained by molding into granular form. The above-mentioned "tobacco powder" is also one form of processed tobacco leaves.
 非たばこ材としては、植物の根(鱗根(鱗茎)、塊根(イモ類)、球根などを含む)、茎、塊茎、皮(茎皮、樹皮などを含む)、葉、花(花弁、雌蕊、雄蕊などを含む)、若しくは種実、又は樹木の幹や枝等を挙げることができる。 Non-tobacco materials include plant roots (including scales (bulbs), tuberous roots (potatoes), bulbs, etc.), stems, tubers, skins (including stem bark, bark, etc.), leaves, flowers (petals, pistils, etc.). , stamens, etc.), seeds, or tree trunks and branches.
 フルクタンを含むたばこシートの製造方法は限定されない。本願のいくつかの実施形態において、上述のたばこシートを調製し、外部からフルクタンを供給することにより、製造することができる。具体的には、前記圧延成形品にフルクタンを供給することが好ましい。圧延成形品は、波型形状を付与される前であっても後であってもよい。 The manufacturing method of tobacco sheets containing fructans is not limited. In some embodiments of the present application, it can be manufactured by preparing the tobacco sheets described above and supplying fructans from the outside. Specifically, it is preferable to supply fructans to the rolled product. The roll-formed article may be before or after being given the corrugated shape.
[第2の態様]
 本態様において非燃焼加熱型香味吸引器用たばこシートは、飽和脂肪酸系添加剤を含む。
 本態様においてたばこシートはオリエント種由来の材料を含んでいてもよい。その場合、前記たばこ原料に対するオリエント種由来の材料の含有量は10質量%以下であることが好ましい。オリエント種由来の材料の含有量がこの範囲であると不快感をより低減させた喫味を提供できる。この観点から、前記含有量の上限は、好ましくは8質量%以下、より好ましくは5質量%以下である。その下限は、好ましくは0.1質量%以上、より好ましくは2質量%以上、さらに好ましくは3質量%以上である。
[Second aspect]
In this aspect, the tobacco sheet for a non-combustion heating type flavor inhaler contains a saturated fatty acid additive.
In this aspect, the tobacco sheet may contain materials derived from Orient species. In that case, the content of the material derived from the Orient species is preferably 10% by mass or less with respect to the tobacco raw material. When the content of the material derived from the Orient species is within this range, it is possible to provide a taste with less discomfort. From this point of view, the upper limit of the content is preferably 8% by mass or less, more preferably 5% by mass or less. The lower limit is preferably 0.1% by mass or more, more preferably 2% by mass or more, and still more preferably 3% by mass or more.
 飽和脂肪酸系添加剤は、モル質量が200~350g/molである飽和脂肪酸、当該飽和脂肪酸のエステル、およびこれらの組合せからなる群より選択される。前記飽和脂肪酸は、喫煙時の不快感を低減する。前記飽和脂肪酸のエステルは、アルコールとモル質量が200~350g/molである飽和脂肪酸とから得られるので、アルコールのモル質量によって当該エステルのモル質量は変動する。当該エステルのモル質量は一態様において210~1300g/molである。飽和脂肪酸のエステルは、一般に脂肪酸よりも蒸気圧が低いため喫煙時の不快感低減効果を喫煙の終始にわたって持続させる。以下、喫煙時の不快感低減効果を単に不快感低減効果ともいう。 The saturated fatty acid additive is selected from the group consisting of saturated fatty acids having a molar mass of 200-350 g/mol, esters of the saturated fatty acids, and combinations thereof. The saturated fatty acid reduces discomfort during smoking. Said esters of saturated fatty acids are obtained from alcohols and saturated fatty acids having a molar mass of 200 to 350 g/mol, so that the molar mass of the ester varies with the molar mass of the alcohol. The molar mass of the ester is in one embodiment from 210 to 1300 g/mol. Esters of saturated fatty acids generally have a lower vapor pressure than fatty acids, so that the effect of reducing discomfort during smoking is sustained throughout smoking. Hereinafter, the effect of reducing discomfort during smoking is also simply referred to as the effect of reducing discomfort.
 前記効果を奏する観点から、前記飽和脂肪酸エステルのモル質量の下限値は好ましくは240g/mol以上、より好ましくは270g/mol以上である。その上限値は1140g/mol以下、1112g/mol以下、300g/mol以下、または290g/mol以下であることが好ましい。 From the viewpoint of achieving the above effects, the lower limit of the molar mass of the saturated fatty acid ester is preferably 240 g/mol or more, more preferably 270 g/mol or more. The upper limit is preferably 1140 g/mol or less, 1112 g/mol or less, 300 g/mol or less, or 290 g/mol or less.
 飽和脂肪酸系添加剤の含有量は、前記たばこ原料の乾物合計質量当たり(乾物質量を100質量%として)0.01~3質量%である。当該含有量が下限値未満であると不快感低減効果が十分でなく、また上限値を超えると異臭感が増大する。この観点から、含有量の下限値は好ましくは1質量%以上であり、その上限値は好ましくは2質量%以下である。乾物質量とは、後述する媒体を除いた質量であり、好ましくは当該組成物を100℃で5時間乾燥した際の残留物の質量である。 The content of the saturated fatty acid-based additive is 0.01 to 3% by mass based on the total dry matter mass of the tobacco raw material (assuming the dry matter content is 100% by mass). If the content is less than the lower limit, the effect of reducing discomfort is not sufficient, and if the content exceeds the upper limit, the offensive odor increases. From this point of view, the lower limit of the content is preferably 1% by mass or more, and the upper limit is preferably 2% by mass or less. The amount of dry substance is the mass excluding the medium described later, preferably the mass of the residue when the composition is dried at 100° C. for 5 hours.
 飽和脂肪酸および前記エステルにおける脂肪酸部位の炭素数は12~20であることが好ましく、15~19であることがより好ましい。炭素数がこの範囲であると、不快感低減効果がより顕著となる。
 飽和脂肪酸系添加剤における飽和脂肪酸の、水に対する溶解度は、好ましくは0.15mg/g以下であり、より好ましくは0.12mg/g以下である。またその下限値は限定されず0mg/gであってもよいが、好ましくは0.05mg/g以上である。
The number of carbon atoms in the fatty acid portion of the saturated fatty acid and the ester is preferably 12-20, more preferably 15-19. When the number of carbon atoms is within this range, the effect of reducing discomfort becomes more pronounced.
The water solubility of the saturated fatty acid in the saturated fatty acid additive is preferably 0.15 mg/g or less, more preferably 0.12 mg/g or less. The lower limit is not limited and may be 0 mg/g, preferably 0.05 mg/g or more.
 前記飽和脂肪酸の好ましい具体例としては、オクタン酸、デカン酸、ミリスチン酸、パルミチン酸、ステアリン酸、およびノナデカン酸が挙げられる。中でも、入手容易性および不快感低減効果発現の観点から、パルミチン酸、ステアリン酸、またはノナデカン酸が好ましい。当該飽和脂肪酸は混合物であってもよいが、混合物ではない単品であることが好ましい。本態様において単品(単一化合物)とは、化合物が純品である場合、または化合物が不可避的に含有される不純物を含んでいる場合を含む。したがって、一態様において飽和脂肪酸はパルミチン酸のみからなる。当該飽和脂肪酸が単品であると、本発明のたばこ組成物をシート等の成形物とするときに、成形物における飽和脂肪酸の分散性が向上する。 Preferred specific examples of the saturated fatty acids include octanoic acid, decanoic acid, myristic acid, palmitic acid, stearic acid, and nonadecanoic acid. Among them, palmitic acid, stearic acid, or nonadecanic acid is preferable from the viewpoint of availability and expression of discomfort-reducing effect. Although the saturated fatty acid may be a mixture, it is preferably a single product rather than a mixture. In this embodiment, the single product (single compound) includes the case where the compound is a pure product, or the case where the compound contains impurities that are unavoidably contained. Thus, in one aspect the saturated fatty acids consist exclusively of palmitic acid. If the saturated fatty acid is a single product, the dispersibility of the saturated fatty acid in the molded article such as a sheet is improved when the tobacco composition of the present invention is formed into the molded article.
 前記飽和脂肪酸のエステル(以下単に「エステル」ともいう)の好ましい具体例としては、前述の飽和脂肪酸のアルキルエステルおよび糖エステルが挙げられる。アルキル部位は、メチル基等の炭素数1~10の直鎖状、分岐状、または環状のアルキル基由来であることが好ましい。また、糖部位は、ショ糖などの二糖類由来であることが好ましい。好ましい前記エステルの例としては、パルミチン酸ショ糖エステルおよびパルミチン酸メチルが挙げられる。当該エステルにおける飽和脂肪酸部位は、前述の理由から単品の飽和脂肪酸に由来することが好ましい。当該エステルにおけるアルコール部位は、単品である必要はないが前述の理由から単品であることが好ましい。前記エステルは乳化剤としての機能も有する。 Preferable specific examples of the ester of saturated fatty acid (hereinafter also simply referred to as "ester") include the aforementioned alkyl ester and sugar ester of saturated fatty acid. The alkyl moiety is preferably derived from a linear, branched or cyclic alkyl group having 1 to 10 carbon atoms such as a methyl group. Also, the sugar moiety is preferably derived from a disaccharide such as sucrose. Examples of preferred said esters include sucrose palmitate and methyl palmitate. The saturated fatty acid moiety in the ester is preferably derived from a single saturated fatty acid for the reasons described above. Although the alcohol moiety in the ester does not have to be a single product, it is preferably a single product for the reason described above. The ester also functions as an emulsifier.
 一態様において飽和脂肪酸系添加剤は、前記飽和脂肪酸と前記エステルを含む。この場合、不快感低減効果をより持続できるという利点がある。また、用いるたばこ原料等によって、飽和脂肪酸系添加剤の種類を適宜選択することもできる。よって、本態様は汎用的であるという利点も備える。 In one aspect, the saturated fatty acid additive contains the saturated fatty acid and the ester. In this case, there is an advantage that the effect of reducing discomfort can be maintained longer. Also, the type of saturated fatty acid additive can be appropriately selected depending on the tobacco raw material used. Therefore, this aspect also has the advantage of being versatile.
 飽和脂肪酸系添加剤の一部または全部は粉末であることが好ましい。飽和脂肪酸系添加剤が粉末であると、後述するとおりシート等の成形体とした場合に成形体において飽和脂肪酸系添加剤の分散性が向上する。そのサイズは限定されないが、例えば、D50は好ましくは30~120μmであり、より好ましくは50~100μmである。また、前記分散性の観点から飽和脂肪酸系添加剤は、蝋や天然油脂に比べて結晶化度が高いことが好ましい。 A part or all of the saturated fatty acid additive is preferably powder. When the saturated fatty acid-based additive is a powder, the dispersibility of the saturated fatty acid-based additive is improved in the molded article such as a sheet, as will be described later. Although its size is not limited, for example, D50 is preferably 30-120 μm, more preferably 50-100 μm. From the viewpoint of dispersibility, the saturated fatty acid additive preferably has a higher degree of crystallinity than wax or natural oils and fats.
 たばこシートは液糖を含んでいてもよい。液糖とは液状の糖である。たばこシートが液糖を含むと、喫煙時の不快感の低減に加えて甘み感が向上する。この観点から、液糖の含有量は、たばこ組成物中の乾物質量当たり、好ましくは3~10質量%であり、より好ましくは5~8質量%である。 The tobacco sheet may contain liquid sugar. Liquid sugar is liquid sugar. When the tobacco sheet contains liquid sugar, the feeling of sweetness is improved in addition to reducing discomfort during smoking. From this point of view, the liquid sugar content is preferably 3 to 10% by mass, more preferably 5 to 8% by mass, based on the amount of dry matter in the tobacco composition.
 たばこシートは天然植物性香料を含んでいてもよい。たばこシートが天然植物性香料を含むと、不快感低減効果に加えて、甘み感が向上する。この観点から、天然植物性香料の含有量は、たばこ組成物中の乾物質量当たり、好ましくは0.5~3質量%であり、より好ましくは2~3質量%である。天然植物性香料としてはたばこ分野において公知のものを使用できるが、本発明においてはリコリスが好ましい。リコリスとはマメ科カンゾウ属であるスペインカンゾウ由来の甘味料である。 "Tobacco sheets may contain natural plant fragrances." When the tobacco sheet contains a natural vegetable flavor, in addition to the effect of reducing unpleasantness, the feeling of sweetness is improved. From this point of view, the content of the natural plant flavor is preferably 0.5 to 3% by mass, more preferably 2 to 3% by mass, based on the amount of dry matter in the tobacco composition. Natural botanical flavors that are known in the field of tobacco can be used, but licorice is preferred in the present invention. Licorice is a sweetener derived from Spanish licorice, which belongs to the genus Glycyrrhiza of the legume family.
 本態様におけるたばこシートに含まれるニコチンの量は限定されないが、一態様においてたばこシートの乾物質量当たり、2質量%以上とすることができる。一般にニコチンの量が増えると喫煙時の不快感が増大する傾向にあるが、本態様においては前述のとおり不快感低減効果が奏されるので、ニコチン量が前記範囲である場合に本態様の効果がより顕著となる。前記ニコチン量の上限は限定されないが、現実的には3質量%以下である。 The amount of nicotine contained in the tobacco sheet in this aspect is not limited, but in one aspect it can be 2% by mass or more based on the amount of dry matter in the tobacco sheet. In general, when the amount of nicotine increases, discomfort during smoking tends to increase. becomes more pronounced. Although the upper limit of the amount of nicotine is not limited, it is practically 3% by mass or less.
 別態様において、前記ニコチンの量を1.5質量%以下とすることができる。ニコチン量が前記範囲であるとよりマイルドな香喫味を与えることができる。前記ニコチン量の下限は限定されないが、現実的には0.1質量%以上である。たばこシートに含まれるニコチンは前記たばこ原料に由来してもよいし、他の成分に由来してもよい。 In another aspect, the amount of nicotine can be 1.5% by mass or less. When the amount of nicotine is within the above range, a milder flavor and taste can be imparted. Although the lower limit of the amount of nicotine is not limited, it is practically 0.1% by mass or more. The nicotine contained in the tobacco sheet may be derived from the tobacco raw material, or may be derived from other components.
 本態様におけるたばこシートは、前述のエアロゾル発生剤を含むことができる。エアロゾル発生剤の量は、たばこシートの乾物質量当たり、好ましくは12質量%以下、より好ましくは11質量%以下である。また、その下限値は限定されず0質量%でもよく、好ましくは1質量%以上である。エアロゾル発生剤の量が上限値を超えるとシートの製造が困難となるおそれがあり、下限値未満であると煙感量が低下するおそれがある。 The tobacco sheet in this aspect can contain the aforementioned aerosol-generating agent. The amount of aerosol-generating agent is preferably 12% by weight or less, more preferably 11% by weight or less, based on the dry matter weight of the tobacco sheet. Moreover, the lower limit is not limited, and may be 0% by mass, preferably 1% by mass or more. If the amount of the aerosol-generating agent exceeds the upper limit, the production of the sheet may become difficult, and if it is less than the lower limit, the smoke sensitivity may decrease.
 たばこシートがバインダーを含むと、シートの強度が向上する。バインダーは繊維同士等を結合するための接着剤である。バインダーとしては、当該分野において公知のものを使用できる。バインダーとしては、ガム類、修飾セルロース、および修飾でんぷん等の増粘多糖類が挙げられる。バインダーの量は用途に応じて適宜調製されるが、例えばたばこシートの乾物質量当たり、1~10質量%程度とすることができる。 When the tobacco sheet contains a binder, the strength of the sheet is improved. A binder is an adhesive for binding fibers together. As the binder, those known in the art can be used. Binders include thickening polysaccharides such as gums, modified celluloses, and modified starches. The amount of the binder is appropriately adjusted depending on the application, and can be, for example, about 1 to 10% by mass based on the amount of dry matter of the tobacco sheet.
 本態様におけるたばこシートは任意の方法で製造される。例えば、前記混合物を調製する際に、飽和脂肪酸系添加剤を混合して、当該添加剤は配合された混合物とし、これを用いて前述の方法でシートを製造できる。その際、粉末の飽和脂肪酸系添加剤を用いて、その粉末状態を保つように混合することが好ましい。このように製造されたたばこシートは、エアロゾル発生剤の分散性が良好となる。分散性が良好であるとは、飽和脂肪酸系添加剤が均一に分散していることをいう。混合工程は飽和脂肪酸系添加剤の融点以下で実施することが好ましい。例えば、この工程は10~50℃で実施することができる。 The tobacco sheet in this aspect is manufactured by any method. For example, when preparing the mixture, a saturated fatty acid-based additive is mixed to obtain a mixture containing the additive, and the sheet can be produced by the method described above. At that time, it is preferable to use a powdery saturated fatty acid-based additive and mix so as to maintain the powdery state. The tobacco sheet produced in this way has good dispersibility of the aerosol generating agent. Good dispersibility means that the saturated fatty acid additive is uniformly dispersed. The mixing step is preferably carried out below the melting point of the saturated fatty acid additive. For example, this step can be carried out at 10-50°C.
 飽和脂肪酸系添加剤を含む混合物(「スラリー」ともいう)は、以下の工程を備える方法で製造されることが好ましい。
 前記たばこ原料またはファイバー状たばこ材料と、一部または全部が粉末である飽和脂肪酸系添加剤と、媒体とを、前記粉末が粉末状態を保つように混合してスラリーとする工程。
A mixture (also referred to as “slurry”) containing a saturated fatty acid-based additive is preferably produced by a method comprising the following steps.
A step of mixing the tobacco raw material or fibrous tobacco material, a saturated fatty acid-based additive that is partly or entirely powdered, and a medium so as to maintain the powdery state to form a slurry.
 当該方法では、飽和脂肪酸系添加剤が粉末状態を保ったままスラリーを調製する。このようにすることで、成形体とした際に成分(B)の分散性が向上する。当該粉末のサイズについては前述のとおりである。飽和脂肪酸系添加剤が粉末状態を保つとは、その一部または全部が粉末状態を保つことをいう。 In this method, the slurry is prepared while the saturated fatty acid-based additive remains powdery. By doing so, the dispersibility of the component (B) is improved when the molding is formed. The size of the powder is as described above. The fact that the saturated fatty acid additive maintains a powdery state means that part or all of it maintains a powdery state.
 媒体としては、水および親水性有機溶媒が挙げられるが、取り扱い上、最も好ましい媒体は水である。 The medium includes water and hydrophilic organic solvents, but the most preferable medium for handling is water.
 本方法は、まず、室温で固体の材料を粉砕等によって粉末とし、これらを混合して粉末混合物を得る。一方で、媒体等の室温で液体またはペースト状の材料を混合して液体混合物を得る。そして粉末混合物と液体混合物を混合する工程を備えることが好ましい。 In this method, first, a material that is solid at room temperature is pulverized into powder, and these are mixed to obtain a powder mixture. On the other hand, liquid or pasty materials such as medium are mixed at room temperature to obtain a liquid mixture. Then, it is preferable to include a step of mixing the powder mixture and the liquid mixture.
 粉末状の飽和脂肪酸系添加剤を媒体中に良好に分散させる観点から、スラリーの25℃での粘度は、100,000~200,000(mPa・s)であることが好ましい。粘度はB型粘度計(Brookfield製 DV―I prime)を用いて、スピンドルNo.LV4を用いて、回転数1.0rpmで測定される。 The viscosity of the slurry at 25°C is preferably 100,000 to 200,000 (mPa·s) from the viewpoint of good dispersion of the powdery saturated fatty acid additive in the medium. The viscosity was measured using a Brookfield viscometer (Brookfield DV-I prime). Measured at 1.0 rpm using LV4.
[第3の態様]
 本態様においてたばこ含有セグメント(以下単に「たばこセグメント」ともいう)は、紙、またはエアロゾル発生剤を含有する紙を含む。本態様におけるたばこセグメントの概要を図4Aに示す。たばこセグメント20Aは、たばこ充填物21と、その周囲を巻装するラッパー22を備える。たばこ充填物21は、前記たばこシートTと紙Pを含む。当該図では、たばこシートTはこれを裁断して得たストランド状であり、紙Pもストランド形状である。ストランドは、たばこシートTと紙Pを積層したシートを裁断したものであってもよい。なお本態様を説明する図において、たばこシートTの波型形状の図示は省略してある。
[Third aspect]
In this embodiment, the tobacco-containing segment (hereinafter also simply referred to as "tobacco segment") includes paper or paper containing an aerosol-generating agent. A schematic of a tobacco segment in this embodiment is shown in FIG. 4A. The tobacco segment 20A comprises a tobacco filler 21 and a wrapper 22 surrounding it. The tobacco filling 21 includes the tobacco sheet T and the paper P. In the figure, the tobacco sheet T has a strand shape obtained by cutting it, and the paper P also has a strand shape. The strand may be obtained by cutting a sheet in which the tobacco sheet T and the paper P are laminated. Note that the wavy shape of the tobacco sheet T is omitted in the drawings for explaining this embodiment.
 図4Bは、シート状のたばこ充填物21を渦巻き状にラッパー22内に充填する態様を示す。シート状のたばこ充填物21は、たばこシートTと紙Pを積層したシートであってもよいし、たばこシートTと紙Pの側面同士または側面近傍部を接合して得たシートであってもよい。 FIG. 4B shows a mode in which the sheet-like tobacco filler 21 is spirally filled into the wrapper 22 . The sheet-shaped tobacco filler 21 may be a sheet in which the tobacco sheet T and the paper P are laminated, or may be a sheet obtained by joining the side surfaces of the tobacco sheet T and the paper P together or in the vicinity of the side surfaces. good.
 図4Cは、シート状のたばこ充填物21を折り畳んでラッパー22内に充填する態様を示す。シート状のたばこ充填物21は、たばこシートTと紙Pを積層したシートであってもよいし、たばこシートTと紙Pの側面同士または側面近傍部を接合して得たシートであってもよい。 FIG. 4C shows a mode in which the sheet-like tobacco filler 21 is folded and filled into the wrapper 22. FIG. The sheet-shaped tobacco filler 21 may be a sheet in which the tobacco sheet T and the paper P are laminated, or may be a sheet obtained by joining the side surfaces of the tobacco sheet T and the paper P together or in the vicinity of the side surfaces. good.
 図4Dは、刻状のたばこ充填物21をラッパー22内に充填する態様を示す。当該図では、たばこシートTから得た刻と刻状紙Pをそれぞれ準備してこれらを充填する態様を示した。刻は、たばこシートTと紙Pを積層したシートを裁刻したものであってもよい。 FIG. 4D shows a mode of filling the shredded tobacco filler 21 into the wrapper 22. FIG. The drawing shows a manner in which chopped pieces of tobacco sheet T and chopped paper P are prepared and filled. The cut may be obtained by cutting a sheet obtained by stacking the tobacco sheet T and the paper P.
 図4Eは、シート状のたばこ充填物21を縦方向および横方向から圧縮して丸め、これをラッパー22内に充填する態様を示す。シート状のたばこ充填物21は、たばこシートTと紙Pを積層したシートであってもよいし、たばこシートTと紙Pの側面同士または側面近傍部を接合して得たシートであってもよい。 FIG. 4E shows a mode in which the sheet-like tobacco filler 21 is rolled up by being compressed in the vertical and horizontal directions and then filled into the wrapper 22 . The sheet-shaped tobacco filler 21 may be a sheet in which the tobacco sheet T and the paper P are laminated, or may be a sheet obtained by joining the side surfaces of the tobacco sheet T and the paper P together or in the vicinity of the side surfaces. good.
(1)紙
(1-1)第3-1の態様
 たばこセグメントは第3-1の態様として、充填物として、たばこシートと、リグニンおよびヘミセルロースの合計含有量が0.1~10質量%である紙を含む。当該充填物とは、たばこセグメント用の充填物である。リグニンとは木等に含まれる高分子フェノール化合物である。ヘミセルロースとは細胞壁に含まれる不溶性の多糖類である。この合計量がこの範囲であると、喫煙時の異臭(繊維臭等)を低減することができる。すなわち本態様では、本来の香喫味を大きく阻害することなく香喫味を希釈できるという効果が奏される。この観点から、リグニンおよびヘミセルロースの合計含有量の上限は9.0質量%以下であることが好ましい。
(1) Paper (1-1) Aspect 3-1 The tobacco segment, as an aspect 3-1, has a total content of tobacco sheet, lignin and hemicellulose of 0.1 to 10% by mass as a filler. Including some paper. The filling is a filling for tobacco segments. Lignin is a high-molecular phenolic compound contained in trees and the like. Hemicellulose is an insoluble polysaccharide contained in cell walls. When the total amount is within this range, offensive odors (such as fiber odors) during smoking can be reduced. That is, in this aspect, the effect of diluting the flavor and taste without greatly impairing the original flavor and taste is exhibited. From this point of view, the upper limit of the total content of lignin and hemicellulose is preferably 9.0% by mass or less.
 リグニンおよびヘミセルロースは公知の方法で測定されるが、本発明においては以下の方法で測定されることが好ましい。
[ヘミセルロースの定量]
 1)紙を、溶媒として水を用いた溶媒抽出に供し、残渣を分離する。液体窒素等を用いて当該残渣を凍結粉砕して試料Aとする。
 2)試料Aと酵素を反応させて、反応生成物を回収する。
 3)反応生成物を加水分解し、加水分解物について波長490nmで吸光度測定を行い、ヘミセルロースを定量する。
Lignin and hemicellulose are measured by known methods, but in the present invention, they are preferably measured by the following methods.
[Quantification of hemicellulose]
1) The paper is subjected to solvent extraction using water as solvent to separate the residue. A sample A is obtained by freeze-pulverizing the residue using liquid nitrogen or the like.
2) The sample A is reacted with the enzyme, and the reaction product is recovered.
3) The reaction product is hydrolyzed, and the hydrolyzate is subjected to absorbance measurement at a wavelength of 490 nm to quantify hemicellulose.
 工程1)は、例えば、Thermo ScientificTM DionexTM ASETM 高速溶媒抽出システム(型番:ASE-350)を使用することができる。 For step 1), for example, a Thermo Scientific™ Dionex™ ASET™ high-speed solvent extraction system (model number: ASE-350) can be used.
 工程2)は、具体的に以下のように実施できる。
 50mgの試料Aをスクリュー瓶に入れ、超純水(ML-Q水)8.5mlとパンクレアチン溶液0.5mlを加え、40℃、125rpmで16時間振盪する。パンクレアチン溶液とは、pH6.4の0.1Mリン酸緩衝液100mlに8gのパンクレアチンを加えて1時間撹拌した後、8000rpmで30分遠心分離した上清である。次いでML-Q水を用いて前記試料液体を、15mlの遠沈管に移し、8000rpmで15分間遠心分離して、上清を取り除く。この洗浄を三回繰り返し行う。洗浄後、5%硫酸水溶液10mlを加え、100℃にて2.5時間加水分解を行う。加水分解反応終了後、試料を室温まで放冷する。次いで、沈殿物をろ別し、ろ液を250mlのメスフラスコに回収する。ろ紙上の残渣をML-Q水で十分に洗浄した後、250mlに定容する。この溶液をヘミセルロース測定用試料とする。当該試料500μlを20ml試験管に移し、5%フェノール水溶液500μlと濃硫酸2.5mlを加え、十秒間激しく撹拌する。当該試料を室温にて20分以上放置し、分光光度計を使用して波長490nmで吸光度測定を行い、ヘミセルロースを定量する。
Step 2) can be specifically implemented as follows.
Put 50 mg of sample A in a screw bottle, add 8.5 ml of ultrapure water (ML-Q water) and 0.5 ml of pancreatin solution, and shake at 40° C. and 125 rpm for 16 hours. The pancreatin solution is the supernatant obtained by adding 8 g of pancreatin to 100 ml of 0.1 M phosphate buffer of pH 6.4, stirring for 1 hour, and centrifuging at 8000 rpm for 30 minutes. The sample liquid is then transferred to a 15 ml centrifuge tube using ML-Q water and centrifuged at 8000 rpm for 15 minutes to remove the supernatant. This wash is repeated three times. After washing, 10 ml of a 5% sulfuric acid aqueous solution is added, and hydrolysis is performed at 100° C. for 2.5 hours. After the hydrolysis reaction is completed, the sample is allowed to cool to room temperature. The precipitate is then filtered off and the filtrate collected in a 250 ml volumetric flask. After thoroughly washing the residue on the filter paper with ML-Q water, the volume is adjusted to 250 ml. This solution is used as a sample for hemicellulose measurement. Transfer 500 μl of the sample to a 20 ml test tube, add 500 μl of 5% phenol aqueous solution and 2.5 ml of concentrated sulfuric acid, and stir vigorously for 10 seconds. The sample is left at room temperature for 20 minutes or longer, and absorbance is measured at a wavelength of 490 nm using a spectrophotometer to quantify hemicellulose.
[リグニンの定量]
 i)前記試料Aを準備する。
 ii)試料Aを酸水溶液中で還流し、還流処理後の試料をろ別する。
 iii)ろ別した試料を乾燥後、秤量してリグニン量とする。
[Quantification of lignin]
i) preparing said sample A;
ii) The sample A is refluxed in an acid aqueous solution, and the sample after the reflux treatment is filtered.
iii) The filtered sample is dried and then weighed to determine the amount of lignin.
 工程ii)、iii)は、具体的に以下のように実施できる。
 100mgの試料Aをスクリュー瓶に入れ、72%硫酸4mlを加え、硫酸に試料を完全に浸らせ、30℃、200rpmにて4時間振盪する。次いで、希釈後の硫酸濃度が4%となるよう超純水(ML-Q水)157.2mlを加えてナスフラスコに移し、110℃のオイルバス中で2時間加熱還流を行う。室温まで放冷後、ろ過を行い、ロータリー乾熱機で乾燥し秤量する。
Steps ii) and iii) can be specifically performed as follows.
100 mg of sample A is placed in a screw bottle, 4 ml of 72% sulfuric acid is added, the sample is completely immersed in sulfuric acid, and shaken at 30° C. and 200 rpm for 4 hours. Next, 157.2 ml of ultrapure water (ML-Q water) is added so that the concentration of sulfuric acid after dilution becomes 4%, transferred to an eggplant flask, and heated under reflux in an oil bath at 110° C. for 2 hours. After allowing to cool to room temperature, filter, dry with a rotary dryer, and weigh.
 本態様で用いる紙の密度は、好ましくは0.05~0.8(g/cm)であり、より好ましくは0.1~0.6(g/cm)である。密度は公知の方法で測定されるが、下記式で求めることが好ましい。
 密度 (g/cm)=重さ(g)/面積(cm)/厚さ(cm)
The density of the paper used in this embodiment is preferably 0.05 to 0.8 (g/cm 3 ), more preferably 0.1 to 0.6 (g/cm 3 ). Although density is measured by a known method, it is preferably determined by the following formula.
Density (g/cm 3 ) = weight (g)/area (cm 2 )/thickness (cm)
 本態様で用いる紙の含有量は、前記たばこシートの乾物質量に対し、好ましくは5~70質量%、より好ましくは10~50質量%、さらに好ましくは15~40質量%である。紙の含有量が当該範囲であると、本来の香喫味を阻害することなく、香喫味を適正なレベルに希釈できる。乾物質量とは、一態様においてたばこシートを100℃で5時間乾燥した際の残留物の質量である。 The content of the paper used in this embodiment is preferably 5-70% by mass, more preferably 10-50% by mass, still more preferably 15-40% by mass, relative to the dry matter content of the tobacco sheet. When the content of the paper is within this range, the flavor and taste can be diluted to an appropriate level without impairing the original flavor and taste. Dry matter content is, in one embodiment, the weight of the residue after drying the tobacco sheet at 100° C. for 5 hours.
 本態様で用いられる紙は、リグニンおよびヘミセルロースの合計含有量が前記範囲であれば限定されず、例えばラッパー等のたばこ用紙や、上質印刷用紙、中質印刷用紙等の印刷用紙を用いることができる。ただし、異臭の発生を抑制する観点から、非塗工紙または微塗工紙であることが好ましい。また、本態様で用いられる紙は、後述するエアロゾル発生剤を含んでいてもよいし、含んでいなくてもよい。その量は、第3-2の態様で説明する範囲であってもよいし、これ以外の範囲であってもよい。 The paper used in this embodiment is not limited as long as the total content of lignin and hemicellulose is within the above range. . However, from the viewpoint of suppressing the generation of offensive odors, non-coated paper or lightly coated paper is preferred. Moreover, the paper used in this embodiment may or may not contain an aerosol generating agent, which will be described later. The amount may be in the range described in the 3-2 aspect, or may be in a range other than this.
(1-2)第3-2の態様
 たばこセグメントは、第3-2の態様として、充填物として、たばこシートと、エアロゾル発生剤を含有する紙とを含む。エアロゾル発生剤とは、加熱により気化し冷却されてエアロゾルを生成するあるいは霧化によってエアロゾルを生成する材料である。本態様ではエアロゾル発生剤を含む紙を用いるので、煙量を低下させることなく香喫味を希釈できるという効果が奏される。エアロゾル発生剤としては前述ものを用いることができる。その量は、前記紙の乾物質量当たり、好ましくは3~20質量%、より好ましくは5~15質量%である。エアロゾル発生剤の量が上限値を超えるとたばこセグメントにしみ等が発生することがあり、下限値未満であると煙感量が低下するおそれがある。含浸または噴霧等により、エアロゾル発生剤を紙に添加することができる。
(1-2) Aspect 3-2 The tobacco segment includes, as an aspect 3-2, a tobacco sheet and a paper containing an aerosol-generating agent as fillers. An aerosol-generating agent is a material that is vaporized by heating and then cooled to form an aerosol or atomized to form an aerosol. Since paper containing an aerosol-generating agent is used in this embodiment, it is possible to dilute the flavor and taste without reducing the amount of smoke. As the aerosol generating agent, those described above can be used. The amount is preferably 3 to 20% by weight, more preferably 5 to 15% by weight, based on the dry matter content of said paper. If the amount of the aerosol-generating agent exceeds the upper limit, stains and the like may occur on the tobacco segment, and if it is less than the lower limit, the smoke sensitivity may decrease. Aerosol-generating agents can be added to the paper, such as by impregnation or spraying.
 前記エアロゾル発生剤を添加した紙の含有量は、前記たばこシートの乾物質量に対して、好ましくは5~75質量%、より好ましくは10~50質量%、さらに好ましくは15~40質量%である。 The content of the paper to which the aerosol generating agent is added is preferably 5 to 75% by mass, more preferably 10 to 50% by mass, still more preferably 15 to 40% by mass, relative to the dry matter content of the tobacco sheet. .
 本態様で用いられる紙は、限定されず、第3-1の態様で説明した紙であってもよい。本態様で用いられるエアロゾル発生剤を添加する前の紙の密度は、第3-1の態様で説明する範囲であってもよいし、これ以外の範囲であってもよい。また本態様で用いられる紙に含まれるリグニンおよびヘミセルロースの量は限定されず、第3-1の態様で説明する範囲であってもよいし、これ以外の範囲であってもよい。 The paper used in this aspect is not limited, and may be the paper described in the 3-1 aspect. The density of the paper before adding the aerosol generating agent used in this embodiment may be within the range described in Embodiment 3-1, or may be within a range other than this. In addition, the amount of lignin and hemicellulose contained in the paper used in this embodiment is not limited, and may be within the range described in Embodiment 3-1, or may be within a range other than this.
(1-3)形状等
 いずれの態様においても、紙の形状は限定されず、たばこシートと混合されやすい形状であればよい。一態様において紙は、シート、刻、またはストランドである。また、好ましい態様において、紙とたばこシートとの形状は同様であり、最も好ましい態様では、紙の刻とたばこシートの刻を使用する。
(1-3) Shape, etc. In any of the embodiments, the shape of the paper is not limited as long as it is easily mixed with the tobacco sheet. In one aspect, the paper is a sheet, cut, or strand. Also, in preferred embodiments, the shapes of the paper and tobacco sheets are similar, and in the most preferred embodiment, shredded paper and shredded tobacco sheets are used.
 また、紙にはメントール等の当該分野で通常用いられている香料などが添加されていてもよい。 In addition, the paper may be added with menthol and other fragrances that are commonly used in the relevant field.
 以下、本実施形態の具体例について説明するが、本発明はこれらに限定されない。 Specific examples of the present embodiment will be described below, but the present invention is not limited to these.
 [実施例1]
 たばこラミナ(葉たばこ)をホソカワミクロンACM機にて乾式粉砕し、たばこ粉末を得た。該たばこ粉末について、マスターサイザー(商品名、スペクトリス株式会社マルバーン・パナリティカル事業部製)を用いて、乾式レーザー回折法により測定される体積基準の粒度分布における累積90%粒子径(D90)を測定したところ、200μmであった。
[Example 1]
Tobacco lamina (leaf tobacco) was dry pulverized with a Hosokawa Micron ACM machine to obtain tobacco powder. For the tobacco powder, the cumulative 90% particle diameter (D90) in the volume-based particle size distribution measured by the dry laser diffraction method is measured using a Mastersizer (trade name, manufactured by Spectris Co., Ltd., Malvern Panalytical Division). As a result, it was 200 μm.
 前記たばこ粉末をたばこ原料として用いて、たばこシートを製造した。具体的には、前記たばこ原料70質量部と、エアロゾル発生剤としてのグリセリン12質量部と、第一の成型剤としての粉末状のカルボキシメチルセルロース4質量部と、第二の成型剤としての水で膨潤させたカルボキシメチルセルロース1質量部と、補強剤としての繊維状パルプ5質量部と、香料としてのココアパウダー8質量部とを混合し、押出成形機にて混練した。混練物を2対の金属製ロールにてシート状に成型して圧延成形品を得た。該圧延成形品に対して製麺用回転式ロール刃を押し当て、短冊状に切断しつつ波型形状を付与した。さらに長さが20mmとなるように切断し、乾燥することで、長さ:20mm、幅:0.8mmのたばこシートを得た。該たばこシートの厚み方向断面は、図1に示されるような断面形状を有していた。 A tobacco sheet was manufactured using the tobacco powder as a tobacco raw material. Specifically, 70 parts by mass of the tobacco raw material, 12 parts by mass of glycerin as an aerosol generating agent, 4 parts by mass of powdered carboxymethyl cellulose as a first molding agent, and water as a second molding agent. 1 part by mass of swollen carboxymethylcellulose, 5 parts by mass of fibrous pulp as a reinforcing agent, and 8 parts by mass of cocoa powder as a flavoring agent were mixed and kneaded in an extruder. The kneaded product was formed into a sheet by two pairs of metal rolls to obtain a rolled product. A rotary roll blade for noodle making was pressed against the rolled product, and the product was cut into strips and given a corrugated shape. Further, it was cut into 20 mm lengths and dried to obtain tobacco sheets with a length of 20 mm and a width of 0.8 mm. The thickness direction cross-section of the tobacco sheet had a cross-sectional shape as shown in FIG.
 得られたたばこシートについて、膨嵩性を測定した。具体的には、たばこシートを22℃、60%の調和室内で48時間存置した後、DD-60A(商品名、ボルグワルド社製)にて膨嵩性を測定した。測定は、たばこシート15gを内径60mmの円筒形容器に入れ、3kg荷重で30秒圧縮した時の容積を求めることで行った。結果を表1に示す。なお、表1において膨嵩性は、後述する比較例1の膨嵩性の値を基準として、該基準値に対する膨嵩性の増加率(%)で示した。 The swelling property of the obtained tobacco sheet was measured. Specifically, after leaving the tobacco sheet in a conditioned room at 22° C. and 60% for 48 hours, the swelling property was measured with DD-60A (trade name, manufactured by Borgwald). The measurement was carried out by placing 15 g of tobacco sheet in a cylindrical container with an inner diameter of 60 mm and compressing the container with a load of 3 kg for 30 seconds to obtain the volume. Table 1 shows the results. In addition, in Table 1, the swelling property is shown as an increase rate (%) of the swelling property with respect to the reference value of the swelling property value of Comparative Example 1 described later.
 [比較例1]
 実施例1と同様の方法により圧延成形品を作製した。その後、複数のリング型の回転刃で短冊状に切断した。さらに長さが20mmとなるように切断することで、長さ:20mm、幅:0.8mmの波型形状が付与されていないたばこシートを得た。得られたたばこシートについて、実施例1と同様に膨嵩性を測定した。結果を表1に示す。
[Comparative Example 1]
A roll-formed product was produced in the same manner as in Example 1. After that, it was cut into strips with a plurality of ring-shaped rotary blades. Further, the tobacco sheet was cut to a length of 20 mm to obtain a tobacco sheet having a length of 20 mm and a width of 0.8 mm. The swelling property of the obtained tobacco sheet was measured in the same manner as in Example 1. Table 1 shows the results.
Figure JPOXMLDOC01-appb-T000001
Figure JPOXMLDOC01-appb-T000001
 表1より、本実施形態に係るたばこシートである実施例1のたばこシートでは、波型形状が付与されていない比較例1のたばこシートと比較して膨嵩性が向上した。 As can be seen from Table 1, the tobacco sheet of Example 1, which is the tobacco sheet according to the present embodiment, has improved swelling properties compared to the tobacco sheet of Comparative Example 1, which is not provided with a corrugated shape.
[参考例1a]
 1.喫煙用組成物シートの調製
 公知の抄造法で製造されたたばこシート(喫煙用組成物シート)を準備した。当該たばこシートをラッパーに充填し喫煙用セグメントとし、図2に示す非燃焼加熱型香味吸引物品を調製した。
[Reference Example 1a]
1. Preparation of Smoking Composition Sheet A tobacco sheet (smoking composition sheet) manufactured by a known papermaking method was prepared. A wrapper was filled with the tobacco sheet to form a smoking segment, and a non-combustion heating type flavor inhalation article shown in FIG. 2 was prepared.
 2.フルクタン又はフルクトース含有喫煙用組成物シートの調製
 プロピレングリコールと水との混合液(プロピレングリコール:水=1:9(質量比)):90gに対して、イヌリン型フルクタン(フジ日本精糖社製、製品名 Fuji FF):10gを加え混合することにより、イヌリン型フルクタンの溶液を得た。そして、上記1.と同様のたばこシートを準備し、当該たばこシートの全体に行き渡るように、イヌリン型フルクタンの溶液をシリンジを用いて添加することにより、添加後の(イヌリン型フルクタンを含有する)喫煙用組成物シート全体に対するイヌリン型フルクタンの含有量が0.5、1.0、2.0、3.0、又は3.5質量%である各シートを得た。
2. Preparation of fructan- or fructose-containing composition sheet for smoking Mixed solution of propylene glycol and water (propylene glycol: water = 1:9 (mass ratio)): 90 g of inulin-type fructan Name Fuji FF): 10 g was added and mixed to obtain an inulin-type fructan solution. And the above 1. A smoking composition sheet (containing an inulin-type fructan) after addition is prepared by adding a solution of inulin-type fructan using a syringe so as to spread over the entire tobacco sheet. Each sheet having an inulin-type fructan content of 0.5, 1.0, 2.0, 3.0, or 3.5% by mass was obtained.
 また、プロピレングリコールと水との混合液(プロピレングリコール:水=1:9(質量比)):90gに対して、フルクトース(八宝食産株式会社社製、製品名:果糖):10gを加え混合することにより、フルクトースの溶液を得た。そして、上記1.と同様のたばこシートを準備し、当該たばこシートの全体に行き渡るように、フルクトースの溶液をシリンジを用いて添加することにより、添加後の(フルクトースを含有する)喫煙用組成物シート全体に対するフルクトースの含有量が0.5、1.0、2.0、3.0、又は3.5質量%である各シートを得た。 In addition, 10 g of fructose (manufactured by Happo Shokusan Co., Ltd., product name: fructose) is added to 90 g of a mixture of propylene glycol and water (propylene glycol: water = 1:9 (mass ratio)). A solution of fructose was obtained by mixing. And the above 1. Prepare a similar tobacco sheet, and add a solution of fructose using a syringe so that it spreads throughout the tobacco sheet, so that the fructose for the entire smoking composition sheet (containing fructose) after addition Each sheet with a content of 0.5, 1.0, 2.0, 3.0, or 3.5% by weight was obtained.
 上記のようにして得られたフルクタン含有喫煙用組成物シート又はフルクトース含有喫煙用組成物シートをラッパーに充填し喫煙用セグメントとし、図2に示す非燃焼加熱型香味吸引物品を調製した。 A wrapper was filled with the fructan-containing smoking composition sheet or fructose-containing composition sheet obtained as described above to form a smoking segment, and the non-combustion heating type flavor inhalation article shown in FIG. 2 was prepared.
 上記イヌリン型フルクタンは、フルクタンの一種であり、イヌリン型フルクタンを含有する喫煙用組成物シートは本願の実施例に相当する。一方、上記フルクトースは単糖類の一種であり、フルクトースを含有する喫煙用組成物シートは本願の比較例に相当する。 The above inulin-type fructan is one type of fructan, and smoking composition sheets containing inulin-type fructans correspond to examples of the present application. On the other hand, the fructose is one type of monosaccharide, and the smoking composition sheet containing fructose corresponds to the comparative example of the present application.
 3.香味及び香喫味阻害感の評価
 上記1又は2のように調製した各非燃焼加熱型香味吸引物品を、図3に示す非燃焼外部加熱型喫煙システムに設置した。
 このようにして準備した各香味吸引物品について、十分に訓練された10名のパネラーにより香味及び香喫味阻害感の評価を行った。本実施例及び比較例において、「香味」とは、たばこ由来の香味とイヌリン型フルクタン又はフルクトース由来の甘い香味とを合わせた香味を意味する。
 各喫煙試験用巻の香味及び香喫味阻害感の評価は、各パネラーが下記表1aの5段階の基準により評価し10名のパネラーの平均値を算出することにより行った。下記表1aの基準においては、イヌリン型フルクタン又はフルクトースを含まないシートと比較して同等であるものを3としている。平均値が小数第2位の値を有する場合は小数第2位を四捨五入することにより点数を算出した。評価結果を表2a及び3a並びに図5に示す。
3. Evaluation of Flavor and Flavor Inhibition Feeling Each of the non-combustion heating flavor inhalation articles prepared as described in 1 or 2 above was installed in the non-combustion external heating smoking system shown in FIG.
Each flavor inhalation article prepared in this way was evaluated for flavor and flavor inhibition by 10 well-trained panelists. In the present Examples and Comparative Examples, the term "flavor" means a combined flavor of tobacco-derived flavor and inulin-type fructan or fructose-derived sweet flavor.
The evaluation of the flavor and flavor inhibition feeling of each smoking test roll was performed by each panelist's evaluation according to the 5-level criteria in Table 1a below, and the average value of the 10 panelists was calculated. In the criteria in Table 1a below, 3 is equivalent to a sheet that does not contain inulin-type fructans or fructose. Scores were calculated by rounding to the second decimal place when the average value had a value of two decimal places. Evaluation results are shown in Tables 2a and 3a and FIG.
Figure JPOXMLDOC01-appb-T000002
Figure JPOXMLDOC01-appb-T000002
Figure JPOXMLDOC01-appb-T000003
Figure JPOXMLDOC01-appb-T000003
Figure JPOXMLDOC01-appb-T000004
Figure JPOXMLDOC01-appb-T000004
 上述のように、イヌリン型フルクタンを含有する喫煙用組成物シートは本願の実施例に相当し、一方、フルクトースを含有する喫煙用組成物シートは本願の比較例に相当する。 As described above, smoking composition sheets containing inulin-type fructans correspond to examples of the present application, while smoking composition sheets containing fructose correspond to comparative examples of the present application.
 表2a及び図5の結果より、イヌリン型フルクタンの含有量が増えるにつれて、香喫味阻害感の数値が減少し香喫味阻害感を抑制できることがわかった。特に、イヌリン型フルクタンの含有量が3.0質量%以上であると、香喫味阻害感の数値が1となり、極めて強力に香喫味阻害感を抑制できることがわかった。このように、香喫味阻害感を抑制する点では、イヌリン型フルクタンの含有量が大きい方が好ましいとわかった。一方、イヌリン型フルクタンの含有量が増えるにつれて、香味が低減する傾向があることがわかった。香味を重視する場合、香味の数値としては1.5以上が望ましいため、香味と香喫味阻害感の抑制効果とを両立する観点からは、イヌリン型フルクタンの含有量は0.5~3質量%が望ましいことがわかった。 From the results in Table 2a and Fig. 5, it was found that as the content of the inulin-type fructan increases, the numerical value of the sensation of flavor and taste inhibition decreases, and the sensation of flavor and taste inhibition can be suppressed. In particular, when the content of the inulin-type fructan is 3.0% by mass or more, the numerical value of the feeling of flavor and taste inhibition becomes 1, indicating that the feeling of flavor and taste inhibition can be suppressed extremely strongly. As described above, it was found that a higher content of inulin-type fructans is preferable from the viewpoint of suppressing the sense of inhibition of flavor and taste. On the other hand, it was found that as the content of inulin-type fructan increased, the flavor tended to decrease. When the flavor is emphasized, the value of the flavor is preferably 1.5 or more. Therefore, from the viewpoint of achieving both the flavor and the effect of suppressing the feeling of inhibition of the flavor, the content of the inulin-type fructan is 0.5 to 3% by mass. was found to be desirable.
 一方、表3a及び図5の結果より、フルクトースの添加によっても一定の香喫味阻害感を抑制する効果があることがわかった。しかし、表2a及び図5に示したイヌリン型フルクタンに比べて、フルクトースは香喫味阻害感を抑制する効果が低く不十分であることがわかった。 On the other hand, from the results in Table 3a and Fig. 5, it was found that the addition of fructose also had the effect of suppressing the feeling of inhibition of flavor and taste to a certain extent. However, compared with the inulin-type fructans shown in Table 2a and FIG. 5, fructose was found to have a low and insufficient effect of suppressing the sense of flavor and taste inhibition.
 また、フルクトースに関して、パネラーからは、香喫味阻害感が喫煙後半になって増えてくる(香喫味阻害感の抑制効果が長続きしない)というコメントがあったため、下記実施例2に示すように、イヌリン型フルクタン及びフルクトースに関して、香喫味阻害感抑制効果持続性について比較実験を行った。 Regarding fructose, a panelist commented that the feeling of inhibition of flavor and taste increases in the latter half of smoking (the effect of suppressing the feeling of inhibition of flavor and taste does not last long). A comparative experiment was carried out on the persistence of inhibitory effects on flavor and taste inhibition sensations of type fructans and fructose.
[参考例2a]
 1.香喫味阻害感抑制効果持続性の評価
 上記参考例1aの「2.フルクタン又はフルクトース含有喫煙用組成物シートの調製」と同様にして調製した非燃焼加熱型香味吸引物品を、図2に示す非燃焼外部加熱型喫煙システムに設置した。
 このようにして準備した各香味吸引物品について、十分に訓練された10名のパネラーにより香喫味阻害感抑制効果持続性の評価を行った。各喫煙試験用巻の香喫味阻害感抑制効果持続性の評価は、喫煙後半までの香喫味阻害感抑制効果及び喫煙後の香喫味阻害感の後残りが無いことについて、各パネラーが下記表4aの5段階の基準により評価し10名のパネラーの平均値を算出することにより行った。平均値が小数第2位の値を有する場合は小数第2位を四捨五入することにより点数を算出した。
 下記表4aの基準において、イヌリン型フルクタンの含有量の違いによる香喫味阻害感抑制効果持続性を評価する場合には、フルクトースを2.0質量%含むシートと比較して同等であるものを3としている。また、フルクトースの含有量の違いによる香喫味阻害感抑制効果持続性を評価する場合には、イヌリン型フルクタンを2.0質量%含むシートと比較して同等であるものを3としている。
 評価結果を表5a及び6a並びに図6に示す。
[Reference Example 2a]
1. Evaluation of Sustainability of Suppressing Effect of Inhibiting Flavor and Taste Inhibition A non-combustion-heating flavor inhalation article prepared in the same manner as in “2. Installed in a combustion externally heated smoking system.
For each flavor inhalation article thus prepared, 10 well-trained panelists evaluated the persistence of the effect of suppressing the sense of inhibition of flavor-smelling taste. For the evaluation of the persistence of the inhibitory effect on the flavor and taste inhibition of each smoking test volume, each panelist was asked to evaluate the effect of suppressing the flavor and taste inhibition until the second half of smoking and the absence of residual after smoking. Table 4a below. , and the average value of 10 panelists was calculated. Scores were calculated by rounding to the second decimal place when the average value had a value of two decimal places.
In the criteria of Table 4a below, when evaluating the persistence of the inhibitory effect on flavor and taste inhibition due to the difference in the content of the inulin-type fructan, 3 equivalent sheets were compared with a sheet containing 2.0% by mass of fructose. and In addition, when evaluating the persistence of the inhibitory effect on flavor and taste inhibition due to the difference in fructose content, 3 is equivalent to a sheet containing 2.0% by mass of inulin-type fructan.
Evaluation results are shown in Tables 5a and 6a and FIG.
Figure JPOXMLDOC01-appb-T000005
Figure JPOXMLDOC01-appb-T000005
Figure JPOXMLDOC01-appb-T000006
Figure JPOXMLDOC01-appb-T000006
Figure JPOXMLDOC01-appb-T000007
Figure JPOXMLDOC01-appb-T000007
 表5a及び図6の結果より、イヌリン型フルクタンは、0.5~3.5質量%のいずれの含有量においても、比較対象の2.0質量%のフルクトースに比べて、香喫味阻害感抑制効果の持続性に優れることがわかった。
 また、表6a及び図6の結果より、フルクトースは、0.5~3.5質量%のいずれの含有量においても、比較対象の2.0質量%のイヌリン型フルクタンに比べて、香喫味阻害感抑制効果の持続性に劣ることがわかった。
 イヌリン型フルクタンは、カラメル化反応により甘い香味を発生させるまでに熱分解の過程を経るため、ゆっくりと長時間にわたって甘い香味を発生させると考えられる。一方、フルクトースは、カラメル化反応により、短時間で甘い香味を発生させると考えられる。甘い香味により香喫味阻害感は抑制されるので、このような甘い香味の発生時間の違いにより、香喫味阻害感抑制効果の持続性の違いが生じたと考えられる。
 以上の結果より、イヌリン型フルクタンはフルクトースよりも香喫味阻害感抑制効果の持続性に優れることが確認できた。
From the results of Table 5a and FIG. 6, the inulin-type fructan suppresses the sensation of flavor and taste inhibition at any content of 0.5 to 3.5% by mass, compared to the 2.0% by mass fructose for comparison. It was found to be excellent in the durability of the effect.
In addition, from the results of Table 6a and FIG. 6, fructose, at any content of 0.5 to 3.5% by mass, compared to the 2.0% by mass inulin-type fructan for comparison, inhibited flavor and taste. It was found that the persistence of the anti-sensitivity effect was inferior.
Inulin-type fructans undergo a process of thermal decomposition before they develop a sweet flavor through a caramelization reaction, so it is thought that they slowly generate a sweet flavor over a long period of time. On the other hand, fructose is thought to generate a sweet flavor in a short period of time through a caramelization reaction. Since the sweet flavor suppresses the sense of inhibition of flavor-smelling taste, it is considered that the difference in duration of the effect of suppressing the sense of inhibition of flavor-drinking taste is caused by the difference in the generation time of the sweet flavor.
From the above results, it was confirmed that the inulin-type fructan is superior to fructose in the persistence of the inhibitory effect on flavor and taste inhibition.
 以上より、本例のたばこ材料は、喫煙行動の初期から後期まで継続して香喫味阻害感が抑制される(香喫味阻害感抑制効果の持続性に優れる)ことがわかった。 From the above, it was found that the tobacco material of this example continuously suppresses the sense of flavor and taste inhibition from the early stage to the latter stage of smoking behavior (excellent persistence of the effect of suppressing the sense of flavor and taste inhibition).
[参考例1b]
 成分(A)として、抄造たばこシートを準備した。当該シートはたばこ材料とエアロゾル発生剤として15質量%のベジタブルグリセリンを含有していた。成分(B)として表1bに示す飽和脂肪酸を準備し、当該シートに噴霧した。たばこ組成物(抄造たばこシートと成分(B)の合計)の乾物質量当たりの成分(B)の添加量は、表1bに示すとおりである。例えば例A1では、たばこ組成物の乾物質量当たりのオクタン酸の添加量は1.0質量%であった。
[Reference Example 1b]
A paper-made tobacco sheet was prepared as the component (A). The sheet contained tobacco material and 15% by weight of vegetable glycerin as an aerosol generator. A saturated fatty acid shown in Table 1b was prepared as component (B) and sprayed onto the sheet. The amount of component (B) added per dry matter amount of the tobacco composition (total of the paper-made tobacco sheet and component (B)) is as shown in Table 1b. For example, in Example A1, the amount of octanoic acid added was 1.0% by weight per dry matter of the tobacco composition.
Figure JPOXMLDOC01-appb-T000008
Figure JPOXMLDOC01-appb-T000008
 前記シートを乾燥した後、複数のスリットを設けた後に巻き上げてたばこロッドを得た。この際、スリットの長手方向がたばこセグメントの長手方向と平行になるようにした。当該たばこロッドを用いて図2に示す構造の非燃焼加熱型たばこ香味吸引物品を製造した。各セグメントの長さは以下のとおりであった。
 たばこセグメント:12mm
 センターホール部:8mm
 紙管:20mm
 アセテートフィルタ:40mm
 外径3.2mm、内径1.3mmの中空円筒ヒーターを用いて、以下の条件で当該非燃焼加熱型たばこ香味吸引物品を加熱して、喫煙試験を実施した。
 電圧:印加電圧3.0Vに設定
 温度プロファイル:320℃一定
 予備加熱時間(喫煙開始前):ヒーターを巻部に挿入後、30秒加熱
 十分に訓練されたパネリスト10名によって、Visual Analog Scale(カテゴリー尺度)法により、成分(B)を添加せずに製造した非燃焼加熱型たばこ香味吸引物品(下記比較参考例参照)を比較対象として試験を実施した。結果を表1bに示す。得点差が低いほど不快感が少ないことを意味する。
After drying the sheet, a plurality of slits were provided and then rolled up to obtain a tobacco rod. At this time, the longitudinal direction of the slit was made parallel to the longitudinal direction of the tobacco segment. Using the tobacco rod, a non-combustion heating tobacco flavor inhalation article having the structure shown in FIG. 2 was manufactured. The length of each segment was as follows.
Tobacco segment: 12mm
Center hole part: 8mm
Paper tube: 20mm
Acetate filter: 40mm
Using a hollow cylindrical heater with an outer diameter of 3.2 mm and an inner diameter of 1.3 mm, the non-combustion heating tobacco flavor inhalation article was heated under the following conditions to carry out a smoking test.
Voltage: Applied voltage set to 3.0 V Temperature profile: Constant at 320°C Preheating time (before starting smoking): Heating for 30 seconds after inserting the heater into the winding part Visual Analog Scale (category A non-combustion-heating tobacco flavor inhalation article (see Comparative Reference Examples below) manufactured without adding component (B) was tested according to the scale) method as a comparison. The results are shown in Table 1b. A lower score difference means less discomfort.
[参考比較例1b]
 成分(B)を用いなかった以外は、参考例1bと同じ方法で非燃焼加熱型たばこ香味吸引物品を製造した。
[Reference Comparative Example 1b]
A non-combustion heating tobacco flavor inhalation article was produced in the same manner as in Reference Example 1b, except that component (B) was not used.
[参考例2b]
 以下の材料を準備した。
 成分(A):たばこラミナ(オリエント種以外)、たばこラミナ(オリエント種)
 成分(B):パルミチン酸、ショ糖パルミチン酸エステル
 その他:リコリス、液糖、針葉樹パルプ、グリセリン、バインダー(グアーガム)
[Reference Example 2b]
The following materials were prepared.
Component (A): tobacco lamina (other than Orient species), tobacco lamina (Orient species)
Ingredient (B): Palmitic acid, sucrose palmitate Others: licorice, liquid sugar, softwood pulp, glycerin, binder (guar gum)
 以下の手順で、非燃焼加熱型たばこ香味吸引物品を製造し、評価した。
 1)たばこラミナをラボミルで粉砕し、原料粒径D90=100μmのたばこ細粉を得た。
 2)顆粒状のパルミチン酸およびショ糖パルミチン酸エステルをラボミルで粉砕し、パウダーを得た。
 3)針葉樹パルプをラボミルで解砕した。
 4)これらの粉末状の材料をKenミキサーに入れ、撹拌混合した。
 5)ミキサー内に、水、グリセリン、リコリス、液糖、バインダー等の液体またはペースト状材料をディスパーサー(Primix社製)に入れて、30分間混合した。
 6)この混合物に、前記パルプを加え、ディスパーサー(Primix社製)で30分間分散させた。
 7)前記4)で得た粉末の混合物を6)の分散液に加えて、ディスパーサー(Primix社製)で30分間混合した。
 8)前記7)で得た混合物を鉄板にキャストした。
 9)前記キャスト膜が形成された鉄板を80℃設定の通風乾燥機にいれ、30分乾燥した後、鉄板から剥離してシート状のたばこ組成物を得た。当該シートの厚さは150μm、坪量は150g/mであった。
 10)シート状たばこ組成物をシュレッダーにかけ、1mm×10mmの刻状たばこ組成物を得た。
 11)所定量の刻状たばこ組成物をφ7×20mmのサイズに巻紙で巻き上げ、単巻を製造した。
 12)単巻をたばこロッドとして用い、図2に示す非燃焼加熱型たばこ香味吸引物品を得た。
 13)当該非燃焼加熱型たばこ香味吸引物品を、加熱デバイス(日本たばこ産業株式会社製 PloomS)に挿入し、加熱して、喫煙評価に供した。十分に訓練されたパネリストによる官能評価を行った。評価結果を表2bに示した。
A non-combustion heated tobacco flavor inhalation article was manufactured and evaluated by the following procedure.
1) Tobacco lamina was pulverized with a lab mill to obtain fine tobacco powder having a raw material particle size D90 of 100 μm.
2) Granular palmitic acid and sucrose palmitate were pulverized with a lab mill to obtain a powder.
3) The softwood pulp was crushed with a lab mill.
4) These powdered materials were placed in a Ken mixer and mixed by stirring.
5) Liquid or pasty materials such as water, glycerin, licorice, liquid sugar, binder, etc. were placed in a mixer (manufactured by Primix) and mixed for 30 minutes.
6) The pulp was added to this mixture and dispersed for 30 minutes with a disperser (manufactured by Primix).
7) The powder mixture obtained in 4) above was added to the dispersion liquid in 6) and mixed with a disperser (manufactured by Primix) for 30 minutes.
8) The mixture obtained in 7) was cast on an iron plate.
9) The iron plate on which the cast film was formed was placed in a ventilation dryer set at 80° C., dried for 30 minutes, and then separated from the iron plate to obtain a sheet-like tobacco composition. The sheet had a thickness of 150 μm and a basis weight of 150 g/m 2 .
10) The sheet tobacco composition was shredded to obtain a shredded tobacco composition of 1 mm x 10 mm.
11) A predetermined amount of the shredded tobacco composition was rolled up with wrapping paper into a size of φ7×20 mm to produce a single roll.
12) A single roll was used as a tobacco rod to obtain a non-combustion heating tobacco flavor inhalation article shown in FIG.
13) The non-combustion heated tobacco flavor inhalation article was inserted into a heating device (PloomS manufactured by Japan Tobacco Inc.), heated, and subjected to smoking evaluation. Sensory evaluation was performed by well-trained panelists. The evaluation results are shown in Table 2b.
[参考比較例2b]
 各成分の配合量を表2bに示すように変更した以外は、参考例2bと同じ方法で非燃焼加熱型たばこ香味吸引物品を製造し、評価した。
[Reference Comparative Example 2b]
A non-combustion heating tobacco flavor inhalation article was produced and evaluated in the same manner as in Reference Example 2b, except that the amount of each component was changed as shown in Table 2b.
Figure JPOXMLDOC01-appb-T000009
Figure JPOXMLDOC01-appb-T000009
 上記から、本例のたばこ製剤によって、喫煙時の不快感が低減されることが明らかである。 From the above, it is clear that the tobacco preparation of this example reduces discomfort during smoking.
[参考比較例1c]
 公知の抄造法で製造されたたばこシートを準備した。当該たばこシートをラッパーに充填したばこセグメントとし、図2に示す非燃焼加熱型香味吸引物品を調製した。当該物品について、十分に訓練されたパネリスト10名(平均年齢40歳)によって喫煙試験を実施した。
[Reference Comparative Example 1c]
A tobacco sheet manufactured by a known papermaking method was prepared. A wrapper was filled with the tobacco sheet to form a tobacco segment, and a non-combustion heating type flavor inhalation article shown in FIG. 2 was prepared. The article was subjected to a smoking test by 10 well-trained panelists (average age 40 years).
[参考例1c、参考比較例2c]
 リグニンおよびヘミセルロースの合計含有量が0.1~10質量%である紙(材料1~7)と、当該含有量が10質量%を超える紙(材料8~10)を準備した。参考比較例1cで準備したものと同じたばこシートおよび各紙を、それぞれ幅が0.3~2.0mm、長さが3~50mmとなるように裁刻した。紙の裁刻物とたばこシートの裁刻物を、質量比で80:20となるように混合し、参考比較例1cと同じ方法で非燃焼加熱型香味吸引物品を調製し、喫煙試験に供した。参考比較例1cの結果を基準とし、香喫味、煙量について以下の基準で評価した。
  1:大いに減る
  2:減る
  3:変わらない(基準)
  4:増える
  5:大いに増える
[Reference Example 1c, Reference Comparative Example 2c]
Papers with a total lignin and hemicellulose content of 0.1 to 10% by mass (Materials 1 to 7) and papers with a total lignin and hemicellulose content of more than 10% by mass (Materials 8 to 10) were prepared. The same tobacco sheet and each paper prepared in Reference Comparative Example 1c were cut into pieces having a width of 0.3 to 2.0 mm and a length of 3 to 50 mm. The cut pieces of paper and cut pieces of tobacco sheet were mixed at a mass ratio of 80:20, and a non-combustion heating type flavor inhalation article was prepared in the same manner as in Reference Comparative Example 1c, and subjected to a smoking test. did. Based on the results of Reference Comparative Example 1c, the smoking flavor and smoke amount were evaluated according to the following criteria.
1: Decrease significantly 2: Decrease 3: No change (standard)
4: increase 5: greatly increase
 繊維臭については以下の基準で評価した。
  1:なし(基準)
  2:非常に低い
  3:低い
  4:中程度
  5:強い
The fiber odor was evaluated according to the following criteria.
1: None (standard)
2: very low 3: low 4: moderate 5: strong
Figure JPOXMLDOC01-appb-T000010
Figure JPOXMLDOC01-appb-T000010
[参考例2c、参考比較例3c]
 たばこシートと、材料5とを、表2cに示す量でブレンドした以外は、参考例1cと同じ方法で非燃焼加熱型香味吸引物品を調製し、喫煙試験を行った。
[Reference Example 2c, Reference Comparative Example 3c]
A non-combustion heated flavor inhalation article was prepared and subjected to a smoking test in the same manner as in Reference Example 1c, except that the tobacco sheet and material 5 were blended in the amounts shown in Table 2c.
Figure JPOXMLDOC01-appb-T000011
Figure JPOXMLDOC01-appb-T000011
[参考例3c]
 たばこシートと材料5とを、表3cに示す量でブレンドした。ただし、材料5には、乾燥質量に対して、エアロゾル発生剤としてグリセリンを10質量%添加した。当該ブレンドを用いた以外は参考例1cと同じ方法で非燃焼加熱型香味吸引物品を調製し、喫煙試験を行った。
[Reference Example 3c]
Tobacco sheets and Material 5 were blended in the amounts shown in Table 3c. However, to Material 5, 10% by mass of glycerin was added as an aerosol generating agent with respect to the dry mass. A non-combustion heated flavor inhalation article was prepared in the same manner as in Reference Example 1c except that the blend was used, and a smoking test was conducted.
Figure JPOXMLDOC01-appb-T000012
Figure JPOXMLDOC01-appb-T000012
[ヘミセルロースの定量]
 1)紙をThermo ScientificTM DionexTM ASETM 高速溶媒抽出システム(型番:ASE-350)用いた溶媒抽出(溶媒:水)に供し、残渣を分離した。液体窒素等を用いて当該残渣を凍結粉砕して試料Aを得た。
 2)試料A50mgをスクリュー瓶に入れ、超純水(ML-Q水)8.5mlとパンクレアチン溶液0.5mlを加え、40℃、125rpmで16時間振盪した。次いでML-Q水を用いて前記試料液体を、15mlの遠沈管に移し、8000rpmで15分間遠心分離して、上清を取り除いた。この洗浄を三回繰り返し行った。洗浄後、5%硫酸水溶液10mlを加え、100℃にて2.5時間加水分解を行った。加水分解反応終了後、試料を室温まで放冷した。次いで、沈殿物をろ別し、ろ液を250mlのメスフラスコに回収した。ろ紙上の残渣をML-Q水で十分に洗浄した後、250mlに定容した。この溶液をヘミセルロース測定用試料とした。
 3)当該試料500μlを20ml試験管に移し、5%フェノール水溶液500μlと濃硫酸2.5mlを加え、十秒間激しく撹拌した。当該試料を室温にて20分以上放置し、分光光度計を使用して波長490nmで吸光度測定を行い、ヘミセルロースを定量した。
[Quantification of hemicellulose]
1) The paper was subjected to solvent extraction (solvent: water) using Thermo Scientific Dionex ASE Fast Solvent Extraction System (model number: ASE-350) to separate the residue. A sample A was obtained by freeze-pulverizing the residue using liquid nitrogen or the like.
2) 50 mg of sample A was placed in a screw bottle, 8.5 ml of ultrapure water (ML-Q water) and 0.5 ml of pancreatin solution were added, and the mixture was shaken at 40° C. and 125 rpm for 16 hours. The sample liquid was then transferred to a 15 ml centrifuge tube using ML-Q water and centrifuged at 8000 rpm for 15 minutes to remove the supernatant. This washing was repeated three times. After washing, 10 ml of a 5% sulfuric acid aqueous solution was added and hydrolysis was carried out at 100° C. for 2.5 hours. After the hydrolysis reaction was completed, the sample was allowed to cool to room temperature. The precipitate was then filtered off and the filtrate was collected in a 250 ml volumetric flask. After thoroughly washing the residue on the filter paper with ML-Q water, the volume was adjusted to 250 ml. This solution was used as a sample for hemicellulose measurement.
3) 500 µl of the sample was transferred to a 20 ml test tube, 500 µl of 5% phenol aqueous solution and 2.5 ml of concentrated sulfuric acid were added, and vigorously stirred for 10 seconds. The sample was allowed to stand at room temperature for 20 minutes or longer, and absorbance was measured at a wavelength of 490 nm using a spectrophotometer to quantify hemicellulose.
[リグニンの定量]
 i)前記試料Aを準備した。
 ii)試料A100mgをスクリュー瓶に入れ、72%硫酸4mlを加え、硫酸に試料を完全に浸らせ、30℃、200rpmにて4時間振盪した。次いで、希釈後の硫酸濃度が4%となるよう超純水(ML-Q水)157.2mlを加えてナスフラスコに移し、110℃のオイルバス中で2時間加熱還流を行った。
 iii)還流処理したものを室温まで放冷後、ろ過を行い、ロータリー乾熱機で乾燥し秤量し、リグニン量とした。
[Quantification of lignin]
i) The sample A was prepared.
ii) 100 mg of sample A was placed in a screw bottle, 4 ml of 72% sulfuric acid was added, the sample was completely immersed in sulfuric acid, and shaken at 30° C. and 200 rpm for 4 hours. Then, 157.2 ml of ultrapure water (ML-Q water) was added so that the concentration of sulfuric acid after dilution was 4%, transferred to an eggplant flask, and heated under reflux in an oil bath at 110° C. for 2 hours.
iii) After the reflux treatment was allowed to cool to room temperature, it was filtered, dried with a rotary drier, and weighed to determine the amount of lignin.
 本例のたばこセグメントは、香喫味を適度に希釈できることが明らかである。 It is clear that the tobacco segment of this example can moderately dilute the flavor and taste.
 以下に実施態様を示す。
[1]たばこ原料を含む非燃焼加熱型香味吸引器用たばこシートであって、前記たばこシートの厚み方向の断面が波型形状を有する、非燃焼加熱型香味吸引器用たばこシート。
[2]前記たばこシートがさらにエアロゾル発生剤を含む、[1]に記載の非燃焼加熱型香味吸引器用たばこシート。
[3]前記エアロゾル発生剤が、グリセリン、プロピレングリコール及び1,3-ブタンジオールからなる群から選択される少なくとも一つである、[2]に記載の非燃焼加熱型香味吸引器用たばこシート。
[4]前記たばこシート100質量%に含まれる前記エアロゾル発生剤の割合が4~50質量%である、[2]又は[3]に記載の非燃焼加熱型香味吸引器用たばこシート。
[5]前記たばこシートが、さらに第一の成型剤及び第二の成型剤を含む、[1]から[4]のいずれかに記載の非燃焼加熱型香味吸引器用たばこシート。
[6]前記第一の成型剤が、多糖類、タンパク及び合成ポリマーからなる群から選択される少なくとも一つである、[5]に記載の非燃焼加熱型香味吸引器用たばこシート。
[7]前記第二の成型剤が、前記第一の成型剤とは異なる、多糖類、タンパク及び合成ポリマーからなる群から選択される少なくとも一つである、[5]又は[6]に記載の非燃焼加熱型香味吸引器用たばこシート。
[8]前記たばこシート100質量%に含まれる前記第一の成型剤の割合が0.1~15質量%である、[5]から[7]のいずれかに記載の非燃焼加熱型香味吸引器用たばこシート。
[9]前記たばこシート100質量%に含まれる前記第二の成型剤の割合が0.1~15質量%である、[5]から[8]のいずれかに記載の非燃焼加熱型香味吸引器用たばこシート。
[10][1]~[9]のいずれかに記載の非燃焼加熱型香味吸引器用たばこシートを含むたばこ含有セグメントを備える非燃焼加熱型香味吸引器。
[11][10]に記載の非燃焼加熱型香味吸引器と、
 前記たばこ含有セグメントを加熱する加熱装置と、
を備える非燃焼加熱型香味吸引システム。
[12][1]から[9]のいずれかに記載の非燃焼加熱型香味吸引器用たばこシートの製造方法であって、
 たばこ原料、エアロゾル発生剤、第一の成型剤、及び第二の成型剤を含む混合物を調製する工程と、
 前記混合物を圧延して圧延成形品を形成する工程と、
 前記圧延成形品に回転式ロール刃を押し当てて短冊状に切断しつつ波型形状を付与する工程と、
を含む方法。
Embodiments are shown below.
[1] A tobacco sheet for a non-combustion heating type flavor inhaler containing a tobacco raw material, the tobacco sheet for a non-combustion heating type flavor inhaler having a corrugated cross-section in the thickness direction of the tobacco sheet.
[2] The tobacco sheet for a non-combustion heating type flavor inhaler according to [1], wherein the tobacco sheet further contains an aerosol generating agent.
[3] The tobacco sheet for non-combustion heating flavor inhalers according to [2], wherein the aerosol generating agent is at least one selected from the group consisting of glycerin, propylene glycol and 1,3-butanediol.
[4] The tobacco sheet for a non-combustion heating type flavor inhaler according to [2] or [3], wherein the ratio of the aerosol generating agent contained in 100% by mass of the tobacco sheet is 4 to 50% by mass.
[5] The tobacco sheet for a non-combustion heating type flavor inhaler according to any one of [1] to [4], further comprising a first molding agent and a second molding agent.
[6] The tobacco sheet for a non-combustion heating type flavor inhaler according to [5], wherein the first molding agent is at least one selected from the group consisting of polysaccharides, proteins and synthetic polymers.
[7] According to [5] or [6], wherein the second molding agent is at least one selected from the group consisting of polysaccharides, proteins and synthetic polymers, which is different from the first molding agent. non-combustion heated flavor inhaler tobacco sheet.
[8] The non-combustion heating type flavor inhalation according to any one of [5] to [7], wherein the ratio of the first molding agent contained in 100% by mass of the tobacco sheet is 0.1 to 15% by mass. Dexterous cigarette sheet.
[9] The non-combustion heating type flavor inhalation according to any one of [5] to [8], wherein the ratio of the second molding agent contained in 100% by mass of the tobacco sheet is 0.1 to 15% by mass. Dexterous cigarette sheet.
[10] A non-combustion heating flavor inhaler comprising a tobacco-containing segment including the tobacco sheet for a non-combustion heating flavor inhaler according to any one of [1] to [9].
[11] The non-combustion heating flavor inhaler according to [10];
a heating device for heating the tobacco-containing segment;
A non-combustion heated flavor suction system.
[12] A method for manufacturing a tobacco sheet for a non-combustion heating type flavor inhaler according to any one of [1] to [9],
preparing a mixture comprising a tobacco material, an aerosol-generating agent, a first shaping agent, and a second shaping agent;
rolling the mixture to form a rolled article;
A step of pressing a rotary roll blade against the rolled product to cut it into strips while imparting a corrugated shape;
method including.
 [1a] フルクタンを含むたばこ材料。
 [2a] 前記フルクタンが、イヌリン型フルクタン、レバン型フルクタン、分岐型フルクタン、フラクトオリゴ糖、及びこれらの混合物からなる群から選択される、[1a]に記載のたばこ材料。
 [3a] 前記たばこ材料全体に対する前記フルクタンの含有量が、0.5~3質量%である、[1a]又は[2]に記載のたばこ材料。
 [4a] たばこシート又はたばこ刻みを更に含む、[1a]~[3a]のいずれか1つに記載のたばこ材料。
 [5a] [1a]~[4a]のいずれか1つに記載のたばこ材料を含む、加熱型喫煙物品。
[1a] A tobacco material containing fructans.
[2a] The tobacco material according to [1a], wherein the fructan is selected from the group consisting of inulin-type fructans, levan-type fructans, branched fructans, fructooligosaccharides, and mixtures thereof.
[3a] The tobacco material according to [1a] or [2], wherein the fructan content relative to the entire tobacco material is 0.5 to 3% by mass.
[4a] The tobacco material according to any one of [1a] to [3a], further comprising tobacco sheets or tobacco shreds.
[5a] A heated smoking article comprising the tobacco material of any one of [1a] to [4a].
 [1b] (A)たばこ材料と、
 (B)飽和脂肪酸系添加剤と、を含むたばこ組成物であって、
 前記成分(B)が、モル質量が200~350g/molである飽和脂肪酸、当該飽和脂肪酸のエステル、およびこれらの組合せからなる群より選択され、
 当該組成物中の乾物質量当たり、成分(B)を0.01~3質量%含有する、たばこ組成物。
 [2b] 成分(B)における飽和脂肪酸および飽和脂肪酸エステルは、それぞれ単品である、[1b]に記載の組成物。
 [3b] 成分(B)の飽和脂肪酸および前記エステルにおける脂肪酸部位の炭素数が12~20である、[1b]または[2b]に記載の組成物。
 [4b] 前記組成物中の乾物質量当たり、1~10質量%の液糖をさらに含む、[1b]~[3b]のいずれかに記載の組成物。
 [5b] 成分(A)中に、10質量%以下のオリエント種由来の材料を含む、[1b]~[4b]のいずれかに記載の組成物。
 [6b] 前記組成物中の乾物質量当たり、0.5~3質量%の天然植物性香料をさらに含む、[1b]~[5b]のいずれかに記載の組成物。
 [7b] 前記組成物中の乾物質量当たり、2質量%以上のニコチンを含有する、[1b]~[6b]のいずれかに記載の組成物。
 [8b] 前記組成物中の乾物質量当たり、1.5質量%以下のニコチンを含有する、[1b]~[6b]のいずれかに記載の組成物。
 [9b] 前記組成物中の乾物質量当たり、12質量%以下のエアロゾル発生剤をさらに含む、[1b]~[8b]のいずれかに記載の組成物。
[10b]  [1b]~[9b]のいずれかに記載のたばこ組成物から形成されたシート。
[11b] 成分(A)と、一部または全部が粉末である成分(B)と、媒体とを、前記粉末が粉末状態を保つように混合してスラリーとする工程、
を備える、[1b]~[10b]のいずれかに記載のたばこ組成物の製造方法。
[12b] 前記スラリーの粘度を100,000~200,000(mPa・s)とすることをさらに備える、[11b]に記載の製造方法。
[1b] (A) a tobacco material;
(B) a tobacco composition comprising a saturated fatty acid additive,
said component (B) is selected from the group consisting of saturated fatty acids having a molar mass of 200 to 350 g/mol, esters of said saturated fatty acids, and combinations thereof;
A tobacco composition containing 0.01 to 3% by weight of component (B) based on the amount of dry matter in the composition.
[2b] The composition according to [1b], wherein the saturated fatty acid and saturated fatty acid ester in component (B) are each a single item.
[3b] The composition according to [1b] or [2b], wherein the fatty acid moiety in the saturated fatty acid and the ester of component (B) has 12 to 20 carbon atoms.
[4b] The composition according to any one of [1b] to [3b], further comprising 1 to 10% by mass of liquid sugar based on the amount of dry matter in the composition.
[5b] The composition according to any one of [1b] to [4b], wherein component (A) contains 10% by mass or less of a material derived from oriental species.
[6b] The composition according to any one of [1b] to [5b], further comprising 0.5 to 3% by mass of a natural botanical fragrance based on the amount of dry matter in the composition.
[7b] The composition according to any one of [1b] to [6b], containing 2% by mass or more of nicotine based on the amount of dry matter in the composition.
[8b] The composition according to any one of [1b] to [6b], containing 1.5% by mass or less of nicotine based on the amount of dry matter in the composition.
[9b] The composition according to any one of [1b] to [8b], further comprising 12% by mass or less of an aerosol-generating agent based on the amount of dry matter in the composition.
[10b] A sheet formed from the tobacco composition according to any one of [1b] to [9b].
[11b] A step of mixing the component (A), the component (B) partially or wholly powder, and a medium so as to keep the powder in a powder state to form a slurry;
A method for producing a tobacco composition according to any one of [1b] to [10b], comprising:
[12b] The production method according to [11b], further comprising setting the viscosity of the slurry to 100,000 to 200,000 (mPa·s).
 [1c]充填物として、
 たばこ材料と、
 紙と、を含み、
 前記紙のリグニンおよびヘミセルロースの合計含有量が0.1~10質量%である、
 加熱用たばこセグメント。
 [2c]充填物として、
 たばこ材料と、
 エアロゾル発生剤を含有する紙と、を含む、
 加熱用たばこセグメント。
 [3c]前記リグニンおよびヘミセルロースの合計含有量が9.0質量%以下である、[1c]に記載のたばこセグメント。
 [4c]前記紙の含有量が、前記たばこ材料の乾物質量に対して5~70質量%である、[1c]または[3c]に記載のたばこセグメント。
 [5c]前記紙の含有量が、前記たばこ材料の乾物質量に対して15~40質量%である、
[4c]に記載のたばこセグメント。
 [6c]前記紙の密度が0.05~0.8[g/cm]である、[1c]~[5c]のいずれかに記載のたばこセグメント。
 [7c]前記紙の含有量が、前記たばこ材料の乾物質量に対して5~75質量%である、[2c]または[6c]に記載のたばこセグメント。
 [8c]前記紙がエアロゾル発生剤を含む、[1c]または[3c]~[6c]のいずれかに記載のたばこセグメント。
 [9c]前記[1c]~[8c]のいずれかに記載のたばこセグメントを備える、非燃焼加熱型香味吸引物品。
 [10c]たばこ材料に、前記紙を混合することを含む、[1c]~[8c]のいずれかに記載のたばこセグメントの製造方法。
[1c] As a filling,
tobacco material;
including paper and
The total content of lignin and hemicellulose in the paper is 0.1 to 10% by mass,
heating tobacco segment;
[2c] as a filler,
tobacco material;
a paper containing an aerosol-generating agent;
heating tobacco segment;
[3c] The tobacco segment according to [1c], wherein the total content of lignin and hemicellulose is 9.0% by mass or less.
[4c] The tobacco segment according to [1c] or [3c], wherein the content of the paper is 5-70% by mass relative to the dry matter content of the tobacco material.
[5c] The content of the paper is 15-40% by mass relative to the dry matter content of the tobacco material.
The tobacco segment according to [4c].
[6c] The tobacco segment according to any one of [1c] to [5c], wherein the paper has a density of 0.05 to 0.8 [g/cm 3 ].
[7c] The tobacco segment of [2c] or [6c], wherein the content of the paper is 5-75% by mass relative to the dry matter content of the tobacco material.
[8c] The tobacco segment of any of [1c] or [3c]-[6c], wherein said paper comprises an aerosol-generating agent.
[9c] A non-combustion heating flavor inhalation article comprising the tobacco segment according to any one of [1c] to [8c] above.
[10c] The method for producing a tobacco segment according to any one of [1c] to [8c], comprising mixing the paper with the tobacco material.
1  たばこシート
2  波
3  鋸歯形状
4  非燃焼加熱型香味吸引器
5  たばこ含有セグメント
6  冷却セグメント
7  センターホールセグメント
8  フィルターセグメント
9  マウスピースセグメント
10 筒状部材
11 穿孔
12 第二の充填層
13 第二のインナープラグラッパー
14 アウタープラグラッパー
15 マウスピースライニングペーパー
16 加熱装置
17 ボディ
18 ヒーター
19 金属管
20 電池ユニット
21 制御ユニット
22 凹部
 
20A たばこ含有セグメント
21 充填物
22 ラッパー
T たばこシート
P 紙
1 Tobacco sheet 2 Wave 3 Sawtooth shape 4 Non-combustion heated flavor inhaler 5 Tobacco-containing segment 6 Cooling segment 7 Center hole segment 8 Filter segment 9 Mouthpiece segment 10 Tubular member 11 Perforations 12 Second filling layer 13 Second Inner plug wrapper 14 Outer plug wrapper 15 Mouthpiece lining paper 16 Heating device 17 Body 18 Heater 19 Metal tube 20 Battery unit 21 Control unit 22 Recess
20A tobacco-containing segment 21 filler 22 wrapper T tobacco sheet P paper

Claims (11)

  1.  たばこ原料を含む非燃焼加熱型香味吸引器用たばこシートであって、前記たばこシートの厚み方向の断面が波型形状を有する、非燃焼加熱型香味吸引器用たばこシート。 A tobacco sheet for a non-combustion heating type flavor inhaler containing a tobacco raw material, the tobacco sheet for a non-combustion heating type flavor inhaler having a wavy cross section in the thickness direction of the tobacco sheet.
  2.  フルクタンをさらに含む、請求項1に記載の非燃焼加熱型香味吸引器用たばこシート。 The tobacco sheet for non-combustion heating type flavor inhalers according to claim 1, further comprising fructans.
  3.  前記フルクタンが、イヌリン型フルクタン、レバン型フルクタン、分岐型フルクタン、フラクトオリゴ糖、及びこれらの混合物からなる群から選択される、請求項1または2に記載の非燃焼加熱型香味吸引器用たばこシート。 The tobacco sheet for non-combustion heating flavor inhalers according to claim 1 or 2, wherein the fructan is selected from the group consisting of inulin-type fructans, levan-type fructans, branched fructans, fructooligosaccharides, and mixtures thereof.
  4.  飽和脂肪酸系添加剤をさらに含み、
     前記添加剤が、モル質量が200~350g/molである飽和脂肪酸、当該飽和脂肪酸のエステル、およびこれらの組合せからなる群より選択され、
     その含有量が、前記シートの乾物質量当たり、0.01~3質量%である、
    請求項1~3のいずれかに記載の非燃焼加熱型香味吸引器用たばこシート。
    further comprising a saturated fatty acid additive,
    said additive is selected from the group consisting of saturated fatty acids having a molar mass of 200-350 g/mol, esters of said saturated fatty acids, and combinations thereof;
    The content is 0.01 to 3% by weight based on the dry matter content of the sheet.
    The tobacco sheet for a non-combustion heating type flavor inhaler according to any one of claims 1 to 3.
  5.  前記飽和脂肪酸および飽和脂肪酸エステルは、それぞれ単品である、請求項4に記載の非燃焼加熱型香味吸引器用たばこシート。 The tobacco sheet for a non-combustion heating type flavor inhaler according to claim 4, wherein the saturated fatty acid and the saturated fatty acid ester are each a single item.
  6.  充填物として、
     請求項1~5のいずれかに記載のシートと、
     紙と、を含み、
     前記紙のリグニンおよびヘミセルロースの合計含有量が0.1~10質量%である、
     たばこ含有セグメント。
    as a filling,
    A sheet according to any one of claims 1 to 5;
    including paper and
    The total content of lignin and hemicellulose in the paper is 0.1 to 10% by mass,
    Tobacco-containing segment.
  7.  充填物として、
     請求項1~5のいずれかに記載のシートと、
     エアロゾル発生剤を含有する紙と、を含む、
     たばこ含有セグメント。
    as a filling,
    A sheet according to any one of claims 1 to 5;
    a paper containing an aerosol-generating agent;
    Tobacco-containing segment.
  8.  請求項1~5のいずれかに記載の非燃焼加熱型香味吸引器用たばこシートを含むたばこ含有セグメントあるいは
     請求項6または7に記載のたばこ含有セグメント
    を備える非燃焼加熱型香味吸引器。
    A tobacco-containing segment comprising the tobacco sheet for a non-combustion-heating flavor inhaler according to any one of claims 1 to 5, or a non-combustion-heating flavor inhaler comprising the tobacco-containing segment according to claim 6 or 7.
  9.  請求項8に記載の非燃焼加熱型香味吸引器と、
     前記たばこ含有セグメントを加熱する加熱装置と、
    を備える非燃焼加熱型香味吸引システム。
    The non-combustion heating flavor inhaler according to claim 8;
    a heating device for heating the tobacco-containing segment;
    A non-combustion heated flavor suction system.
  10.  請求項1~3のいずれかに記載の非燃焼加熱型香味吸引器用たばこシートの製造方法であって、
     たばこ原料と、エアロゾル発生剤と、第一の成型剤及び第二の成型剤と、を含む混合物を調製する工程と、
     前記混合物を圧延して圧延成形品を形成する工程と、
     前記圧延成形品に回転式ロール刃を押し当てて短冊状に切断しつつ波型形状を付与する工程と、
     必要に応じて、前記圧延成形品に前記フルクタンを添加する工程と、
    を備える方法。
    A method for producing a tobacco sheet for a non-combustion heating type flavor inhaler according to any one of claims 1 to 3,
    preparing a mixture comprising a tobacco raw material, an aerosol-generating agent, a first shaping agent and a second shaping agent;
    rolling the mixture to form a rolled article;
    A step of pressing a rotary roll blade against the rolled product to cut it into strips while imparting a corrugated shape;
    optionally adding the fructan to the rolled product;
    How to prepare.
  11.  請求項4または5に記載の非燃焼加熱型香味吸引器用たばこシートの製造方法であって、
     たばこ原料と、エアロゾル発生剤と、第一の成型剤及び第二の成型剤と、飽和脂肪酸系添加剤と、を含む混合物を調製する工程と、
     前記混合物を圧延して圧延成形品を形成する工程と、
     前記圧延成形品に回転式ロール刃を押し当てて短冊状に切断しつつ波型形状を付与する工程と、
    を備える方法。
    A method for producing a tobacco sheet for a non-combustion heating type flavor inhaler according to claim 4 or 5,
    preparing a mixture comprising a tobacco raw material, an aerosol-generating agent, a first molding agent and a second molding agent, and a saturated fatty acid-based additive;
    rolling the mixture to form a rolled article;
    A step of pressing a rotary roll blade against the rolled product to cut it into strips while imparting a corrugated shape;
    How to prepare.
PCT/JP2022/018913 2021-04-26 2022-04-26 Tobacco sheet for non-combustion heating-type fragrance inhaler and method for manufacturing same, non-combustion heating-type fragrance inhaler, and non-combustion heating-type fragrance inhaling system WO2022230886A1 (en)

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JP2023517562A JPWO2022230886A1 (en) 2021-04-26 2022-04-26
EP22795799.0A EP4331389A1 (en) 2021-04-26 2022-04-26 Tobacco sheet for non-combustion heating-type fragrance inhaler and method for manufacturing same, non-combustion heating-type fragrance inhaler, and non-combustion heating-type fragrance inhaling system
KR1020237040043A KR20240000551A (en) 2021-04-26 2022-04-26 Tobacco sheet for non-combustion heating type flavor inhaler and manufacturing method thereof, non-combustion heating type flavor inhaler, and non-combustion heating type flavor inhalation system
US18/493,162 US20240049767A1 (en) 2021-04-26 2023-10-24 Tobacco sheet for non-combustion heating-type fragrance inhaler and method for manufacturing same, non-combustion heating-type fragrance inhaler, and non-combustion heating-type fragrance inhaling system

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JP2018516075A (en) * 2015-05-29 2018-06-21 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム How to make tobacco cut filler
JP2018533916A (en) * 2015-09-16 2018-11-22 アレクサンドラ ディルマン Method and apparatus for treating vaporized liquid streams supplied by electronic cigarettes, and electronic cigarettes for oral ingestion of vaporized liquids containing additive compositions
WO2019049619A1 (en) * 2017-09-05 2019-03-14 日本製紙パピリア株式会社 Water-dispersible sheet
CN111084405A (en) * 2020-02-19 2020-05-01 安徽集友广誉科技有限公司 Reconstituted tobacco sheet and preparation method thereof
JP2020520638A (en) * 2017-05-24 2020-07-16 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム Homogenized botanical material containing basic pH adjuster
JP2020114206A (en) * 2018-12-20 2020-07-30 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム Aerosol-generating article with light hollow segment

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JPS6045914B2 (en) 1983-09-26 1985-10-12 日本たばこ産業株式会社 Manufacturing method for wrinkled sheet cigarettes
WO2009084458A1 (en) * 2007-12-27 2009-07-09 Japan Tobacco Inc. Non-combustion type smoking article with carbonaceous heat source
US20160208440A1 (en) * 2015-01-16 2016-07-21 R.J. Reynolds Tobacco Company Tobacco-derived cellulose material and products formed thereof
JP2018516075A (en) * 2015-05-29 2018-06-21 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム How to make tobacco cut filler
JP2018533916A (en) * 2015-09-16 2018-11-22 アレクサンドラ ディルマン Method and apparatus for treating vaporized liquid streams supplied by electronic cigarettes, and electronic cigarettes for oral ingestion of vaporized liquids containing additive compositions
JP2020520638A (en) * 2017-05-24 2020-07-16 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム Homogenized botanical material containing basic pH adjuster
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JP2020114206A (en) * 2018-12-20 2020-07-30 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム Aerosol-generating article with light hollow segment
CN111084405A (en) * 2020-02-19 2020-05-01 安徽集友广誉科技有限公司 Reconstituted tobacco sheet and preparation method thereof

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